CN215609458U

CN215609458U - Rapid crystallization equipment of potassium fluotitanate

Info

Publication number: CN215609458U
Application number: CN202122066527.2U
Authority: CN
Inventors: 刘阳; 刘志鸿; 岳炜; 廖范武; 刘小勇
Original assignee: Hengyang Dongfu New Material Co ltd
Current assignee: Hengyang Dongfu New Material Co ltd
Priority date: 2021-08-30
Filing date: 2021-08-30
Publication date: 2022-01-25
Anticipated expiration: 2031-08-30

Abstract

The utility model discloses rapid crystallization equipment of potassium fluotitanate, which comprises a kettle body, wherein a support frame is sleeved in the middle of the outer surface of the kettle body, four corners of the lower end of the support frame are fixedly connected with support columns, the lower ends of the four support columns are fixedly connected with a base together, four corners of the lower end of the base are fixedly connected with support legs, the left part of the upper end of the support frame is fixedly connected with a refrigerating device, the refrigerating device extends into the kettle body, the upper end of the kettle body is fixedly connected with a rotating device, the middle part of the upper end of the rotating device is fixedly connected with a stirring device, the lower end of the kettle body is fixedly connected with a discharge pipe, the lower end of the discharge pipe is fixedly connected with a discharge cover, and the right part of the front end of the support frame is fixedly connected with a control panel. According to the rapid crystallization equipment for potassium fluotitanate, the stirring device and the refrigerating device are arranged on the whole device, so that the temperature of a solution in a kettle body is rapidly reduced, the crystallization process is promoted, the mixing is uniform, and the reaction is rapid.

Description

Rapid crystallization equipment of potassium fluotitanate

Technical Field

The utility model relates to the field of equipment, in particular to rapid crystallization equipment for potassium fluotitanate.

Background

Potassium fluotitanate is a white flaky crystal, the chemical formula is K2TiF6, in the production process of producing potassium fluotitanate, the clear liquid of fluotitanate and potassium chloride solution need to be fully reacted under the conditions of normal temperature and normal pressure to obtain potassium fluotitanate crystal, the process is carried out in a synthesis kettle, in order to enable the reaction to be rapidly and effectively carried out, the clear liquid of fluotitanate and the potassium chloride solution need to be fully mixed, 1, most of the existing crystallization equipment of potassium fluotitanate is cooled by a natural cooling mode, the crystallization time is long, and the production efficiency of sodium fluoride is low; 2. the prior synthesis kettle has the problem of insufficient mixing of fluotitanic acid clear solution and potassium chloride solution; therefore, a novel rapid crystallization device of potassium fluotitanate is provided.

SUMMERY OF THE UTILITY MODEL

The utility model mainly aims to provide equipment for quickly crystallizing potassium fluotitanate, which can effectively solve the problems in the background technology.

In order to achieve the purpose, the utility model adopts the technical scheme that:

the utility model provides a potassium fluotitanate's quick crystallization equipment, includes the cauldron body, the support frame has been cup jointed at the surface middle part of the cauldron body, the equal fixedly connected with support column in lower extreme four corners of support frame, the common fixedly connected with base of lower extreme of four support columns, the equal fixedly connected with supporting legs in lower extreme four corners of base, the upper end left part fixedly connected with refrigerating plant of support frame, and refrigerating plant extend to the internal portion of cauldron, the upper end fixedly connected with rotating device of the cauldron body, rotating device's upper end middle part fixedly connected with agitating unit, the lower extreme fixedly connected with discharging pipe of the cauldron body, the lower extreme fixedly connected with ejection of compact lid of discharging pipe, the front end right part fixedly connected with control panel of support frame.

Preferably, rotating device includes a driver and sealed lid, the output of a driver runs through sealed lid and fixedly connected with thermantidote, open at the upper end middle part of sealed lid has the interlude hole, the surface lower part fixedly connected with a plurality of buckle of sealed lid, a driver fixed connection is in the upper end right part of sealed lid, sealed lid fixed connection is on the surface upper portion of the cauldron body.

Preferably, refrigerating plant includes the water tank, the upper end fixedly connected with water pipe of water tank, the surface of water pipe has cup jointed the water pump, the other end fixedly connected with refrigeration pipe of water pipe, refrigeration pipe's the other end is provided with the gas outlet, water tank fixed connection is in the upper end left part of support frame.

Preferably, agitating unit includes the driver No. two, the output of driver No. two runs through sealed lid and fixedly connected with bull stick, a plurality of puddler has been cup jointed to the surface of bull stick, the equal fixedly connected with stirring leaf in upper end of puddler, No. two driver fixed connection are in the upper end middle part of sealed lid.

Preferably, the refrigeration pipe is of a snake-shaped structure and is fixedly connected to the inner wall of the kettle body.

Preferably, the second driver is electrically connected with the control board, and the stirring rods are not in contact with the refrigerating pipe.

