CN216125747U - High-efficient separation and extraction device of progesterone in red date - Google Patents
High-efficient separation and extraction device of progesterone in red date Download PDFInfo
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- CN216125747U CN216125747U CN202121930427.3U CN202121930427U CN216125747U CN 216125747 U CN216125747 U CN 216125747U CN 202121930427 U CN202121930427 U CN 202121930427U CN 216125747 U CN216125747 U CN 216125747U
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Abstract
The utility model discloses a high-efficiency separation and extraction device for progesterone in red dates, which comprises a stirring and crushing barrel, wherein a first rotating shaft in the stirring and crushing barrel is sleeved with an installation sleeve, after a crushed raw material enters an extraction box through a connecting pipeline, the crushed raw material can fall on a filter screen, a box door is opened, an ethanol solution is added into the extraction box, the solution is immersed in the crushed raw material on the filter screen, the extraction box is subjected to microwave heating through a microwave heating device on the outside, the extraction treatment method of microwave heating is adopted, the process can be simplified, the process flow is simple to operate and low in cost, the extraction rate of the red date progesterone is improved, the functional characteristics of the red date progesterone are kept, then the filter screen is hooked out through a hook ring, so that the extracted crushed red dates are taken out of the extraction box, then a flocculating agent is added into the extraction box, a concentrated solution with the progesterone can be obtained, and then the concentrated solution is led out through a discharge connecting pipe, thereby, progesterone can be rapidly extracted from the concentrated solution.
Description
Technical Field
The utility model relates to the technical field of progesterone extraction equipment, and particularly relates to a high-efficiency separation and extraction device for progesterone in red dates.
Background
As recorded in Chinese herbal books, the red dates have sweet taste and warm property, enter spleen and stomach channels, and have the functions of tonifying middle-jiao and Qi, nourishing blood and tranquilization and relieving drug property; modern pharmacology finds that red dates contain rich nutritional ingredients such as proteins, saccharides, organic acids, vitamin A, vitamin C, various trace amounts of calcium, amino acids and the like, and the red dates, also called the red dates, belong to angiosperms, dicotyledons, Rhamnales, Rhamnaceae and Ziziphus, have very high vitamin content, have the reputation of 'natural vitamin pills', have the effects of nourishing yin and tonifying yang and replenishing blood, have various functional ingredients in the red dates, and one important ingredient of the functional ingredients is flavonoid compounds, namely jujube flavone. The flavone can be used as a therapeutic drug and a health-care product, has the vitamin P-like effect, can reduce the permeability and fragility of capillary vessels, promote cell proliferation and prevent hemagglutination, has the effects of resisting inflammation, resisting allergy, promoting urination, relieving spasm, relieving cough, reducing blood fat and the like, is also called progesterone hormone and luteinizing hormone, is a main progestational hormone secreted by ovaries and has bioactivity, can protect the endometrium of a female, can provide support and guarantee for the early growth and development of a fetus during pregnancy of the female, and can play a certain role in calming the uterus. In addition, progesterone hormone and estrogen are closely related and both are important female hormones. The estrogen mainly promotes the development and maturation of the female second sexual characteristics, and the progesterone hormone further promotes the development and maturation of the second sexual characteristics on the basis of the action of the estrogen, so that the estrogen and the progesterone have a synergistic effect. It is mainly obtained by the oxidation of gestagen ketone. Adding dried toluene into a dry reaction pot, adding cyclohexanone and gestrinone, stirring for dissolving, evaporating toluene to remove water completely, rapidly adding aluminum isopropoxide, oxidizing at 115 deg.C for 2h, cooling to about 80 deg.C, adding 5% dilute sulfuric acid under stirring, standing for layering, removing water layer, washing toluene layer with water to neutrality, distilling with steam, and distilling to remove toluene and cyclohexanone. Cooling, filtering, stirring the filter residue with petroleum ether to obtain slurry, filtering, washing with petroleum ether, and drying to obtain progesterone crude product. Dissolving the crude product in ethanol, decolorizing with active carbon, and recrystallizing to obtain the final product with yield of 80%.
When existing equipment extracts progesterone through using the red dates, the preparation steps are separated and are tedious, and the red dates cannot be quickly crushed and sent out of a crushing device to be subjected to progesterone extraction.
