CN216092990U

CN216092990U - Water knockout drum for organic experiments

Info

Publication number: CN216092990U
Application number: CN202122538085.7U
Authority: CN
Inventors: 李文森
Original assignee: Heading Nanjing Pharmtechnologies Co ltd
Current assignee: Heading Nanjing Pharmtechnologies Co ltd
Priority date: 2021-10-21
Filing date: 2021-10-21
Publication date: 2022-03-22
Anticipated expiration: 2031-10-21

Abstract

The utility model provides a water separator for organic experiments, which belongs to the technical field of organic experimental instruments and comprises a liquid collecting pipe, wherein a communicating pipe is installed at the right lower end of the liquid collecting pipe, a first deflection pipe is integrally connected to the upper end of a steam pipe, the liquid collecting pipe is mutually connected with the communicating pipe, a second deflection pipe and the steam pipe, and the first deflection pipe and the liquid collecting pipe through connecting pieces respectively, a condensation assembly is installed on the outer side of the liquid collecting pipe, and a heat insulation assembly is arranged on the outer side of the steam pipe. The utility model solves the problems that the existing water separator for organic experiments is easy to crack in the experimental process, the whole water separator adopts an integrated structure, the whole water separator needs to be replaced, the use cost is greatly improved, meanwhile, the condensation of a liquid collecting pipe is generally carried out by an external condenser, the use cost of the added instrument is increased, the installation is time-consuming, and the steam pipe cannot preserve heat, so that the corresponding part begins to condense when part of steam does not rise, and the efficiency of the organic experiments is reduced.

Description

Water knockout drum for organic experiments

The technical field is as follows:

the utility model belongs to the technical field of organic experimental instruments, and particularly relates to a water separator for an organic experiment.

Background art:

experiment refers to one of the basic methods of scientific research, which, according to the purpose of scientific research, eliminates the external influence as much as possible, highlights the main factors and artificially reforms, controls or simulates the research object by using some special instruments and equipment, so that some things (or processes) occur or reappear, thereby knowing the natural phenomenon, nature and law. Organic experiments are also common in experiments, and the water separator is a common experimental instrument in the organic experiments.

However, current for the organic experiment water knockout drum experimentation lead to cracked easily, whole water knockout drum adopts the integral type structure, and then leads to needing to change whole water knockout drum, has improved use cost greatly, and the condensation of collecting tube is generally plus the condenser and condenses simultaneously, the use cost of the instrument of increase, the installation is also consuming time to and the steam pipe can't keep warm, and then lead to partial steam to correspond the position when not rising and just begin the condensation, the efficiency of organic experiment has been reduced.

The utility model content is as follows:

the utility model provides a water separator for organic experiments, which aims to solve the problems that the existing water separator for organic experiments is easy to crack in the experimental process, the whole water separator adopts an integrated structure, the whole water separator needs to be replaced, the use cost is greatly improved, meanwhile, the condensation of a liquid collecting pipe is generally carried out by an additional condenser, the use cost of the added instrument is increased, the installation is time-consuming, the steam pipe cannot preserve heat, the condensation of the corresponding part is started when partial steam does not rise, and the efficiency of the organic experiments is reduced.

The embodiment of the utility model provides a water separator for organic experiments, which comprises a liquid collecting pipe, wherein a communicating pipe is installed at the right lower end of the liquid collecting pipe, a second baffling pipe is integrally connected to the upper end of the communicating pipe, a steam pipe is installed at the right end of the second baffling pipe, a first baffling pipe is integrally connected to the upper end of the steam pipe, a floating plate is installed in the liquid collecting pipe, a telescopic rod is installed on the upper end surface of the floating plate, an upper drainage pipe is installed on the left side of the liquid collecting pipe, a lower drainage pipe is installed at the lower end of the liquid collecting pipe, valves are respectively installed on the upper drainage pipe, the lower drainage pipe and the communicating pipe, the liquid collecting pipe, the second baffling pipe, the steam pipe, the first baffling pipe and the liquid collecting pipe are respectively connected with one another through connecting pieces, a condensing assembly is installed on the outer side of the liquid collecting pipe, and a heat preservation assembly is arranged on the outer side of the steam pipe.

Through adopting above-mentioned technical scheme, utilize the connecting piece can carry out the dismouting combination to the water knockout drum, and then after the water knockout drum part damages, can dismantle the change with the part that corresponds the damage, greatly reduced use cost, simultaneously can accelerate the flow velocity of collector tube surface air through the condensation subassembly, and then the speed of the steam condensation in the inflow collector tube has been accelerated, make the water knockout drum from taking condensation structure, not only reduced consuming time of installation, use cost has also been reduced, and the heat preservation subassembly can keep warm to the steam pipe, avoid the thermal excessive loss of steam in the steam pipe to lead to steam not to rise the time correspond the position and just begin the condensation, and then the efficiency of organic experiment has been improved greatly.

