CN215743453U - Reaction kettle system - Google Patents
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- CN215743453U CN215743453U CN202122358763.1U CN202122358763U CN215743453U CN 215743453 U CN215743453 U CN 215743453U CN 202122358763 U CN202122358763 U CN 202122358763U CN 215743453 U CN215743453 U CN 215743453U
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Abstract
The utility model relates to the technical field of pharmacy, in particular to a reaction kettle system. The reaction kettle system comprises a synthesis reaction kettle and a post-treatment reaction kettle. Wherein, synthetic reation kettle is used for stirring multiple raw and other materials and mixes formation reaction liquid, aftertreatment reation kettle and synthetic reation kettle pass through first pneumatic valve intercommunication, and aftertreatment reation kettle and first vacuum valve intercommunication, first vacuum valve one end can communicate with aftertreatment reation kettle, the other end communicates with vacuum generating device, make aftertreatment reation kettle can be through control and synthetic reation kettle's pressure differential with the reaction liquid drainage to aftertreatment reation kettle in, aftertreatment reation kettle can be for carrying out the aftertreatment to the reaction liquid in order to obtain final product. This reation kettle system is through transferring reaction liquid through pressure difference between synthetic reation kettle and the aftertreatment reation kettle, avoids the artifical transfer of operator to alleviate operator intensity of labour, and automatic transfer process is favorable to improving experimental efficiency.
Description
Technical Field
The utility model relates to the technical field of pharmacy, in particular to a reaction kettle system.
Background
With the progress of science and technology, the requirements of people on the automatic experiment of a pharmaceutical laboratory are increasingly improved, so that the purposes of reducing the labor intensity and improving the test efficiency are achieved.
In the prior art, in the process of drug preparation experiments, after various raw materials are reacted in a synthesis reaction kettle, the reaction solution needs to be transferred by manpower and then subjected to aftertreatment, so that the problems of low experimental efficiency and easy fatigue of operators are caused.
In order to solve the above problems, it is desirable to provide a reaction kettle system.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a reaction kettle system to achieve the effects of improving the experimental efficiency and reducing the labor intensity of operators.
In order to achieve the purpose, the utility model adopts the following technical scheme:
a reactor system, comprising:
the synthesis reaction kettle is configured to stir and mix a plurality of raw materials to form reaction liquid; and
aftertreatment reation kettle, with synthetic reation kettle passes through a pneumatic valve intercommunication, just aftertreatment reation kettle and first vacuum valve intercommunication, first vacuum valve one end can with aftertreatment reation kettle intercommunication, the other end and vacuum generating device intercommunication make aftertreatment reation kettle can through control with synthetic reation kettle's pressure differential will the reaction liquid drainage extremely in the aftertreatment reation kettle, aftertreatment reation kettle is configured as right the reaction liquid carries out the aftertreatment in order to obtain final product.
As a preferred embodiment, the synthesis reaction kettle comprises:
the first reaction kettle body is configured to contain the raw materials, and is provided with a first opening;
the output end of the first stirring component can extend into the first reaction kettle body so as to stir the raw materials; and
a first cover covering the first opening, the first cover configured to isolate the first reactor body from an external environment.
As a preferable scheme, the synthesis reaction kettle further comprises:
the output end of the temperature monitoring assembly can penetrate through the first cover body and extend into the first reaction kettle body.
As a preferred embodiment, the reactor system further comprises:
the heat-preserving container, first reation kettle body can be placed so that in the heat-preserving container first reation kettle body can be in the ultra-low temperature state.
As a preferred embodiment, the post-treatment reaction kettle comprises:
a second reaction vessel body configured to accommodate the reaction liquid transferred from the synthesis reaction vessel;
the output end of the second stirring component can extend into the second reaction kettle body so as to stir the reaction liquid; and
a second cover configured to isolate the second reaction vessel body from an external environment.
As a preferred embodiment, the reactor system further comprises:
an automatic filling mechanism configured to periodically and quantitatively fill the raw material into the synthesis reaction kettle.
As a preferred embodiment, the reactor system further comprises:
and the condensation liquid-separating component can be communicated with the synthesis reaction kettle and is configured to condense and separate the evaporated steam in the synthesis reaction kettle.
