CN215312391U - Novel condensation hydrolysis reaction cauldron - Google Patents

Abstract

The utility model relates to the technical field of chemistry science and technology, and discloses a novel condensation product hydrolysis reaction kettle, which comprises a bottom plate, wherein the top of the bottom plate is bolted with a water tank, the top of the inner wall of the water tank is bolted with a heater, the front side of the top of the water tank is communicated with an air pipe, and the middle part of the air pipe is communicated with a three-way valve; through adding water in to the water tank, utilize the heater to heat up rapidly, produce steam, and carry into the reaction cover through the trachea, to the reaction process heat supply in the retort, through the three-way valve, select specific one to carry out the hydrolysis method reaction in two retort, through pipeline and condensation tank intercommunication, make the steam in the reaction cover can get into in the condensation tank, work through the condenser, make the steam condensate into water, and in flowing into the water tank through the pipe drainage that falls into water, can guarantee the thermal continuous supply in the reaction process, accelerate reaction rate, can realize the cyclic utilization of water resource, the waste of effectual reduction water resource.

Description

Novel condensation hydrolysis reaction cauldron

Technical Field

The utility model relates to the technical field of chemistry science and technology, in particular to a novel condensation product hydrolysis reaction kettle.

Background

The condensate is defined as: the organic chemical concept in the hydrolysis reaction is that water reacts with another compound, the compound is decomposed into two parts, hydrogen in water is added to one part of the compound, and hydroxyl is added to the other part of the compound, so that the reaction process of obtaining two or more new compounds is an important means in chemical application.

Through a large amount of searches, the Chinese utility model patent: 202020348477. X; the utility model belongs to the field of reaction kettles, in particular to a novel condensation reaction kettle, which aims at solving the problems that in the prior art, when stirring, only a stirring shaft is adopted, so that the reaction rate is relatively slow, and the preparation time is overlong, and the scheme is provided, which comprises a support cover, wherein a reaction kettle is connected in the support cover in a sliding way, a rotating shaft is rotatably connected on the inner wall of one side of the reaction kettle, one end of the rotating shaft extends to the outer side of the reaction kettle and is in transmission connection with the top of the support cover, a stirring grid is fixedly arranged at the other end of the rotating shaft, a U-shaped frame is fixedly arranged on the support cover, and an air pump is fixedly arranged at the top of the U-shaped frame, the reaction kettle can be driven to do annular motion by starting a driving motor, and the stirring grid can be rotated, so as to realize the rapid stirring of mother liquor, the reaction rate is improved, and the preparation time is greatly shortened.

But current device often can have following problem when specifically using, at first, the reaction process when current device is mainly to condensation thing preparation, can not be applicable to the hydrolysis, and the hydrolysis is endothermic reaction, need have stable exothermic source to come the auxiliary work, the purpose that can promote work efficiency has been reached, secondly, when using vapor to supply heat to the reaction process, a large amount of moisture can be taken away in the giving off of vapor, direct emission can cause serious water waste, need circulate it for use, for this reason, we propose a novel condensation thing hydrolysis reaction cauldron and solve above-mentioned problem.

SUMMERY OF THE UTILITY MODEL

The utility model aims to provide a novel condensation product hydrolysis reaction kettle, which has the advantages of providing a stable heat source and realizing the cyclic utilization of water resources and solves the problems of low working efficiency and resource waste of the existing device.

In order to achieve the purpose, the utility model provides the following technical scheme: the utility model provides a novel condensation thing hydrolysis reaction cauldron, includes the bottom plate, the top bolt of bottom plate has the water tank, the top bolt of water tank inner wall has the heating machine, the front side intercommunication at water tank top has the trachea, tracheal middle part intercommunication has the three-way valve, the top that the trachea is located the three-way valve both sides all communicates with the reaction hood, the inside bolt of reaction hood has the reaction tank, the top bolt of reaction tank has changeing the case, the inside bolt of changeing the case has the motor, the output of motor extends to the inside of reaction tank and the bolt has the stirring arm, two the top of reaction hood all communicates there is the pipeline, the other end intercommunication of pipeline has the condensation box, the top bolt of condensation box inner wall has the condenser, the bottom intercommunication of condensation box has the pipe, the other end and the water tank intercommunication of pipe fall into water.

