CN215877983U

CN215877983U - Saturated absorption reaction vessel

Info

Publication number: CN215877983U
Application number: CN202121320011.XU
Authority: CN
Inventors: 陈力群; 裴征
Original assignee: Pucheng Yuteng New Material Technology Co ltd
Current assignee: Pucheng Yuteng New Material Technology Co ltd
Priority date: 2021-06-11
Filing date: 2021-06-11
Publication date: 2022-02-22
Anticipated expiration: 2031-06-11

Abstract

A saturated absorption reaction vessel comprises a reaction bottle body, a filler column and an absorption column; the reaction bottle body is a double-layer bottle body, and the filler column and the absorption columns are arranged above the reaction bottle body and are communicated with the inner-layer bottle body of the reaction bottle body. The utility model can be suitable for detecting the saturated adsorption quantity of the product in the environmental chemical industry. The gas generation and adsorption integration of the utility model can effectively reduce the gas leakage, and the design of multiple absorption columns can effectively improve the quality inspection efficiency.

Description

Saturated absorption reaction vessel

Technical Field

The utility model belongs to the field of chemical experimental articles, and particularly relates to a saturated absorption reaction vessel.

Background

At present, in the environment, the chemical industry generally needs to treat pollutants, adsorption removal is the mainstream of a waste gas treatment method, various adsorption products or chemical adsorption or physical adsorption can produce excellent adsorption removal effect, however, the adsorption capacity of the product has a limit, so that the unit adsorption capacity becomes a key index for judging the product quality.

However, the saturated adsorption test is often assembled by various experimental devices due to lack of integrated special experimental instruments, and is complicated and inconvenient in detection of a large amount of samples, and the experimental process is complicated and tedious. The experimental tools are continuously replaced according to different experimental requirements; the repeated assembling and disassembling of the front and the back experimental devices for each detection has potential safety hazards of gas leakage, meanwhile, the experimental efficiency is greatly reduced, the high-efficiency, quick and accurate obtaining of required data is not facilitated, and the sample quality is judged.

Disclosure of Invention

The present invention is directed to a saturable absorption reactor vessel to solve the above problems.

In order to achieve the purpose, the utility model adopts the following technical scheme:

a saturated absorption reaction vessel comprises a reaction bottle body, a filler column and an absorption column; the reaction bottle body is a double-layer bottle body, and the filler column and the absorption columns are arranged above the reaction bottle body and are communicated with the inner-layer bottle body of the reaction bottle body.

Furthermore, the number of the absorption columns is six, and the absorption columns are respectively arranged on two sides of the packed column.

Further, the lower end of the packed column extends to the inside of the reaction flask body.

Furthermore, circulating liquid interfaces are arranged on two sides of an interlayer outside the reaction bottle body.

Furthermore, the inner bottom of the absorption column is provided with a pressing sheet, the two surfaces of the pressing sheet are both porous glass plates, the side surface is open, and a cavity is arranged in the pressing sheet.

Furthermore, the filler column port and the absorption column port have the same specification and are provided with plungers or tail connecting pipes.

Further, the thickness of the tablet is more than or equal to one centimeter.

Further, the reaction bottle body is a spherical bottle body.

Compared with the prior art, the utility model has the following technical effects:

the utility model can introduce various media with temperature control function according to the requirement; the porous glass plate at the bottom of the absorption column and the container are integrally formed, and the gas passing is not influenced by the pores; the pressing sheet is independent from the main body, and both sides of the pressing sheet are porous glass plates, the side surfaces of the pressing sheet are open, and cavities are arranged in the pressing sheet; the filler column mouth and the absorption column mouth have the same specification, the filler column mouth and the absorption column mouth can be commonly used for a tail connecting pipe and a plunger, and after the plunger is inserted, water can be added into the annular extension of the connecting part for liquid sealing.

The using principle of the absorption columns is from inside to outside, the unused absorption columns are sealed by using plungers, when the six absorption columns are used completely, only the absorption columns on two sides are connected with the tail connecting pipe, and the other four absorption columns inside are sealed by using the plungers, so that the sample in each absorption column can be contacted with sufficient gas to be detected.

The utility model can be suitable for detecting the saturated adsorption quantity of the product in the environmental chemical industry. The gas generation and adsorption integration of the utility model can effectively reduce the gas leakage, and the design of multiple absorption columns can effectively improve the quality inspection efficiency.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a diagram of the construction of a tablet of the present invention;

FIG. 3 is a schematic view of the plunger of the present invention;

FIG. 4 is a structural view of the tailpipe of the present invention.