Compared with the prior art, the utility model has the following beneficial effects:

1. according to the utility model, the whole device is provided with the refrigerating device, the water pump is turned on, water is pumped to the refrigerating pipe through the water pipe for refrigerating, the first driver is started to drive the cooling fan to rotate, so that cold air generated in the kettle body is cooled and dispersed in a large area, the temperature of a solution in the kettle body is rapidly reduced, and the precipitation of crystals is accelerated.

2. Through set up agitating unit on whole device, utilize the output effect of No. two drivers to drive the bull stick and rotate, make its a plurality of puddler can stir the internal portion solution of cauldron, thereby improve the contact of hydrogen fluoride gas and sodium carbonate solution, a plurality of stirring leaf of fixed mounting makes fluotitanic acid solution and potassium chloride solution stirring, the reaction more abundant, and the reaction is faster on the puddler.

Drawings

FIG. 1 is a schematic view of the overall structure of an apparatus for rapid crystallization of potassium fluotitanate according to the present invention;

FIG. 2 is a schematic view showing the overall structure of a rotating device of a rapid potassium fluotitanate crystallization apparatus according to the present invention;

FIG. 3 is a schematic diagram showing the overall structure of a refrigerating apparatus of the rapid crystallization apparatus for potassium fluotitanate according to the present invention;

FIG. 4 is a schematic connection diagram of a stirring device of a rapid potassium fluotitanate crystallization device according to the present invention.

In the figure: 1. a support frame; 2. a support pillar; 3. a base; 4. supporting legs; 5. a control panel; 6. a discharging cover; 7. a discharge pipe; 8. a refrigeration device; 9. a stirring device; 10. a rotating device; 11. a kettle body; 101. a driver number one; 102. a cooling fan; 103. a sealing cover; 104. buckling; 105. inserting holes; 81. a water tank; 82. a water pump; 83. a water pipe; 84. a refrigeration pipe; 85. an air outlet; 91. a second driver; 92. a rotating rod; 93. a stirring rod; 94. stirring the leaves.

Detailed Description

In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the utility model easy to understand, the utility model is further described with the specific embodiments.

In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.

In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, such as "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.

As shown in fig. 1-4, a quick crystallization device of potassium fluotitanate, including the cauldron body 11, support frame 1 has been cup jointed at the surface middle part of the cauldron body 11, equal fixedly connected with support column 2 in the lower extreme four corners of support frame 1, the common fixedly connected with base 3 of the lower extreme of four support columns 2, equal fixedly connected with supporting legs 4 in the lower extreme four corners of base 3, the upper end left part fixedly connected with refrigerating plant 8 of support frame 1, and refrigerating plant 8 extends to the cauldron body 11 inside, the upper end fixedly connected with rotating device 10 of the cauldron body 11, the upper end middle part fixedly connected with agitating unit 9 of rotating device 10, the lower extreme fixedly connected with discharging pipe 7 of the cauldron body 11, the lower extreme fixedly connected with discharging lid 6 of discharging pipe 7, the front end right part fixedly connected with control panel 5 of support frame 1.

The rotating device 10 comprises a first driver 101 and a sealing cover 103, the first driver 101 drives the cooling fan 102 to rotate under the output action of the first driver 101, the output end of the first driver 101 penetrates through the sealing cover 103 and is fixedly connected with the cooling fan 102, a through hole 105 is formed in the middle of the upper end of the sealing cover 103, a plurality of buckles 104 are fixedly connected to the lower portion of the outer surface of the sealing cover 103, the sealing cover 103 and the kettle body 11 can be fixedly installed, the sealing performance is high, the first driver 101 is fixedly connected to the right portion of the upper end of the sealing cover 103, and the sealing cover 103 is fixedly connected to the upper portion of the outer surface of the kettle body 11; the refrigerating device 8 comprises a water tank 81, the upper end of the water tank 81 is fixedly connected with a water pipe 83, the outer surface of the water pipe 83 is sleeved with a water pump 82, the other end of the water pipe 83 is fixedly connected with a refrigerating pipe 84, the other end of the refrigerating pipe 84 is provided with an air outlet 85, and the water tank 81 is fixedly connected to the left part of the upper end of the support frame 1; the stirring device 9 comprises a second driver 91, the output end of the second driver 91 penetrates through the sealing cover 103 and is fixedly connected with a rotating rod 92, the outer surface of the rotating rod 92 is sleeved with a plurality of stirring rods 93, the solution in the kettle body 11 can be stirred by the dry stirring rods 93, so that the contact between the hydrogen fluoride gas and the sodium carbonate solution is improved, the upper ends of the stirring rods 93 are fixedly connected with stirring blades 94, the stirring rods 93 are fixedly provided with a plurality of stirring blades 94, so that the fluorotitanic acid solution and the potassium chloride solution are uniformly stirred and react more fully, and the second driver 91 is fixedly connected to the middle part of the upper end of the sealing cover 103; the output end of the second driver 91 is used for driving the rotating rod 92 to rotate, the refrigeration pipe 84 is of a snake-shaped structure, so that the refrigeration is uniform, and the refrigeration pipe 84 is fixedly connected to the inner body wall of the kettle body 11; the second driver 91 is electrically connected with the control board 5, and the plurality of stirring rods 93 are not in contact with the refrigerating pipe 84, so that rubbing and damage to equipment are avoided