SUMMERY OF THE UTILITY MODEL
The utility model mainly aims to provide a device for efficiently separating and extracting progesterone from red dates, which can effectively solve the problems in the background art.
In order to achieve the purpose, the utility model adopts the technical scheme that:
the utility model provides a progesterone high efficiency separation extraction element in red date, smashes the bucket including the stirring, and the last fixed surface of bucket is smashed in the stirring is connected with the top cap, the first servo motor of last fixed surface of top cap is connected with, the first pivot of one end fixedly connected with of first servo motor, the outer fixed surface of first pivot is connected with the installation cover, the outer fixed surface of installation cover is connected with the puddler, the lantern ring is smashed to the outer fixed surface of puddler, the lower fixed surface of bucket is smashed in the stirring is connected with second servo motor, the one end fixedly connected with second pivot of second servo motor, the outer fixed surface of second pivot is connected with the connecting sleeve, the rotatory push pedal of connecting sleeve's outer fixed surface is connected with.
In order to enable the raw materials to enter the extraction box, as the efficient separation and extraction device for the progesterone in the red dates, the inner wall of the outer surface of the stirring and crushing barrel is fixedly connected with the connecting pipeline, and one end of the connecting pipeline is fixedly connected with the extraction box.
In order to conveniently prepare the progesterone extracting solution, as the efficient separation and extraction device for progesterone in red dates, the inner wall of the extraction box is fixedly connected with a fixed filter screen, the upper surface of the fixed filter screen is provided with a filter screen, and the upper surface of the filter screen is fixedly connected with a hook ring.
In order to enable liquid in the extraction box to flow out, as the efficient separation and extraction device for the progesterone in the red dates, one side face of the extraction box is fixedly connected with a discharge connecting pipe, and the inner wall of the discharge connecting pipe is fixedly connected with an outlet plug.
In order to pour the raw materials into the stirring and crushing barrel, the device for efficiently separating and extracting the progesterone from the red dates is provided, and the upper surface of the top cover is fixedly connected with the feeding hole.
In order to support the stirring and crushing barrel and the extraction box, the device for efficiently separating and extracting progesterone from red dates is provided, wherein the lower surface of the stirring and crushing barrel is fixedly connected with the support column, and the lower surface of the extraction box is fixedly connected with the support leg.
In order to take out the filter screen, the upper surface of the extraction box is fixedly connected with the box door through a hinge as the efficient separation and extraction device for the progesterone in the red dates.
In order to protect the motor, the efficient separation and extraction device for the progesterone in the red dates is characterized in that the lower surface of the stirring and crushing barrel is fixedly connected with a lower protective shell, and the upper surface of the top cover is fixedly connected with an upper protective shell.
Compared with the prior art, the utility model has the following beneficial effects:
1. the device for efficiently separating and extracting progesterone from red dates comprises an installation sleeve, a stirring rod, a crushing sleeve ring, a connecting sleeve and a rotary push plate, wherein the installation sleeve is sleeved on a first rotating shaft inside a stirring and crushing barrel, the stirring rod is welded on the outer surface of the installation sleeve, the crushing sleeve ring is installed on the outer surface of the stirring rod, the connecting sleeve is sleeved on the outer surface of a second rotating shaft inside the stirring and crushing barrel, the rotary push plate is fixed on the surface of the connecting sleeve, when progesterone is extracted from the red dates, the red dates are usually ground into powder firstly, a first servo motor is started to rotate the first rotating shaft when the crushing work is carried out, after the raw materials are put into the stirring and crushing barrel, the stirring rod and the crushing sleeve ring outside the stirring rod are subjected to crushing work, the dry red date raw materials inside are stirred and crushed, and the red dates are prevented from being pushed inside the barrel due to the fact that an internal stirring and crushing device rotates at a high speed, only can be smashed the lantern ring fast and smash, the barrel head portion can be reachd to the red date after smashing, then start second servo motor and make the second pivot rotate, thereby make the outside rotatory push pedal of adapter sleeve begin to work, the red date raw materials after smashing the bottom send into through connecting tube and draw the case, carry out progesterone and draw work on next step in drawing the incasement, thereby make things convenient for follow-up extraction to progesterone, like this can be fast with the raw materials breakage and send out reducing mechanism, and conveniently draw going on of work on next step, just so can draw out progesterone from the red date sooner in follow-up work.