Furthermore, the second flow folding pipe and the first flow folding pipe are both arranged towards the steam pipe in an inclined mode.

By adopting the technical scheme, the product generated by the reaction can smoothly and completely flow into the reaction container.

Furthermore, the connecting piece comprises two connecting flanges and four screws I, and the two connecting flanges are in sealing seamless connection through the four screws I.

Through adopting above-mentioned technical scheme, be convenient for carry out the dismouting combination to the water knockout drum through the connecting piece, guarantee can change the partial dismantlement that corresponds when the damage appears in the water knockout drum part, greatly reduced the experiment cost.

Furthermore, the avris of kickboard is provided with the brush, evenly be provided with the through-hole on the kickboard, brush on the kickboard contacts with the inner wall of collector tube.

Through adopting above-mentioned technical scheme, when the kickboard was movable in the collector tube, the brush of usable kickboard avris cleared up the inner wall of collector tube.

Furthermore, the upper liquid discharge pipe is of an L-shaped structure, and a liquid outlet of the upper liquid discharge pipe is arranged downwards.

Through adopting above-mentioned technical scheme, utilize the last drain pipe to discharge the water on upper strata.

Further, the condensation subassembly includes annular pipe, venthole, connecting pipe one, connecting pipe two, connecting pipe three, micro fan and screw two, the annular pipe is provided with five, five the annular pipe evenly installs the outside at the collector tube, the venthole has evenly been seted up on the annular pipe, the venthole sets up towards the collector tube slope, the avris switch-on of annular pipe has connecting pipe one, the connecting pipe two is installed to the one end that the annular pipe was kept away from to connecting pipe one, one side that the annular pipe was kept away from to connecting pipe two is provided with two connecting pipes three, two install micro fan between the connecting pipe three, micro fan and the mutual locking of connecting pipe three screw two.

Through adopting above-mentioned technical scheme, pour into cold air in toward connecting pipe three through micro fan, spout cold air to the collector tube through connecting pipe two, connecting pipe one, ring pipe and venthole on, and then realize the rapid condensation to the intraductal steam of collector tube for the water knockout drum is from taking the condensation structure, has not only reduced consuming time of installation, has also reduced use cost.

Further, the heat preservation assembly adopts a heat preservation sleeve.

Through adopting above-mentioned technical scheme, the insulation cover can keep warm to the steam pipe, avoids the steam pipe in the steam pipe too fast the loss lead to steam not to rise the time correspond the position just begin the condensation, and then improved the efficiency of organic experiment greatly.

The utility model has the beneficial effects that:

1. according to the utility model, through the arrangement of the connecting piece, the water distributor can be disassembled and assembled by using the connecting piece, and further, after the water distributor is partially damaged, the corresponding damaged part can be disassembled and replaced, so that the use cost is greatly reduced.

2. According to the utility model, through the arrangement of the condensation component, the flow speed of air on the surface of the liquid collecting pipe can be accelerated by the condensation component, so that the condensation speed of steam flowing into the liquid collecting pipe is accelerated, the water separator is provided with a condensation structure, the time consumption in the installation process is reduced, and the use cost is also reduced.

3. According to the utility model, through the arrangement of the heat insulation component, the heat insulation component can insulate the heat of the steam pipe, so that the phenomenon that the corresponding part begins to be condensed when the steam does not rise due to the too fast loss of the heat of the steam in the steam pipe is avoided, and the efficiency of an organic experiment is greatly improved.

Additional features and advantages of the utility model will be set forth in the description which follows, and in part will be obvious from the description, or may be learned by practice of the utility model. The objectives and other advantages of the utility model may be realized and attained by the structure particularly pointed out in the written description and drawings.

Description of the drawings:

the accompanying drawings, which are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate embodiments of the utility model and together with the description serve to explain the principles of the utility model and not to limit the utility model. In the drawings:

FIG. 1 is a schematic overall structure diagram of an embodiment of the present invention;

FIG. 2 is a schematic front view of an embodiment of the present invention;

FIG. 3 is a schematic main sectional view of an embodiment of the present invention;

FIG. 4 is an enlarged schematic view of a portion of FIG. 3 according to an embodiment of the present invention;

reference numerals: 1. a liquid collecting pipe; 2. a communicating pipe; 3. a second baffling pipe; 4. a steam pipe; 5. a first baffling pipe; 6. a connecting member; 7. a floating plate; 8. a telescopic rod; 9. an upper drainage pipe; 10. a lower drain pipe; 11. a valve; 12. a condensing assembly; 13. a heat preservation assembly; 61. a connecting flange; 62. a first screw; 121. an annular tube; 122. an air outlet; 123. a first connecting pipe; 124. a second connecting pipe; 125. a third connecting pipe; 126. a micro fan; 127. and a second screw.

