CN215655107U - Reation kettle is used in tetramethylammonium hydroxide production - Google Patents

Abstract

The utility model discloses a reaction kettle for producing tetramethylammonium hydroxide, which comprises a barrel, stirring rods and fixing rods, wherein the middle part of the upper end of the barrel is connected with a stirring motor through a bolt, the transmission output end of the stirring motor is connected with a stirring shaft through a key, the stirring shaft penetrates through the barrel, the bottom end of the stirring shaft is rotatably connected with a fixed seat, the fixed seat is connected with the barrel through a bolt, the stirring rod is connected onto the stirring shaft through a bolt, and the fixing rods are arranged between the stirring rods. Has the advantages that: according to the utility model, by arranging the stirring shaft, the stirring rod and the fixing rod, the fixing rod is fixedly arranged on the barrel body, and the stirring rod and the fixing rod are mutually matched, so that the stirring efficiency of the device can be improved, the materials are uniformly mixed, the production quality is improved, the resistance on the stirring shaft can be reduced, the load on the stirring motor is further reduced, and the energy consumption is saved.

Description

Reation kettle is used in tetramethylammonium hydroxide production

Technical Field

The utility model relates to the technical field of tetramethylammonium hydroxide production devices, and particularly relates to a reaction kettle for tetramethylammonium hydroxide production.

Background

Tetramethyl ammonium hydroxide is an organic base and has extremely wide application in the field of industrial scientific research, domestic tetramethyl ammonium hydroxide is mainly used as a main catalyst in the synthesis of organosilicon series products, such as silicone oil, silicone rubber, silicone resin and the like, although the dosage is not large, the influence on the yield and the quality of the products is large, and foreign tetramethyl ammonium hydroxide is mainly used for polyester polymers, textiles, plastic products, food, leather and foreign tetramethyl ammonium hydroxide and is mainly used for polyester polymers, textiles, plastic products, food, leather, wood processing, electroplating, microorganisms and the like.

The reation kettle is needed to be used to tetramethyl ammonium hydroxide when production to realize the heating of technological requirement, evaporation, cooling and low high-speed thoughtlessly join in marriage the function, and current reation kettle stirring efficiency is lower, makes the material stirring mix inhomogeneous easily, influences tetramethyl ammonium hydride's production quality, and current reation kettle produces vibrations easily when the stirring in addition, and stability is relatively poor, influences the result of use of device.

SUMMERY OF THE UTILITY MODEL

Technical problem to be solved

In order to overcome the defects of the prior art, the reaction kettle for producing tetramethylammonium hydroxide is provided, and the problems that the stirring efficiency of the existing reaction kettle is low, the materials are stirred and mixed unevenly easily, and the production quality of tetramethylammonium hydroxide is influenced are solved.

(II) technical scheme

The utility model is realized by the following technical scheme: the utility model provides a reaction kettle for producing tetramethylammonium hydroxide, which comprises a barrel, a stirring rod and a fixed rod, wherein the middle part of the upper end of the barrel is connected with a stirring motor through a bolt, the transmission output end of the stirring motor is connected with a stirring shaft through a key, the stirring shaft penetrates through the barrel, the bottom end of the stirring shaft is rotatably connected with a fixed seat, the fixed seat is connected with the barrel through a bolt, the stirring rod is connected with the stirring rod through a bolt, the fixed rod is arranged between the stirring rods, the fixed rod is connected with the barrel through a bolt, the bottom end of the barrel is connected with a buffer plate through a bolt, the bottom end of the buffer plate is connected with a supporting leg through a bolt, a heat-insulating layer is formed on the inner wall of the barrel, one side of the heat-insulating layer is connected with a heating plate through a hook, one side outside the barrel is connected with a heat exchanger through a hook, the heat exchanger is connected with a heat exchange tube through a tube hoop, and one end of the heat exchange tube is inserted into the barrel.

Through adopting above-mentioned technical scheme, can give the barrel provides the outrigger, simultaneously passes through the buffer board can absorb the anti-seismic force that the barrel received improves the stability of device, slows down vibrations, improves the result of use, can improve simultaneously the heat preservation effect of barrel improves material reaction efficiency, also can produce heat, heats at first use or winter and keeps reaction temperature, improves the reaction rate of material, simultaneously passes through the heat exchange tube can be with the leading-in of heat that produces in the reaction process in the heat exchanger, carry out the heat exchange, guarantee that cooling heat transfer is balanced, can improve resource utilization simultaneously.

Further, a solvent adding port is formed in one side of the upper end of the cylinder, a spraying tube bundle is connected to the top end in the cylinder through a clamping groove, and the spraying tube bundle is connected with the solvent adding port through a pipeline.