Preferably, a fixing frame is bolted between the two reaction covers, the upper side and the lower side of the fixing frame are respectively bolted with the top of the water tank and the bottom of the condensing tank, and the stability of the two reaction tanks can be ensured by arranging the fixing frame.

Preferably, two the top of retort one side all communicates there is the inlet pipe, the other end of inlet pipe extends to the outside of reaction cover and rotates and be connected with the adapter sleeve, through setting up inlet pipe and adapter sleeve, can make things convenient for the staff to add corresponding raw materials in to the retort.

Preferably, two one side of retort all communicates with the discharging pipe below being located the inlet pipe, the other end of discharging pipe extends to the outside of reaction cover and the fixed switch that has cup jointed, through setting up discharging pipe and switch, can conveniently be with the material release after the reaction.

Preferably, the opening has been seted up to the bottom of condenser box, open-ended inside joint has the filter screen, the front side joint of filter screen has the clamp splice, through setting up opening and filter screen, can guarantee the normal work of condensing engine.

Preferably, the other side of the clamping block is bolted with a spring, the other end of the spring is bolted with the inner wall of the condensing box, and the clamping block can automatically clamp the filter screen by arranging the spring.

Preferably, the top of condensing box has seted up the notch, the top bolt of clamp splice has the shifting block, shifting block and notch sliding connection through setting up the shifting block, can conveniently be dialled the clamp splice, put into the filter screen.

Compared with the prior art, the utility model provides a novel condensation product hydrolysis reaction kettle, which has the following beneficial effects:

the water tank is filled with water, the heater is utilized to rapidly raise the temperature, steam is generated and is conveyed into the reaction cover through the air pipe to supply heat to the reaction process in the reaction tanks, and a specific one of the two reaction tanks is selected to carry out the hydrolysis reaction through the three-way valve, so that the continuous supply of heat in the reaction process can be ensured, and the reaction rate is accelerated;

through pipeline and condenser box intercommunication for in the vapor in the reaction cover can get into the condenser box, through the work of condensing engine, make vapor condensate into water, and in flowing into the water tank through the pipe drainage that falls into water, can realize the cyclic utilization of water resource, the waste of effectual reduction water resource.

Drawings

FIG. 1 is a perspective view of the present invention;

FIG. 2 is a schematic cross-sectional view of a heating chamber of the present invention;

FIG. 3 is a schematic cross-sectional view of a reaction tank of the present invention;

FIG. 4 is a schematic cross-sectional view of a condenser case according to the present invention;

FIG. 5 is a schematic top view, partially in section, of a condenser case according to the present invention;

FIG. 6 is an enlarged view of a portion of FIG. 1 according to the present invention.

In the figure: 1. a base plate; 2. a water tank; 3. a heater; 4. an air tube; 5. a three-way valve; 6. a reaction hood; 7. a reaction tank; 8. box turning; 9. a motor; 10. a stirring arm; 11. a pipeline; 12. a condenser tank; 13. a condenser; 14. a downpipe; 15. a fixed mount; 16. a feed pipe; 17. connecting sleeves; 18. a discharge pipe; 19. a switch; 20. an opening; 21. filtering with a screen; 22. a clamping block; 23. a spring; 24. a notch; 25. and (5) shifting blocks.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1, 2, 3 and 6, a novel condensation hydrolysis reaction kettle comprises a bottom plate 1, a water tank 2 is bolted to the top of the bottom plate 1, a heater 3 is bolted to the top of the inner wall of the water tank 2, a gas pipe 4 is communicated with the front side of the top of the water tank 2, a three-way valve 5 is communicated with the middle of the gas pipe 4, reaction covers 6 are communicated with the tops of the gas pipe 4 at two sides of the three-way valve 5, a reaction tank 7 is bolted to the inside of the reaction cover 6, a rotating box 8 is bolted to the top of the reaction tank 7, a motor 9 is bolted to the inside of the rotating box 8, and the output end of the motor 9 extends to the inside of the reaction tank 7 and is bolted to a stirring arm 10.