As a preferred scheme, the condensation liquid separation component comprises:
the liquid separator can be communicated with the synthesis reaction kettle;
the condensation pipe is communicated with the liquid separator and is arranged above the liquid separator, and the condensation pipe is configured to cool and condense the evaporated gas in the synthesis reaction kettle; and
and the collecting bottle is communicated with the liquid distributor and is arranged below the liquid distributor.
As a preferred scheme, the condensation liquid separation component further comprises:
and one end of the second vacuum valve can be communicated with the condensation liquid-separating component, and the other end of the second vacuum valve is communicated with the vacuum generating device.
As a preferred embodiment, the reactor system further comprises:
and the support frame body is configured to fix the synthesis reaction kettle, the post-treatment reaction kettle and the condensation liquid-separating component.
The utility model has the beneficial effects that:
the utility model discloses a reaction kettle system which comprises a synthesis reaction kettle and a post-treatment reaction kettle. Wherein, synthetic reation kettle is used for stirring multiple raw and other materials and mixes formation reaction liquid, aftertreatment reation kettle and synthetic reation kettle pass through first pneumatic valve intercommunication, and aftertreatment reation kettle and first vacuum valve intercommunication, first vacuum valve one end can communicate with aftertreatment reation kettle, the other end communicates with vacuum generating device, make aftertreatment reation kettle can be through control and synthetic reation kettle's pressure differential with the reaction liquid drainage to aftertreatment reation kettle in, aftertreatment reation kettle can be for carrying out the aftertreatment to the reaction liquid in order to obtain final product. This reation kettle system is through transferring reaction liquid through pressure difference between synthetic reation kettle and the aftertreatment reation kettle, avoids the artifical transfer of operator to alleviate operator intensity of labour, and automatic transfer process is favorable to improving experimental efficiency.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings used in the description of the embodiments of the present invention will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the contents of the embodiments of the present invention and the drawings without creative efforts.
FIG. 1 is a schematic structural diagram of a reactor system according to an embodiment of the present invention;
FIG. 2 is a schematic structural diagram of a reactor system according to a second embodiment of the present invention.
The figures are labeled as follows:
100-a synthesis reaction kettle; 110-a first reaction kettle body; 120-a first stirring assembly; 121-a first stirring drive; 122-a first stirring shaft; 123-a first blade; 130-a first cover; 140-a temperature monitoring assembly;
200-post-treatment reaction kettle; 210-a second reaction kettle body; 220-a second stirring assembly; 221-a second stirring drive; 222-a second stirring shaft; 223-a second blade; 230-a second cover;
300-a first pneumatic valve;
400-a first vacuum valve;
500-condensation liquid separation component; 510-a liquid distributor; 520-a condenser tube; 530-a collection bottle; 540-a second vacuum valve;
600-a heat-preserving barrel;
700-temperature control mechanism;
800-automatic filling mechanism.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings and examples. It is to be understood that the specific embodiments described herein are merely illustrative of the utility model and are not limiting of the utility model. It should be further noted that, for the convenience of description, only the structures related to the present invention are shown in the drawings, not the entire structures.
In the description of the present invention, unless expressly stated or limited otherwise, the terms "connected," "connected," and "fixed" are to be construed broadly, e.g., as meaning permanently connected, removably connected, or integral to one another; can be mechanically or electrically connected; they may be directly connected or indirectly connected through intervening media, or may be structurally related or interoperable between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
In the present invention, unless otherwise expressly stated or limited, "above" or "below" a first feature means that the first and second features are in direct contact, or that the first and second features are not in direct contact but are in contact with each other via another feature therebetween. Also, the first feature being "on," "above" and "over" the second feature includes the first feature being directly on and obliquely above the second feature, or merely indicating that the first feature is at a higher level than the second feature. A first feature being "under," "below," and "beneath" a second feature includes the first feature being directly under and obliquely below the second feature, or simply meaning that the first feature is at a lesser elevation than the second feature.
In the description of the present embodiment, the terms "upper", "lower", "left", "right", and the like are used based on the orientations and positional relationships shown in the drawings only for convenience of description and simplification of operation, and do not indicate or imply that the referred device or element must have a specific orientation, be configured and operated in a specific orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used only for descriptive purposes and are not intended to have a special meaning.
Example one
With the progress of science and technology, the requirements of people on the automatic experiment of a pharmaceutical laboratory are increasingly improved, so that the purposes of reducing the labor intensity and improving the test efficiency are achieved.