2. The device for efficiently separating and extracting the progesterone from the red dates is characterized in that through the arrangement of an extraction box, a fixed filter screen, a filter screen and a shackle, after the crushed raw materials enter the extraction box through the connecting pipeline, the crushed raw materials fall on the filter screen, the box door is opened to add ethanol solution into the extraction box, the solution is immersed in the crushed raw materials on the filter screen, microwave heating the extraction box by a microwave heating device outside, adopting a microwave heating extraction treatment method, can simplify the process, simplify the process flow, simplify the operation of the process flow, reduce the cost, improve the extraction rate of the red date progesterone, maintain the functional characteristics of the red date progesterone, then hooking the filter screen out through a shackle, taking the extracted crushed red dates out of the extraction box, adding a flocculating agent into the extraction box, can obtain the concentrate that has progesterone, derive the concentrate through ejection of compact connecting pipe again to can be quick extract progesterone from the concentrate.
Drawings
FIG. 1 is a schematic structural diagram of an efficient separation and extraction device for progesterone from red dates in example 1 of the present invention;
FIG. 2 is a schematic sectional view of an orthographic view of an efficient separation and extraction device for progesterone from red dates in example 1 of the present invention;
FIG. 3 is a schematic view of an axial structure of a device for efficiently separating and extracting progesterone from red dates without a top cover according to example 1 of the present invention;
fig. 4 is a schematic axial view of a sectional view of an efficient separation and extraction device for separating progesterone from red dates in embodiment 1 of the present invention;
fig. 5 is a schematic structural diagram of a protective housing in embodiment 2 of the present invention.
In the figure: 1. stirring and crushing the barrel; 2. a top cover; 3. a first servo motor; 4. a first rotating shaft; 5. installing a sleeve; 6. a stirring rod; 7. crushing the lantern ring; 8. a second servo motor; 9. a second rotating shaft; 10. a connecting sleeve; 11. rotating the push plate; 12. connecting a pipeline; 13. an extraction box; 14. fixing the filter screen; 15. a filter screen; 16. a shackle; 17. a discharge connecting pipe; 18. an outlet plug; 19. a feed inlet; 20. a support pillar; 21. supporting legs; 22. a box door; 23. a lower protective housing; 24. and an upper protective housing.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
As shown in fig. 1-4, a high-efficient separation and extraction device of progesterone in red date, including stirring crushing barrel 1, the last fixed surface of stirring crushing barrel 1 is connected with top cap 2, the last fixed surface of top cap 2 is connected with first servo motor 3, the first pivot 4 of the one end fixedly connected with of first servo motor 3, the fixed surface of first pivot 4 is connected with installation cover 5, the fixed surface of installation cover 5 is connected with puddler 6, the fixed surface of puddler 6 is connected with smashes lantern ring 7, the fixed surface of stirring crushing barrel 1 is connected with second servo motor 8, the one end fixedly connected with second pivot 9 of second servo motor 8, the fixed surface of second pivot 9 is connected with connecting sleeve 10, the fixed surface of connecting sleeve 10 is connected with rotatory push pedal 11.
During the specific use, cup joint installation cover 5 on stirring crushing barrel 1 inside first pivot 4, 5 skin weld of installation cover have puddler 6, the skin mounting of puddler 6 has crushing lantern ring 7, 9 skin of second pivot in the stirring crushing barrel 1 has cup jointed connecting sleeve 10, there is rotatory push pedal 11 at connecting sleeve 10 skin fixation, after the raw materials gets into the stirring crushing barrel 1, start first servo motor 3 and make first pivot 4 rotate, then make puddler 6 and its outside crushing lantern ring 7 work, stir crushing the dry red date raw materials of inside, then start second servo motor 8 and make second pivot 9 rotate, thereby make the outside rotatory push pedal 11 of connecting sleeve 10 begin to work, send into the bottom raw materials through connecting tube 12 and draw case 13, thereby conveniently carry out the extraction of progesterone.