The three-way valve 5 is a valve device with three ports, one inlet and two outlets, the three-way valve is different from the common valve in that the bottom is provided with an outlet, when the inner valve core is at different positions, the outlets are different, if the valve core is at the lower part, the left outlet is communicated with the right outlet, if the valve core is at the upper part, the right outlet is blocked, the left outlet is communicated with the lower outlet, because the left port and the right port are not on the same horizontal line, when the valve is tightened and separated, the water is fed to a bypass, the three-way valve is divided into a flow combining valve and a flow dividing valve according to the fluid action mode, the flow combining valve is provided with two inlets, the flow combining valve flows out from one outlet, the flow dividing valve is provided with one fluid inlet, and the flow is divided into two fluid outlets to flow out.

Through adding water to water tank 2, utilize heater 3 to heat up rapidly, produce vapor to carry into reaction cover 6 through trachea 4, to the reaction process heat supply in retort 7, through three-way valve 7, select specific one to carry out the hydrolysis method reaction in two retort 7, can guarantee the thermal continuous supply in the reaction process for reaction rate.

Further, a fixing frame 15 is bolted between the two reaction covers 6, the upper side and the lower side of the fixing frame 15 are respectively bolted with the top of the water tank 2 and the bottom of the condensation box 12, and the stability of the two reaction tanks 7 can be ensured by arranging the fixing frame 15.

Further, the top of two retort 7 one sides all communicates there is inlet pipe 16, and the other end of inlet pipe 16 extends to the outside of reaction housing 6 and swivelling joint has adapter sleeve 17, through setting up inlet pipe 16 and adapter sleeve 17, can make things convenient for the staff to add corresponding raw materials in to retort 7.

Further, one side of two retort 7 all communicates with discharging pipe 18 below being located inlet pipe 16, and the other end of discharging pipe 18 extends to the outside of reaction cover 6 and fixed the cover switch 19 that has cup jointed, through setting up discharging pipe 18 and switch 19, can conveniently be with the material release after the reaction.

Referring to fig. 1, 4 and 5, the top of each of two reaction chambers 6 is connected to a pipe 11, the other end of the pipe 11 is connected to a condenser 12, the top of the inner wall of the condenser 12 is bolted to a condenser 13, the bottom of the condenser 12 is connected to a water falling pipe 14, and the other end of the water falling pipe 14 is connected to the water tank 2.

The condenser 13 sucks working medium steam with lower pressure from the evaporator through a compressor thereof, the working medium steam with lower pressure is sent into the condenser after the pressure of the working medium steam is increased, the working medium steam is condensed into liquid with higher pressure in the condenser, the liquid with higher pressure is sent into the evaporator after the liquid with lower pressure is obtained after the throttling of the throttle valve, the liquid with lower pressure is absorbed in the evaporator and evaporated into steam with lower pressure, and therefore the refrigeration cycle is completed.

Through pipeline 11 and condenser 12 intercommunication for during vapor in the reaction hood 6 can get into condenser 12, through the work of condensing engine 13, make vapor condensate into water, and flow into water tank 2 through pipe in the water pipe 14, can realize the cyclic utilization of water resource, the waste of effectual reduction water resource.

Further, opening 20 has been seted up to the bottom of condenser box 12, and the inside joint of opening 20 has filter screen 21, and the front side joint of filter screen 21 has clamp splice 22, through setting up opening 20 and filter screen 21, can guarantee the normal work of condensing engine 13.