It should be noted that the utility model is a potassium fluotitanate rapid crystallization device, through the fixed mounting of the supporting foot 4 in the four corners of the bottom of the base 3, the stability of the whole device is improved, the right part of the front end of the supporting frame 1 is fixedly mounted with the control panel 5, to make it operate each device, the second driver 91 is started, the output end function of the second driver 91 is utilized, thereby driving the rotating rod 92 to rotate, making its several stirring rods 93 stir the solution in the kettle body 11, thereby improving the contact between the hydrogen fluoride gas and the sodium carbonate solution, the stirring rod 93 is fixedly mounted with several stirring blades 94 to make the solution of fluotitanate and the solution of potassium chloride stir evenly, the reaction is more sufficient, the reaction is faster, when the interior of the kettle body 11 needs to be cooled, the water pump 82 is opened, the water pipe 83 pumps to the cooling pipe 84 for cooling, the first driver 101 is started, the output function of the first driver 101 is utilized, the cooling fan 102 is driven to rotate, so that the cold air generated in the kettle body 11 is cooled and dissipated in a large surface, the temperature of the solution in the kettle body 11 is quickly reduced, the precipitation of crystals is accelerated, the whole device is simple in structure and high in adaptability, and the use of the potassium fluotitanate in the quick crystallization work is facilitated.

The foregoing shows and describes the general principles and broad features of the present invention and advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the utility model as claimed. The scope of the utility model is defined by the appended claims and equivalents thereof.

Claims

1. The utility model provides a quick crystallization equipment of potassium fluotitanate, includes the cauldron body (11), its characterized in that: the middle part of the outer surface of the kettle body (11) is sleeved with a support frame (1), four corners of the lower end of the support frame (1) are fixedly connected with support columns (2), the lower ends of the four support columns (2) are fixedly connected with a base (3) together, four corners of the lower end of the base (3) are fixedly connected with supporting legs (4), the left part of the upper end of the supporting frame (1) is fixedly connected with a refrigerating device (8), the refrigerating device (8) extends into the kettle body (11), the upper end of the kettle body (11) is fixedly connected with a rotating device (10), the middle part of the upper end of the rotating device (10) is fixedly connected with a stirring device (9), the lower end of the kettle body (11) is fixedly connected with a discharge pipe (7), the lower end of the discharge pipe (7) is fixedly connected with a discharge cover (6), the right part of the front end of the support frame (1) is fixedly connected with a control panel (5).

2. The apparatus for the rapid crystallization of potassium fluotitanate according to claim 1, wherein: rotating device (10) include a driver (101) and sealed lid (103), the output of a driver (101) runs through sealed lid (103) and fixedly connected with thermantidote (102), open at the upper end middle part of sealed lid (103) has interlude hole (105), the surface lower part fixedly connected with a plurality of buckle (104) of sealed lid (103), the upper end right part of a driver (101) fixed connection at sealed lid (103), sealed lid (103) fixed connection is on the surface upper portion of the cauldron body (11).

3. The apparatus for the rapid crystallization of potassium fluotitanate according to claim 1, wherein: refrigerating plant (8) include water tank (81), upper end fixedly connected with water pipe (83) of water tank (81), water pump (82) have been cup jointed to the surface of water pipe (83), the other end fixedly connected with refrigeration pipe (84) of water pipe (83), the other end of refrigeration pipe (84) is provided with gas outlet (85), water tank (81) fixed connection is in the upper end left part of support frame (1).

4. The apparatus for the rapid crystallization of potassium fluotitanate according to claim 1, wherein: agitating unit (9) are including No. two driver (91), the output of No. two driver (91) runs through sealed lid (103) and fixedly connected with bull stick (92), a plurality of puddler (93) have been cup jointed to the surface of bull stick (92), the equal fixedly connected with stirring leaf (94) in upper end of puddler (93), No. two driver (91) fixed connection are in the upper end middle part of sealed lid (103).

5. The apparatus for rapidly crystallizing potassium fluotitanate according to claim 3, wherein: the refrigeration pipe (84) is of a snake-shaped structure, and the refrigeration pipe (84) is fixedly connected to the inner body wall of the kettle body (11).

6. The apparatus for rapidly crystallizing potassium fluotitanate according to claim 4, wherein: the second driver (91) is electrically connected with the control board (5), and the stirring rods (93) are not in contact with the refrigerating pipe (84).