In this embodiment, the inner wall of the outer surface of the stirring and pulverizing barrel 1 is fixedly connected with a connecting pipe 12, and one end of the connecting pipe 12 is fixedly connected with an extraction box 13.
During the specific use, connecting tube 12 installs and smashes 1 and draw the case 13 between stirring, conveniently smashes the back raw materials and gets into through connecting tube 12 and draw in the case 13.
In this embodiment, a fixed filter screen 14 is fixedly connected to the inner wall of the extraction box 13, a filter screen 15 is disposed on the upper surface of the fixed filter screen 14, and a hook ring 16 is fixedly connected to the upper surface of the filter screen 15.
In particular, the filter screen 15 is placed on the fixed filter screen 14, and the filter screen 15 can be hooked out of the extraction box 13 by the hook ring 16.
In this embodiment, a discharge connecting pipe 17 is fixedly connected to one side surface of the extraction box 13, and an outlet plug 18 is fixedly connected to the inner wall of the discharge connecting pipe 17.
When the device is used specifically, the outlet plug 18 seals the discharge connecting pipe 17, the outlet plug 18 can be pulled out after extraction work is finished, and the internal solution is led out.
In this embodiment, a feed opening 19 is fixedly connected to the upper surface of the top cover 2.
When in specific use, the feed inlet 19 is fixed at the upper opening of the top cover 2, so that raw materials can enter the stirring and crushing barrel 1 conveniently.
In this embodiment, the lower surface of the stirring and pulverizing barrel 1 is fixedly connected with a support column 20, and the lower surface of the extraction box 13 is fixedly connected with a support leg 21.
When the stirring and crushing device is used specifically, the supporting column 20 is fixed below the stirring and crushing barrel 1 to support the stirring and crushing barrel, and the supporting legs 21 are fixed below the extraction box 13 to support the stirring and crushing barrel.
In the present embodiment, a door 22 is fixedly connected to the upper surface of the extraction box 13 by a hinge.
In particular, the door 22 is mounted on the upper surface of the extraction box 13, so that the additive can be conveniently added into the extraction box during the operation.
The working principle is as follows: the red date crushing device is characterized in that a first rotating shaft 4 in a stirring and crushing barrel 1 is sleeved with an installation sleeve 5, the outer surface of the installation sleeve 5 is welded with a stirring rod 6, the outer surface of the stirring rod 6 is provided with a crushing lantern ring 7, the outer surface of a second rotating shaft 9 in the stirring and crushing barrel 1 is sleeved with a connecting sleeve 10, the surface of the connecting sleeve 10 is fixed with a rotary push plate 11, when progesterone is extracted from red dates, the red dates are usually ground into powder, when crushing is carried out, a first servo motor 3 is started to enable the first rotating shaft 4 to rotate, after the raw materials are placed into the stirring and crushing barrel 1, the stirring rod 6 and the crushing lantern ring 7 outside the stirring rod are then subjected to crushing and stirring work, the dry red date raw materials inside are stirred and crushed, because an internal stirring and crushing device rotates at a high speed, the red dates cannot be pushed inside the barrel, only the crushing lantern ring 7 can be quickly crushed, the crushed red dates can reach the bottom of the barrel, then the second servo motor 8 is started to make the second rotating shaft 9 rotate, so that the rotary push plate 11 outside the connecting sleeve 10 starts to work, the bottom raw material is sent into the extraction box 13 through the connecting pipeline 12, the next step of extraction of the progesterone is carried out in the extraction box 13, so that the extraction of the progesterone is convenient, after the crushed raw material enters the extraction box 13 through the connecting pipeline 12, the crushed raw material falls on the filter screen 15, the box door 22 is opened to add ethanol solution into the extraction box 13, the solution is submerged in the crushed raw material on the filter screen 15, the microwave heating device is used for carrying out microwave heating on the extraction box 13, the microwave heating extraction treatment method is adopted, the process can be simplified, the process flow is simple to operate and low in cost, the extraction rate of the red date progesterone is improved, the functional characteristics of the red date progesterone are retained, and then the filter screen 15 is hooked out through the hook ring 16, thereby take out the extraction case 13 with garrulous red date, then add the flocculating agent, can obtain the concentrate that has progesterone, export the concentrate through ejection of compact connecting pipe 17 again to can be quick extract progesterone.