Furthermore, the other side of the clamping block 22 is bolted with a spring 23, the other end of the spring 23 is bolted with the inner wall of the condensation box 12, and the clamping block 22 can automatically clamp the filter screen 21 by arranging the spring 23.

Furthermore, a notch 24 is formed in the top of the condensation box 12, a shifting block 25 is bolted to the top of the clamping block 22, the shifting block 25 is connected with the notch 24 in a sliding mode, and the shifting block 25 is arranged, so that the clamping block 22 can be conveniently shifted out and placed into the filter screen 21.

During the use, at first select suitable retort 7 for use, add the raw materials through adapter sleeve 17 and inlet pipe 16 in to retort 7, utilize motor 9 to drive rabbling arm 10 and rotate the stirring, make the raw materials fully fuse, make the reaction more thorough, utilize shifting block 25 to stir clamp splice 22, with filter screen 21 joint in opening 20 department, later add water to water tank 2, utilize heater 3 to heat rapidly, produce vapor, and utilize three-way valve 5 to control the flow direction of vapor, make it flow into in correct reaction housing 6, carry out continuous heat supply to the hydrolysis reaction in the corresponding retort 7, the reaction process accelerates, later vapor can flow into condensation tank 12 through pipeline 11, condenser 13 works, become liquid water with the vapor condensation, and flow into water tank 2 through pipe 14, can accomplish work.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. A novel condensation hydrolysis reaction kettle comprises a bottom plate (1), and is characterized in that: the top of bottom plate (1) has been bolted water tank (2), the top of water tank (2) inner wall has been bolted and has been connected heater (3), the front side intercommunication at water tank (2) top has trachea (4), the middle part intercommunication of trachea (4) has three-way valve (5), the top that trachea (4) is located three-way valve (5) both sides all communicates and has reacted cover (6), the inside bolt of reaction cover (6) has retort (7), the top bolt of retort (7) has changeed case (8), the inside bolt of changeing case (8) has motor (9), the output of motor (9) extends to the inside of retort (7) and has bolted mixing arm (10), two the top of retort (6) all communicates and has pipeline (11), the other end intercommunication of pipeline (11) has condensing box (12), the top bolt of condensing box (12) inner wall has condenser (13), the bottom of the condensation tank (12) is communicated with a water falling pipe (14), and the other end of the water falling pipe (14) is communicated with the water tank (2).

2. A novel condensate hydrolysis reactor as claimed in claim 1, wherein: a fixing frame (15) is bolted between the two reaction covers (6), and the upper side and the lower side of the fixing frame (15) are respectively bolted with the top of the water tank (2) and the bottom of the condensing tank (12).

3. A novel condensate hydrolysis reactor as claimed in claim 1, wherein: two the top of retort (7) one side all communicates there is inlet pipe (16), the other end of inlet pipe (16) extends to the outside of reaction cover (6) and rotates and be connected with adapter sleeve (17).

4. A novel condensate hydrolysis reactor as claimed in claim 1, wherein: and discharge pipes (18) are communicated with one side of the two reaction tanks (7) and positioned below the feed pipe (16), and the other ends of the discharge pipes (18) extend to the outside of the reaction cover (6) and are fixedly sleeved with switches (19).

5. A novel condensate hydrolysis reactor as claimed in claim 1, wherein: opening (20) have been seted up to the bottom of condenser box (12), the inside joint of opening (20) has filter screen (21), the front side joint of filter screen (21) has clamp splice (22).

6. A novel condensate hydrolysis reactor as claimed in claim 5, wherein: the other side of the clamping block (22) is bolted with a spring (23), and the other end of the spring (23) is bolted with the inner wall of the condensation box (12).

7. A novel condensate hydrolysis reactor as claimed in claim 5, wherein: notch (24) have been seted up at the top of condenser box (12), shifting block (25) have been bolted connection to the top of clamp splice (22), shifting block (25) and notch (24) sliding connection.

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