The specific implementation mode is as follows:

in order to make the objects, technical solutions and advantages of the technical solutions of the present invention clearer, the technical solutions of the embodiments of the present invention will be clearly and completely described below with reference to the drawings of the specific embodiments of the present invention. Like reference symbols in the various drawings indicate like elements. It should be noted that the described embodiments are only some embodiments of the utility model, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the utility model without any inventive step, are within the scope of protection of the utility model.

Referring to fig. 1, 2 and 3, the embodiment of the utility model provides a water separator for organic experiments, which comprises a liquid collecting pipe 1, a communicating pipe 2 is arranged at the right lower end of the liquid collecting pipe 1, a baffling pipe two 3 is integrally connected to the upper end of the communicating pipe 2, a steam pipe 4 is arranged at the right end of the baffling pipe two 3, a baffling pipe one 5 is integrally connected to the upper end of the steam pipe 4, the baffling pipe two 3 and the baffling pipe one 5 are obliquely arranged towards the steam pipe 4, so that a product generated by reaction can smoothly and completely flow into a reaction container, a floating plate 7 is arranged in the liquid collecting pipe 1, a brush is arranged at the side of the floating plate 7, through holes are uniformly arranged on the floating plate 7, the brush on the floating plate 7 is in contact with the inner wall of the liquid collecting pipe 1, when the floating plate 7 moves in the liquid collecting pipe 1, the inner wall of the liquid collecting pipe 1 can be cleaned by the brush at the side of the floating plate 7, a telescopic rod 8 is arranged on the upper end surface of the floating plate 7, upper liquid discharge pipe 9 is installed in the left side of collector pipe 1, upper liquid discharge pipe 9 is L font structure, the liquid outlet of upper liquid discharge pipe 9 sets up down, utilize upper liquid discharge pipe 9 to discharge the water on upper strata, lower liquid discharge pipe 10 is installed to the lower extreme of collector pipe 1, upper liquid discharge pipe 9, respectively install a valve 11 on lower liquid discharge pipe 10 and the communicating pipe 2, collector pipe 1 and communicating pipe 2, second 3 and steam pipe 4 of baffling pipe, baffling pipe 5 is respectively through connecting piece 6 interconnect with collector pipe 1, connecting piece 6 includes two flange 61 and four screws 62, two flange 61 are through the sealed seamless connection of four screws 62, be convenient for carry out the dismouting combination to the hydrophone through connecting piece 6, guarantee can dismantle the part that corresponds when the damage appears in the water knockout drum part and change, greatly reduced the experimental cost.

Referring to fig. 1, 2, 3 and 4, a condensing assembly 12 is installed on the outer side of a liquid collecting pipe 1, the condensing assembly 12 includes five annular pipes 121, air outlet holes 122, a first connecting pipe 123, a second connecting pipe 124, a third connecting pipe 125, a second micro-fan 126 and a second screw 127, the five annular pipes 121 are evenly installed on the outer side of the liquid collecting pipe 1, the air outlet holes 122 are evenly opened on the annular pipes 121, the air outlet holes 122 are obliquely arranged towards the liquid collecting pipe 1, the first connecting pipe 123 is communicated with the side of the annular pipe 121, the second connecting pipe 124 is installed at one end of the first connecting pipe 123 far away from the annular pipe 121, the third connecting pipe 125 is installed at one side of the second connecting pipe 124 far away from the annular pipe 121, the micro-fan 126 is installed between the third connecting pipes 125, the micro-fan 126 and the third connecting pipes 125 are mutually locked through the second screw 127, and cold air is injected into the third connecting pipes 125 through the micro-fan 126, through connecting pipe two 124, connecting pipe 123, ring pipe 121 and venthole 122 with the cold gas spout the collector tube 1 on, and then realize the rapid condensation to steam in the collector tube 1 for the water knockout drum is from taking the condensation structure, has not only reduced consuming time of installation, has also reduced use cost.

Referring to fig. 1, 2 and 3, the outside of steam pipe 4 is provided with heat preservation subassembly 13, and heat preservation subassembly 13 adopts the insulation cover, and the insulation cover can keep warm to the steam pipe, avoids the too fast loss of steam heat in the steam pipe to lead to steam not to rise the time corresponding position just begin the condensation, and then has improved the efficiency of organic experiment greatly.

