CN215084990U

CN215084990U - Controllable dynamic crystallization equipment of temperature

Info

Publication number: CN215084990U
Application number: CN202121047569.5U
Authority: CN
Inventors: 陈先进; 刘华华; 邱凯; 汪文清
Original assignee: Hubei Zhonglan Hongyuan New Energy Materials Co Ltd
Current assignee: Hubei Zhonglan Hongyuan New Energy Materials Co Ltd
Priority date: 2021-05-17
Filing date: 2021-05-17
Publication date: 2021-12-10
Anticipated expiration: 2031-05-17

Abstract

The utility model discloses a controllable dynamic crystallization equipment of temperature, including reation kettle, heating rod, temperature sensor, control cabinet and motor, inside first cavity and the second cavity of being provided with of reation kettle, first cavity has the heating rod through fixed block fixed mounting, the heating rod shape is the U type, the second cavity is close to second cavity one side fixed mounting and has temperature sensor, the control cabinet fixed mounting be in reation kettle outer wall one end, motor fixed mounting is at reation kettle top center, motor output shaft has the live-rollers, the live-rollers outer wall is provided with first stirring vane, be provided with the mechanism of disturbing in disorder on the first stirring vane, reation kettle bottom center is provided with row material pipe. Compared with the prior art, the utility model provides high heat conduction between the solution prevents that the solution inside and outside from being heated inhomogeneously to can accurate monitoring solution be heated the temperature of crystallization, carry out the temperature regulation and control.

Description

Controllable dynamic crystallization equipment of temperature

Technical Field

The utility model relates to a crystallization technique field especially relates to a controllable dynamic crystallization equipment of temperature.

Background

Traditional reation kettle generally adopts electrical heating or heating fluid heating, and the heating is not even enough, need install the temperature when a plurality of temperature controllers detect the crystallization, has the local overheat phenomenon of solution, can not effectual intensification or cooling control.

An effective solution to the problems in the related art has not been proposed yet.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the defects existing in the prior art and providing a temperature-controllable dynamic crystallization device.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

a temperature-controllable dynamic crystallization device, which comprises a reaction kettle, a heating rod, a temperature sensor, a console and a motor, a first cavity and a second cavity are arranged in the reaction kettle, a heating rod is fixedly arranged in the first cavity through a fixing block, the heating rod is U-shaped, one side of the second cavity close to the second cavity is fixedly provided with a temperature sensor, the control console is fixedly arranged at one end of the outer wall of the reaction kettle, the motor is fixedly arranged at the center of the top of the reaction kettle, the output shaft of the motor is connected with a rotating roller, the outer wall of the rotating roller is provided with a first stirring blade, the first stirring blade is provided with a disordering mechanism, the center of the bottom of the reaction kettle is provided with a discharging pipe, the top end of the discharge pipe is communicated with the first cavity, and a second stirring blade is arranged on the part, extending into the discharge pipe, of one end of the rotating roller.

Further, the disturbing mechanism comprises a round rod, the round rod is fixed on the first stirring blades, the outer wall of one end of the round rod is connected with a rotating sleeve in a rotating mode, the outer wall of the rotating sleeve is provided with disturbing blades, and the disturbing blades are symmetrically arranged.

Furthermore, a heat insulation layer is arranged on one side, close to the outer wall of the reaction kettle, of the second cavity, and a material guide table is arranged at the bottom end inside the second cavity.

Further, the temperature sensor, the heating rod and the motor are electrically connected with the console.

Furthermore, a feeding pipe is arranged at one end of the top of the reaction kettle.

Furthermore, one end of the outer wall of the discharge pipe is provided with a switch valve.

Furthermore, both ends of the bottom of the reaction kettle are provided with supporting legs which are symmetrically arranged.

The utility model has the advantages that:

1. through heating rod to first cavity internal heating, heat transfer absorbs to the solution in the second cavity, starter motor drives the live-rollers rotation simultaneously, make first stirring vane be heated the solution stirring, the vortex that stirs solution formation through first stirring vane is disturbed the leaf and is rotated and give and break up, improve heat conduction between the solution, prevent that solution from forming the swirl and leading to the solution inside and outside not homogeneous that is heated, thereby can make temperature sensor accurate monitoring solution be heated the temperature of crystallization, thereby can change the power of heating rod according to actual conditions through the control cabinet.

2. Lead to arranging the condition that the material pipe blockked up after can preventing the solution crystallization through second stirring vane, can make things convenient for the crystal to discharge through the guide platform.

3. The heat insulation layer can prevent heat from being dissipated outwards, and energy loss of the heat insulation layer is reduced.