In the prior art, in the process of drug preparation experiments, after various raw materials are reacted in the synthesis reaction kettle 100, the reaction solution needs to be transferred by manpower and then post-treated, so that the problems of low experimental efficiency and easy fatigue of operators are caused.
To solve the above problem, as shown in fig. 1, the present embodiment provides a reaction kettle system, which includes a synthesis reaction kettle 100 and a post-treatment reaction kettle 200. Wherein, synthetic reation kettle 100 is used for stirring multiple raw and other materials and mixes formation reaction liquid, aftertreatment reation kettle 200 communicates through first pneumatic valve 300 with synthetic reation kettle 100, and aftertreatment reation kettle 200 and first vacuum valve 400 intercommunication, first vacuum valve 400 one end can communicate with aftertreatment reation kettle 200, the other end communicates with vacuum generating device, make aftertreatment reation kettle 200 can be through control and synthetic reation kettle 100 pressure differential with reaction liquid drainage to aftertreatment reation kettle 200 in, aftertreatment reation kettle 200 can be for carrying out the aftertreatment to the reaction liquid in order to obtain final product. This reation kettle system passes through between synthetic reation kettle 100 and the aftertreatment reation kettle 200 through pressure differential transfer reaction liquid, avoids the manual work of operator to shift to alleviate operator intensity of labour, and automatic transfer process is favorable to improving experimental efficiency.
In order to improve the automation degree of the reaction kettle system and further improve the experimental efficiency of the reaction kettle system, the reaction kettle system further comprises a controller, and the controller can be electrically connected with the first pneumatic valve 300 and the first vacuum valve 400, so that the controller can control the opening and closing of the first pneumatic valve 300 and the first vacuum valve 400. Meanwhile, the controller can control the vacuum strength of the first vacuum valve 400, thereby controlling the amount of the transfer reaction liquid between the synthesis reaction kettle 100 and the post-treatment reaction kettle 200, and the like.
Further, as shown in fig. 1, the reaction kettle system further includes an automatic feeding mechanism 800, and the automatic feeding mechanism 800 can regularly and quantitatively feed the raw material into the synthesis reaction kettle 100, so as to improve the automation degree of the reaction kettle system, improve the precision of feeding the raw material, and improve the success probability and precision of the experiment.
Referring now to fig. 1, the detailed structure of the synthesis reactor 100 will be described.
As shown in fig. 1, the synthesis reaction kettle 100 includes a first reaction kettle body 110, and the first reaction kettle body 110 is used for accommodating raw materials and providing a reaction environment for the raw materials. Synthetic reation kettle 100 still includes first lid 130, first opening has been seted up to first reation kettle body 110, first lid 130 covers on first opening, first lid 130 can keep apart first reation kettle body 110 with external environment, make the interior confined reaction space that forms of first reation kettle, avoid gas such as oxygen in first reation kettle body 110 air to participate in the chemical reaction of raw and other materials, be favorable to guaranteeing that the chemical reaction in first reation kettle body 110 can be according to the raw and other materials composition control that the operator provided, thereby be favorable to improving the precision of experiment.
In order to improve the experimental efficiency of the reaction kettle system, the reaction kettle system further comprises a feeding assembly, and the feeding assembly is used for providing required raw materials for the first reaction kettle body 110. Particularly, be provided with a plurality of feedholes on the first lid 130, the feeding unit is connected with every feedhole respectively with the composition according to the nature of feed, and simultaneously, the feeding unit can be connected with the controller electricity, makes the controller can control feeding unit feed quantity to guarantee the feed precision, further improve reation kettle system's experiment precision.
Illustratively, since the solid raw material particles have a large diameter, in order to make the raw material supply smooth, the feedwell for supplying the solid raw material is preferably 100mm in diameter. The diameter of the feed port for supplying the liquid raw material is preferably 25mm, and the 25mm diameter enables smooth circulation of the liquid raw material and uniform flow rate.
With reference to fig. 1, the synthesis reactor 100 further includes a first stirring component 120, an output end of the first stirring component 120 can extend into the first reactor body 110 to stir the raw materials, so that the raw materials can be fully mixed and chemically reacted in the first reactor body 110, thereby facilitating the full reaction of the raw materials and avoiding the phenomenon that part of the raw materials cannot participate in the reaction due to the non-uniform raw materials.