The implementation mode is specifically as follows: when the device is used, the water separator is fixed by the fixing device, the water separator is positioned above the reaction container, the opening of the liquid collecting pipe 1 is sealed by the plug, the lower end of the steam pipe 4 is communicated with the reaction container, in the experimental process, the power supply of the condensation component 12 is communicated, the micro fan 126 injects cold air into the connecting pipe III 125, the cold air is sprayed onto the liquid collecting pipe 1 through the connecting pipe II 124, the connecting pipe I123, the annular pipe 121 and the air outlet 122, so that the steam in the liquid collecting pipe 1 is rapidly condensed, the liquid collecting pipe 1 can separate water and organic liquid in the condensate, meanwhile, the heat insulation component 13 on the steam pipe 4 can insulate the steam pipe 4, the phenomenon that the corresponding part begins to be condensed when the steam does not rise due to the too rapid loss of the heat of the steam in the steam pipe 4 is avoided, the efficiency of an organic experiment is greatly improved, and after the experiment is finished, the water separator is detached and cleaned, when the water distributor part is damaged, the first screw 62 on the connecting piece 6 of the corresponding part can be screwed out, the corresponding damaged part is disassembled, the replaced new part is arranged at the appointed position, and the corresponding connecting flange 61 is locked through the first screw 62, so that the damaged part of the water distributor is replaced, and the experiment cost is greatly reduced.

The foregoing shows and describes the general principles and broad features of the present invention and advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the utility model as claimed. The scope of the utility model is defined by the appended claims and equivalents thereof.

Claims

1. The utility model provides a water knockout drum for organic experiments, includes collector tube (1), communicating pipe (2) are installed to the right lower extreme of collector tube (1), the upper end integral type of communicating pipe (2) is connected with baffling pipe two (3), steam pipe (4) are installed to the right-hand member of baffling pipe two (3), the upper end integral type of steam pipe (4) is connected with baffling pipe one (5), install kickboard (7) in collector tube (1), telescopic link (8) are installed to the up end of kickboard (7), last drain pipe (9) are installed in the left side of collector tube (1), lower drain pipe (10) are installed to the lower extreme of collector tube (1), respectively install a valve (11) on last drain pipe (9), lower drain pipe (10) and communicating pipe (2), its characterized in that, collector tube (1) and communicating pipe (2) respectively, The baffling pipe II (3) and the steam pipe (4), the baffling pipe I (5) and the liquid collecting pipe (1) are connected with each other through a connecting piece (6) respectively, a condensation component (12) is installed on the outer side of the liquid collecting pipe (1), and a heat insulation component (13) is arranged on the outer side of the steam pipe (4).

2. The water separator for organic experiments according to claim 1, wherein: the second baffling pipe (3) and the first baffling pipe (5) are both arranged towards the steam pipe (4) in an inclined mode.

3. The water separator for organic experiments according to claim 1, wherein: the connecting piece (6) comprises two connecting flanges (61) and four screws I (62), and the two connecting flanges (61) are in sealed seamless connection through the four screws I (62).

4. The water separator for organic experiments according to claim 1, wherein: the avris of kickboard (7) is provided with the brush, evenly be provided with the through-hole on kickboard (7), the brush on kickboard (7) contacts with the inner wall of collector tube (1).

5. The water separator for organic experiments according to claim 1, wherein: the upper liquid discharge pipe (9) is of an L-shaped structure, and a liquid outlet of the upper liquid discharge pipe (9) is arranged downwards.

6. The water separator for organic experiments according to claim 1, wherein: the condensation component (12) comprises an annular pipe (121), an air outlet hole (122), a first connecting pipe (123), a second connecting pipe (124), a third connecting pipe (125), a micro fan (126) and a second screw (127), five annular pipes (121) are arranged, the five annular pipes (121) are uniformly arranged on the outer side of the liquid collecting pipe (1), the annular pipe (121) is uniformly provided with air outlet holes (122), the air outlet holes (122) are obliquely arranged towards the liquid collecting pipe (1), the side of the annular pipe (121) is communicated with a first connecting pipe (123), one end of the first connecting pipe (123) far away from the annular pipe (121) is provided with a second connecting pipe (124), one side of the second connecting pipe (124) far away from the annular pipe (121) is provided with two third connecting pipes (125), a micro-fan (126) is arranged between the two third connecting pipes (125), the micro fan (126) and the connecting pipe III (125) are mutually locked through a screw II (127).

7. The water separator for organic experiments according to claim 1, wherein: the heat insulation component (13) adopts a heat insulation sleeve.