Through adopting above-mentioned technical scheme, make the barrel provides the outrigger, and the tetramethylammonium hydroxide production reaction of being convenient for, agitator motor provides drive power, drives the (mixing) shaft and the puddler rotates, and then stirs the material, through the fixing base is right the (mixing) shaft carries out fixed stay, ensures the (mixing) shaft rotates stably, through the puddler with the dead lever is mutually supported, both can improve the stirring efficiency of device, makes the material misce bene, can reduce simultaneously the resistance that the (mixing) shaft received, and then reduces agitator motor receives, practices thrift the energy consumption, through solvent interpolation mouth can to add methyl alcohol in the barrel, and pass through spray the bank blowout, ensure that methyl alcohol sprays evenly, improve material mixing efficiency.

Further, a feeding hole is formed in one side of the upper end of the cylinder body, and an operation panel is connected to the side wall of the cylinder body through a clamping groove.

By adopting the technical scheme, the material can be conveniently added into the barrel, and the operation of the device is controlled by the operation panel.

(III) advantageous effects

Compared with the prior art, the utility model has the following beneficial effects:

1. in order to solve the problems that the stirring efficiency of the existing reaction kettle is low, the materials are easily stirred and mixed unevenly, and the production quality of tetramethylammonium hydride is influenced, the stirring efficiency of the device can be improved, the materials are uniformly mixed, the production quality is improved, the resistance on the stirring shaft can be reduced, the load on the stirring motor is further reduced, and the energy consumption is saved by arranging the stirring shaft, the stirring rod and the fixed rod, fixedly installing the fixed rod on the barrel and mutually matching the stirring rod and the fixed rod;

2. in order to solve the problems that the existing reaction kettle is easy to shake during stirring, has poor stability and affects the use effect of the device, the reaction kettle provided by the utility model can absorb the shock resistance of the barrel by arranging the buffer plate and the supporting legs, thereby improving the stability of the device, slowing down the shock and improving the use effect.

Drawings

FIG. 1 is a schematic structural diagram of a reaction kettle for producing tetramethylammonium hydroxide according to the present invention;

FIG. 2 is a sectional view of a reaction vessel for producing tetramethylammonium hydroxide according to the present invention;

FIG. 3 is a top view of a reaction vessel for producing tetramethylammonium hydroxide according to the present invention.

The reference numerals are explained below:

1. a stirring motor; 2. a feed inlet; 3. a barrel; 4. a buffer plate; 5, supporting legs; 6. an operation panel; 7. a solvent addition port; 8. a spray pipe bundle; 9. heating plates; 10. a fixed seat; 11. a stirring rod; 12. fixing the rod; 13. a heat-insulating layer; 14. a stirring shaft; 15. a heat exchanger; 16. a heat exchange tube.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the utility model and are not intended to limit the utility model.

As shown in fig. 1-3, the reaction kettle for tetramethylammonium hydroxide production in this embodiment comprises a barrel 3, a stirring rod 11 and a fixing rod 12, wherein the barrel 3 provides stable support to facilitate tetramethylammonium hydroxide production reaction, the middle part of the upper end of the barrel 3 is connected with a stirring motor 1 through a bolt, the transmission output end of the stirring motor 1 is connected with a stirring shaft 14 through a key, the stirring shaft 14 penetrates through the barrel 3, the bottom end of the stirring shaft 14 is rotatably connected with a fixing seat 10, the fixing seat 10 is connected with the barrel 3 through a bolt, the stirring shaft 14 is connected with the stirring rod 11 through a bolt, the fixing rod 12 is arranged between the stirring rods 11, the fixing rod 12 is connected with the barrel 3 through a bolt, the stirring motor 1 provides driving force to drive the stirring shaft 14 and the stirring rod 11 to rotate to stir materials, and the stirring shaft 14 is fixedly supported by the fixing seat 10, ensure (mixing) shaft 14 and rotate stably, mutually support through puddler 11 and dead lever 12, both can improve the stirring efficiency of device, make the material misce bene, can reduce the resistance that (mixing) shaft 14 received simultaneously, and then reduce the load that agitator motor 1 received, practice thrift the energy consumption, barrel 3 upper end one side shaping has solvent to add mouth 7, the top is connected with spray tube bank 8 through the draw-in groove in the barrel 3, spray tube bank 8 adds mouth 7 with the solvent and passes through the pipe connection, can add methyl alcohol to barrel 3 in through solvent interpolation mouth 7, and spout through spray tube bank 8, ensure that methyl alcohol sprays evenly, improve material mixing efficiency, barrel 3 upper end one side shaping has feed inlet 2, be connected with operating panel 6 through the draw-in groove on the barrel 3 lateral wall, be convenient for through feed inlet 2 to add the material in barrel 3, and operate through operating panel 6 controlling means.