Specifically, as shown in fig. 1, the first stirring assembly 120 includes a first stirring driver 121, a first stirring shaft 122, and a first blade 123. The output end of the first stirring driving member 121 is connected to the first stirring shaft 122, the first stirring driving member 121 is electrically connected to the controller, the first stirring shaft 122 passes through the first cover 130 and extends into the first reaction kettle body 110, and the first blade 123 is disposed on the first stirring shaft 122. This embodiment enables the controller to control the start or stop of the first stirring drive member 121, thereby avoiding manual operation. The first stirring driving member 121 can drive the first stirring shaft 122 to rotate, and drive the first blade 123 to rotate in the raw material, thereby realizing the stirring of the raw material. Illustratively, the first agitation drive 121 is preferably a blender, which is of conventional construction, readily available and inexpensive to purchase.
More preferably, when the synthesis reaction kettle 100 needs to perform a chemical reaction at an extremely low temperature, the synthesis reaction kettle 100 may be further provided with a heat-preserving container 600, and the first reaction kettle body 110 is placed in the heat-preserving container 600, so that the first reaction kettle body 110 can be in an ultra-low temperature state. Specifically, the heat-preserving container 600 is preferably a liquid nitrogen heat-preserving container 600, so that the synthesis reaction kettle 100 can be in a low-temperature state for reaction, thereby meeting the requirements of a special reaction environment and being beneficial to improving the application range of the reaction kettle system.
In some chemical reactions, the temperature is a condition factor of the chemical reaction, and therefore, the synthesis reaction kettle 100 further includes a temperature monitoring component 140, and an output end of the temperature monitoring component 140 can penetrate through the first cover 130 and extend into the first reaction kettle body 110, so as to achieve the purpose of monitoring the reaction temperature in the first reaction kettle body 110. An operator can set the monitoring temperature range of the temperature monitoring component 140, namely the preset minimum temperature and the preset maximum temperature, according to the temperature requirements of different experiments, and when the temperature monitoring component 140 monitors that the temperature in the first reaction kettle body 110 is higher than the maximum temperature or lower than the minimum temperature, the controller can give an alarm.
The detailed structure of the post-treatment reactor 200 will now be described with reference to fig. 1.
As shown in fig. 1, the post-treatment reaction tank 200 includes a second reaction tank body 210, and the second reaction tank body 210 is used for accommodating the reaction liquid transferred from the synthesis reaction tank 100, so that the reaction liquid can be post-treated in the second reaction tank body 210. Aftertreatment reation kettle 200 still includes second lid 230, second lid 230 can keep apart second reation kettle body 210 and external environment, the second opening has been seted up to second reation kettle body 210, second lid 230 covers on the second opening, second lid 230 can keep apart second reation kettle body 210 and external environment, make the formation of confined reaction space in the second reation kettle, avoid gas such as oxygen in the second reation kettle air to participate in the aftertreatment reaction of reaction solution, be favorable to guaranteeing that the chemical reaction in second reation kettle body 210 can go on under operator's control, thereby be favorable to improving the precision of experiment.
Further, with continued reference to fig. 1, the post-treatment reactor 200 further includes a second stirring assembly 220. The output of second stirring subassembly 220 can extend to in the second reation kettle body 210 to stirring reaction liquid, thereby make reaction liquid can intensive mixing and carry out the aftertreatment in second reation kettle body 210, thereby be favorable to reaction liquid can the intensive reaction, avoid leading to partial reaction liquid can not participate in the reaction because reaction liquid is inhomogeneous.
Specifically, as shown in fig. 1, the second stirring assembly 220 includes a second stirring driving member 221, a second stirring shaft 222, and second blades 223. Wherein, the output end of the second stirring driving member 221 is connected to the second stirring shaft 222, and the second stirring driving member 221 is electrically connected to the controller, the second stirring shaft 222 passes through the second cover 230 and extends into the second reaction kettle body 210, and the second blades 223 are disposed on the second stirring shaft 222. This embodiment enables the controller to control the start or stop of the second stirring drive 221, thereby avoiding manual operation. The second stirring driving member 221 can drive the second stirring shaft 222 to rotate and drive the second blade 223 to rotate in the reaction solution, so as to stir the reaction solution. Illustratively, the second agitator drive member 221 is preferably an agitator of conventional construction, readily available and inexpensive.