1-reaction bottle body 2-circulating liquid interface 3-porous glass plate 4-absorption column 5-filling column

6- -pressing sheet 7- -plunger 8- -tail connecting pipe

Detailed Description

The utility model is further described below with reference to the accompanying drawings:

referring to fig. 1 to 4 of the drawings,

a saturated absorption reaction vessel comprises a reaction bottle body, a filler column and an absorption column; the reaction bottle body is a double-layer bottle body, and the filler column and the absorption columns are arranged above the reaction bottle body and are communicated with the inner-layer bottle body of the reaction bottle body. Various media with temperature control function can be introduced according to the requirement; the porous glass plate at the bottom of the absorption column and the container are integrally formed, and the gas passing is not influenced by the pores; the pressing sheet is independent from the main body, and both sides of the pressing sheet are porous glass plates, the side surfaces of the pressing sheet are open, and cavities are arranged in the pressing sheet; the filler column mouth and the absorption column mouth have the same specification, the filler column mouth and the absorption column mouth can be commonly used for a tail connecting pipe and a plunger, and after the plunger is inserted, water can be added into the annular extension of the connecting part for liquid sealing.

The inner bottom of the absorption column is provided with a pressing sheet, the two surfaces of the pressing sheet are both porous glass plates, the side surfaces of the pressing sheet are open, and a cavity is arranged in the pressing sheet.

The specifications of the filler column port and the absorption column port are consistent, and a plunger or a tail connecting pipe is arranged.

The thickness of the pressed sheet is more than or equal to one centimeter.

The reaction bottle body is a spherical bottle body.

When the sulfur capacity content of the desulfurizer is detected, a three-neck flask, a condenser pipe, a water bath kettle and the like are needed for assembling the experimental device, the assembly is time-consuming, and each set of device can only detect a single sample.

The utility model is used, only enough reactant is added into the packed column, cooling water is introduced, the plunger is plugged, the sample is placed in the absorption column, the tabletting is filled up and down, the tail gas is guided into the absorption liquid by the upper tail connecting pipe, the utility model is fast and safe, at most six samples can be detected simultaneously, and the efficiency is greatly improved.

When carrying out the saturation adsorption capacity of molecular sieve, equipment experimental apparatus needs beaker, packed column, three-neck flask etc. and the equipment is time-consuming and each set of device can only detect single sample, and the complicated gas composition proportion that each set of device produced also is difficult to hold, causes the difference between the different group's experiments.

The utility model is used, only enough reactant is added into the packed column, cooling water is introduced, the plunger is plugged, the sample is placed in the absorption column, the tabletting is filled up and down, the tail gas is guided into the absorption liquid by the upper tail connecting pipe, the generated gas components are uniform, different products are placed under the same condition, the result is more accurate and reliable, the detection is rapid and safe, at most, six samples can be detected simultaneously, and the efficiency is greatly improved.

Claims

1. A saturated absorption reaction vessel is characterized by comprising a reaction bottle body (1), a filler column (5) and an absorption column (4); the reaction bottle body (1) is a double-layer bottle body, and the filler column (5) and the absorption columns (4) are arranged above the reaction bottle body (1) and are communicated with the inner-layer bottle body of the reaction bottle body (1).

2. A saturable absorption reactor vessel as claimed in claim 1, wherein the number of the absorption columns (4) is six, and the six are respectively disposed at both sides of the packed column (5).

3. A saturable absorption reactor vessel as claimed in claim 1, wherein the lower end of the packed column (5) extends to the inside of the reaction vessel body (1).

4. A saturable absorption reactor vessel as claimed in claim 1, wherein the reaction flask (1) has circulating liquid ports (2) on both sides of the outer sandwich layer.

5. A saturable absorption reactor vessel as claimed in claim 1, wherein the absorption column (4) is provided with a pressing sheet (6) at the inner bottom, and the pressing sheet (6) has porous glass plates on both sides, open side and hollow cavity therein.

6. A saturable absorption reactor vessel as claimed in claim 1, wherein the packing port and the absorption port are in conformity with specification and are provided with a plunger (7) or a tail pipe (8).

7. A saturable absorption reactor vessel as claimed in claim 5, wherein the thickness of the compressed sheet (6) is one centimeter or more.

8. A saturable absorption reactor vessel as claimed in claim 1, wherein the reaction flask (1) is a spherical flask.