Example 2
As shown in fig. 5, the distinguishing features of this embodiment that distinguish embodiment 1 are: the lower surface of the stirring and crushing barrel 1 is fixedly connected with a lower protective shell 23, and the upper surface of the top cover 2 is fixedly connected with an upper protective shell 24.
In particular use, the lower protective casing 23 and the upper protective casing 24 are respectively arranged on the outer surfaces of the second servo motor 8 and the first servo motor 3 so as to protect the two.
The foregoing shows and describes the general principles and broad features of the present invention and advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the utility model as claimed. The scope of the utility model is defined by the appended claims and equivalents thereof.
Claims (8)
1. The utility model provides a high-efficient separation and extraction device of progesterone in red date, smashes bucket (1) including the stirring, its characterized in that: the upper surface of the stirring and crushing barrel (1) is fixedly connected with a top cover (2), the upper surface of the top cover (2) is fixedly connected with a first servo motor (3), one end of the first servo motor (3) is fixedly connected with a first rotating shaft (4), the outer surface of the first rotating shaft (4) is fixedly connected with an installation sleeve (5), the outer surface of the installation sleeve (5) is fixedly connected with a stirring rod (6), the outer surface of the stirring rod (6) is fixedly connected with a crushing lantern ring (7), the lower surface of the stirring and crushing barrel (1) is fixedly connected with a second servo motor (8), one end of the second servo motor (8) is fixedly connected with a second rotating shaft (9), the outer surface of the second rotating shaft (9) is fixedly connected with a connecting sleeve (10), the outer surface of the connecting sleeve (10) is fixedly connected with a rotary push plate (11).
2. The efficient separation and extraction device for progesterone in red dates as claimed in claim 1, which is characterized in that: the inner wall fixedly connected with connecting tube (12) of bucket (1) surface is smashed in the stirring, the one end fixedly connected with of connecting tube (12) draws case (13).
3. The efficient separation and extraction device for progesterone in red dates as claimed in claim 2, which is characterized in that: draw inner wall fixedly connected with fixed filter screen (14) of case (13), the upper surface of fixed filter screen (14) is provided with filter screen (15), the last fixed surface of filter screen (15) is connected with shackle (16).
4. The efficient separation and extraction device for progesterone in red dates as claimed in claim 2, which is characterized in that: one side face of the extraction box (13) is fixedly connected with a discharge connecting pipe (17), and the inner wall of the discharge connecting pipe (17) is fixedly connected with an outlet plug (18).
5. The efficient separation and extraction device for progesterone in red dates as claimed in claim 1, which is characterized in that: the upper surface of the top cover (2) is fixedly connected with a feeding hole (19).
6. The efficient separation and extraction device for progesterone in red dates as claimed in claim 2, which is characterized in that: the lower fixed surface of stirring crushing bucket (1) is connected with support column (20), the lower fixed surface who draws case (13) is connected with supporting leg (21).
7. The efficient separation and extraction device for progesterone in red dates as claimed in claim 2, which is characterized in that: the upper surface of the extraction box (13) is fixedly connected with a box door (22) through a hinge.
8. The efficient separation and extraction device for progesterone in red dates as claimed in claim 1, which is characterized in that: the lower fixed surface of stirring crushing bucket (1) is connected with down protecting sheathing (23), the last fixed surface of top cap (2) is connected with protecting sheathing (24).
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| CN202121930427.3U CN216125747U (en) | 2021-08-16 | 2021-08-16 | High-efficient separation and extraction device of progesterone in red date |
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| CN202121930427.3U CN216125747U (en) | 2021-08-16 | 2021-08-16 | High-efficient separation and extraction device of progesterone in red date |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114699798A (en) * | 2022-06-07 | 2022-07-05 | 湖南国华制药有限公司 | Device and method for extracting volatile oil of radix angelicae and angelica sinensis |
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2021
- 2021-08-16 CN CN202121930427.3U patent/CN216125747U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114699798A (en) * | 2022-06-07 | 2022-07-05 | 湖南国华制药有限公司 | Device and method for extracting volatile oil of radix angelicae and angelica sinensis |
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