As shown in FIG. 1 and FIG. 2, in this embodiment, there are buffer board 4 in the barrel 3 bottom through bolted connection, and there is supporting leg 5 in the buffer board 4 bottom through bolted connection, can provide the outrigger for barrel 3, can absorb the anti-seismic force that barrel 3 received through buffer board 4 simultaneously, improve the stability of device, slow down vibrations, improve the result of use.

As shown in fig. 2, in this embodiment, one side of the heat preservation layer 13 is connected with the heating plate 9 through a hook, one side of the outer side of the cylinder 3 is connected with the heat exchanger 15 through a hook, the heat exchange tube 16 is connected to the heat exchanger 15 through a pipe hoop, one end of the heat exchange tube 16 is inserted into the cylinder 3, the heating plate 9 can generate heat, the heat is heated to maintain the reaction temperature when the heat exchanger is used for the first time or in winter, the reaction rate of the material is increased, meanwhile, the heat generated in the reaction process can be introduced into the heat exchanger 15 through the heat exchange tube 16, the heat exchange is performed, the balance of cooling and heat exchange is ensured, and meanwhile, the resource utilization rate can be increased.

The specific implementation process of this embodiment is as follows: when in use, the device is connected with an external power supply, the operation of the device is controlled by the operation panel 6, materials can be conveniently added into the barrel 3 through the feed inlet 2, the barrel 3 is firstly heated through the heating plate 9, the reaction temperature is kept, the stirring motor 1 provides driving force to drive the stirring shaft 14 and the stirring rod 11 to rotate so as to stir the materials, the fixing seat 10 is used for fixedly supporting the stirring shaft 14 so as to ensure the stable rotation of the stirring shaft 14, the stirring rod 11 and the fixing rod 12 are mutually matched, the stirring efficiency of the device can be improved, the materials are uniformly mixed, the resistance borne by the stirring shaft 14 can be reduced, the load borne by the stirring motor 1 is further reduced, the energy consumption is saved, the methanol can be added into the barrel 3 through the solvent adding port 7 and is sprayed out through the spraying pipe bundle 8, the uniform spraying of the methanol is ensured, and the material mixing efficiency is improved, simultaneously can be with the leading-in heat exchanger 15 of the heat that produces in the reaction process in through heat exchange tube 16, carry out the heat exchange, guarantee that the cooling heat transfer is balanced, the shaping of barrel 3 inner wall has heat preservation 13, can improve the heat preservation effect of barrel 3, improves the reaction rate of material, can absorb the anti-seismic force that barrel 3 received through buffer board 4 simultaneously, improves the stability of device, slows down vibrations, improves the result of use.

The above-described embodiments are merely illustrative of the preferred embodiments of the present invention and do not limit the spirit and scope of the present invention. Various modifications and improvements of the technical solutions of the present invention may be made by those skilled in the art without departing from the design concept of the present invention, and the technical contents of the present invention are all described in the claims.

Claims (3)

1. The utility model provides a reation kettle is used in tetramethylammonium hydroxide production which characterized in that: comprises a barrel body (3), stirring rods (11) and fixing rods (12), wherein the middle part of the upper end of the barrel body (3) is connected with a stirring motor (1) through bolts, the transmission output end of the stirring motor (1) is connected with a stirring shaft (14) through a key, the stirring shaft (14) penetrates through the barrel body (3), the bottom end of the stirring shaft (14) is rotatably connected with a fixing seat (10), the fixing seat (10) is connected with the barrel body (3) through bolts, the stirring shaft (14) is connected with the stirring rods (11) through bolts, the fixing rods (12) are arranged between the stirring rods (11), the fixing rods (12) are connected with the barrel body (3) through bolts, the bottom end of the barrel body (3) is connected with a buffer plate (4) through bolts, the bottom end of the buffer plate (4) is connected with supporting legs (5) through bolts, and a heat-insulating layer (13) is formed on the inner wall of the barrel body (3), one side of the heat preservation layer (13) is connected with a heating plate (9) through a hook, one side of the outer side of the barrel body (3) is connected with a heat exchanger (15) through a hook, the heat exchanger (15) is connected with a heat exchange tube (16) through a tube hoop, and one end of the heat exchange tube (16) is connected with the barrel body (3) in an inserting mode.

2. The reaction kettle for producing tetramethylammonium hydroxide according to claim 1, wherein: the device is characterized in that a solvent adding port (7) is formed in one side of the upper end of the barrel body (3), a spraying tube bundle (8) is connected to the inner top end of the barrel body (3) through a clamping groove, and the spraying tube bundle (8) is connected with the solvent adding port (7) through a pipeline.

3. The reaction kettle for producing tetramethylammonium hydroxide according to claim 1, wherein: a feeding hole (2) is formed in one side of the upper end of the barrel body (3), and an operation panel (6) is connected to the side wall of the barrel body (3) through a clamping groove.

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