Further, the bottom of the second reaction vessel body 210 is connected with a second pneumatic valve, and the second pneumatic valve is electrically connected with a controller, which can control the opening and closing of the second pneumatic valve to control the discharge of the material in the second reaction vessel body 210, thereby reducing the manual operation of the operator.
Further, in order to avoid the safety factor of the reaction system from being reduced due to the vibration of the synthesis reaction kettle 100 and the post-treatment reaction kettle 200 in the chemical reaction process, the reaction kettle system further comprises a support frame body, and the support frame body is used for fixing the synthesis reaction kettle 100 and the post-treatment reaction kettle 200.
Example two
The present embodiment provides a reaction kettle system, the structure of the reaction kettle system of the present embodiment is substantially the same as that of the reaction kettle system of the first embodiment, and the difference between the reaction kettle system of the present embodiment and the reaction kettle system of the first embodiment is: the reaction kettle system in the second embodiment does not comprise the heat preservation barrel 600, and the condensation liquid-separating component 500 is added.
As shown in fig. 2, in order to realize the heat preservation of the first reaction vessel body 110, a jacket may be sleeved outside the first reaction vessel body 110 in this embodiment, so that the first reaction vessel body 110 can continuously maintain a heat preservation state.
Correspondingly, please continue to refer to fig. 2, in order to control the heat preservation condition in the jacket, the reaction kettle system of this embodiment further includes a temperature control mechanism 700, and the temperature control mechanism 700 is connected to the jacket, so as to control the temperature rise or decrease of the jacket, so as to ensure that the temperature inside the first reaction kettle body 110 is at the preset temperature for performing the chemical reaction, which is beneficial to improving the success probability of the experiment. Specifically, the temperature control mechanism 700 can raise the temperature of the raw materials to a suitable temperature, and the first reaction vessel body 110 is subjected to a chemical reaction at a constant temperature in cooperation with the jacket. Meanwhile, the improvement of the temperature in the first reaction kettle body 110 is also beneficial to the improvement of the reaction efficiency, and further the experimental efficiency of the reaction kettle system is improved.
As shown in fig. 2, in this embodiment, the reaction kettle system further includes a condensation and liquid separation assembly 500. The condensation liquid-separating component 500 can be communicated with the synthesis reaction kettle 100, and the condensation liquid-separating component 500 is used for condensing and separating the steam evaporated in the synthesis reaction kettle 100, so that the liquid evaporated at high temperature in the synthesis reaction kettle 100 can be condensed and recovered in the condensation liquid-separating component 500. Condensation divides liquid subassembly 500 can enough avoid steam to volatilize and cause air pollution in the air, through retrieving the recycle with the boil-off gas condensation simultaneously, is favorable to practicing thrift the experiment cost.
Specifically, with continued reference to fig. 2, the condensation liquid separation assembly 500 includes a liquid separator 510 and a condensation pipe 520. The dispenser 510 can communicate with the synthesis reaction tank 100, so that the steam in the first reaction tank body 110 can enter into the dispenser 510. Meanwhile, the condensation pipe 520 is communicated with the liquid distributor 510 and is arranged above the liquid distributor 510, the condensation pipe 520 can cool and condense the evaporated gas in the synthesis reaction kettle 100, namely, the vapor can be condensed under the condensation effect of the condensation pipe 520 to become liquid, the liquid flows downwards into the liquid distributor 510, the liquid can be kept still in the liquid distributor 510 for a certain time, the liquid with different densities is of a layered structure, and then the liquid can be recycled layer by layer below the liquid distributor 510.
In addition, as shown in fig. 2, the condensation and separation assembly 500 further comprises a collection bottle 530, and the collection bottle 530 is communicated with the liquid distributor 510 and is arranged below the liquid distributor 510. The collection bottle 530 is capable of collecting the liquid separated from the dispenser 510. Meanwhile, the collecting bottle 530 is connected with the condenser through the control valve, and an operator can control the collecting bottle 530 to be connected with or disconnected from the condenser through the control valve, so that the control of discharging of the split liquid is realized.
Further, please refer to fig. 2, the condensation liquid-separating assembly 500 further includes a second vacuum valve 540, one end of the second vacuum valve 540 can be communicated with the condensation liquid-separating assembly 500, the other end is communicated with the vacuum generating device, and an operator can control the vacuum state in the condensation liquid-separating assembly 500 and the synthesis reaction kettle 100 by controlling the second vacuum valve 540, so as to avoid the chemical reaction that the components in the air are remained in the first reaction kettle body 110. Preferably, the second vacuum valve 540 is electrically connected to the controller, so that the controller controls the second vacuum valve 540 to automatically control the opening and closing of the second vacuum valve 540 and the vacuum condition.
It is noted that the foregoing shows and describes the general principles and features of the present invention, together with the advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are merely illustrative of the principles of the present invention, but that various changes and modifications may be made without departing from the spirit and scope of the utility model, which is defined by the appended claims and their equivalents.
Claims (10)
1. A reactor system, comprising:
a synthesis reaction kettle (100) configured to stir and mix a plurality of raw materials to form a reaction solution; and
aftertreatment reation kettle (200), with synthetic reation kettle (100) communicate through first pneumatic valve (300), just aftertreatment reation kettle (200) and first vacuum valve (400) intercommunication, first vacuum valve (400) one end can with aftertreatment reation kettle (200) intercommunication, the other end and vacuum generating device intercommunication make aftertreatment reation kettle (200) can through control with the pressure differential of synthetic reation kettle (100) will the reaction liquid drainage extremely in aftertreatment reation kettle (200), aftertreatment reation kettle (200) are configured as right the reaction liquid carries out the aftertreatment in order to obtain final product.
2. The reactor system of claim 1, wherein the synthesis reactor (100) comprises:
a first reaction kettle body (110) configured to contain the raw material, the first reaction kettle body (110) being provided with a first opening;
a first stirring assembly (120), an output end of the first stirring assembly (120) being extendable into the first reaction tank body (110) to stir the raw material; and
a first cover (130) covering the first opening, the first cover (130) configured to isolate the first reactor body (110) from an external environment.
3. The reactor system of claim 2, wherein the synthesis reactor (100) further comprises:
a temperature monitoring assembly (140), wherein an output end of the temperature monitoring assembly (140) can penetrate through the first cover body (130) and extend into the first reaction kettle body (110).
4. The reactor system of claim 2, further comprising:
the heat-preserving container (600), first reation kettle body (110) can be placed in heat-preserving container (600) so that first reation kettle body (110) can be in the ultra-low temperature state.
5. A reactor system according to any one of claims 1 to 4, wherein the post-treatment reactor (200) comprises:
a second reaction vessel body (210) configured to accommodate the reaction liquid transferred from the synthesis reaction vessel (100);
the output end of the second stirring component (220) can extend into the second reaction kettle body (210) to stir the reaction liquid; and
a second cover (230) configured to isolate the second reactor body (210) from an external environment.
6. The reactor system according to any one of claims 1 to 4, further comprising:
an automatic filling mechanism (800) configured to periodically and quantitatively fill the raw material into the synthesis reaction kettle (100).
7. The reactor system according to any one of claims 1 to 4, further comprising:
the condensation liquid separation component (500) can be communicated with the synthesis reaction kettle (100), and the condensation liquid separation component (500) is configured to condense and separate the steam evaporated in the synthesis reaction kettle (100).
8. The reactor system of claim 7, wherein the condensation separation assembly (500) comprises:
a liquid distributor (510) capable of communicating with the synthesis reaction vessel (100);
a condenser pipe (520) communicated with the liquid distributor (510) and arranged above the liquid distributor (510), wherein the condenser pipe (520) is configured to cool and condense the evaporated gas in the synthesis reaction kettle (100); and
a collection bottle (530) in communication with the dispenser (510) and disposed below the dispenser (510).
9. The reactor system of claim 8, wherein the condensation separation assembly (500) further comprises:
and one end of the second vacuum valve (540) can be communicated with the condensed liquid-separating component (500), and the other end is communicated with the vacuum generating device.
10. The reactor system as set forth in any one of claims 8 to 9, further comprising:
a support frame body configured to fix the synthesis reaction kettle (100), the post-treatment reaction kettle (200) and the condensation and liquid separation assembly (500).
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|---|---|---|---|
| CN202122358763.1U CN215743453U (en) | 2021-09-28 | 2021-09-28 | Reaction kettle system |
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| CN202122358763.1U CN215743453U (en) | 2021-09-28 | 2021-09-28 | Reaction kettle system |
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| CN215743453U true CN215743453U (en) | 2022-02-08 |
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