Drawings

FIG. 1 is a schematic front view of a temperature-controlled dynamic crystallization apparatus according to example 1;

FIG. 2 is a schematic diagram of the internal structure of a temperature-controlled dynamic crystallization apparatus proposed in example 1;

FIG. 3 is a schematic view showing the internal structure of a discharge pipe of the temperature-controlled dynamic crystallization apparatus set forth in example 1;

FIG. 4 is a schematic diagram of the structure of the disturbing mechanism of the temperature-controllable dynamic crystallization apparatus proposed in example 1.

In the figure: the device comprises a reaction kettle 1, a first cavity 2, a heat insulation layer 3, a fixing block 4, a heating rod 5, supporting legs 6, a temperature sensor 7, a control console 8, a motor 9, a second cavity 10, a first stirring blade 11, a round rod 12, a rotating sleeve 13, a disturbing blade 14, a feeding pipe 15, a material guiding platform 16, a discharging pipe 17, a switch valve 18, a rotating roller 19 and a second stirring blade 20.

Detailed Description

The technical solution of the present patent will be described in further detail with reference to the following embodiments.

Reference will now be made in detail to embodiments of the present application, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are exemplary only for the purpose of explaining the present patent and are not to be construed as limiting the present patent.

In the description of the present application, it is to be understood that the terms "center", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on those shown in the drawings, and are used merely for convenience in describing the present application and for simplicity in description, and do not indicate or imply that the referenced devices or elements must have a particular orientation, be constructed in a particular orientation, and be operated, and therefore, should not be construed as limiting the present patent.

In the description of the present application, it should be noted that unless otherwise explicitly stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and can, for example, be fixedly connected, disposed, detachably connected, disposed, or integrally connected and disposed. The specific meaning of the above terms in this patent may be understood by those of ordinary skill in the art as appropriate.

Example 1

Referring to fig. 1-4, a temperature-controllable dynamic crystallization device comprises a reaction kettle 1, a heating rod 4, a temperature sensor 7, a control console 8 and a motor 9, wherein a first cavity 2 and a second cavity 10 are arranged inside the reaction kettle 1, the first cavity 2 is fixedly provided with the heating rod 5 through a fixing block 4, the heating rod 5 is U-shaped, the second cavity 2 is fixedly provided with the temperature sensor 7 near one side of the second cavity 10, the control console 8 is fixedly arranged at one end of the outer wall of the reaction kettle 1, the motor 9 is fixedly arranged at the top center of the reaction kettle 1, an output shaft of the motor 9 is connected with a rotating roller 19, the outer wall of the rotating roller 19 is provided with a first stirring blade 11, the first stirring blade 11 is provided with a disordering mechanism, the bottom center of the reaction kettle 1 is provided with a material discharge pipe 17, the top end of the material discharge pipe 17 is communicated with the first cavity 10, a portion of one end of the rotating roller 19 extending into the discharge pipe 17 is provided with a second stirring blade 20.

Wherein, the mechanism of disturbing order includes round bar 12, round bar 12 is fixed on first stirring

vane

11, 12 one end outer walls of round bar rotate and are connected with and rotate cover 13, it is provided with the leaf of disturbing order 14 to rotate cover 13 outer wall, the leaf of disturbing order 14 is the symmetry and places.

A heat insulation layer 3 is arranged on one side, close to the outer wall of the reaction kettle 1, of the second cavity 2, and a material guide table 16 is arranged at the bottom end inside the second cavity 10.

Wherein, the temperature sensor 7, the heating rod 5 and the motor 9 are electrically connected with the console 8.

Wherein, a feeding pipe 15 is arranged at one end of the top of the reaction kettle 1.

Wherein, the one end of the outer wall of the discharge pipe 17 is provided with a switch valve 18.

Wherein, reation kettle 1 bottom both ends are provided with landing leg 6, landing leg 6 is the symmetry and places.

The working principle is as follows: during the use, add through inlet pipe 15 and treat crystallization solution, heat in to first cavity 2 through heating rod 5, the solution absorption in heat transfer second cavity 10, starter motor 9 drives rotor roll 19 and rotates simultaneously, make first stirring vane 11 be heated solution stirring, the vortex that forms through first stirring vane 11 stirring solution is disturbed leaf 14 and is rotated and give and break up, improve heat conduction between the solution, it leads to the solution inside and outside inhomogeneous that is heated to prevent that solution from forming the swirl, thereby can make temperature sensor 7 accurate monitoring solution be heated the temperature of crystallization, thereby can change the power of heating rod 3 according to actual conditions through control cabinet 8, heat or cooling process. The second stirring blade 20 prevents the discharge pipe 17 from being clogged after the solution is crystallized. The crystal can be conveniently discharged through the material guide table 16, and meanwhile, heat can be prevented from being dissipated outwards through the heat insulation layer 3, so that energy loss of the crystal is reduced.

The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims

1. The temperature-controllable dynamic crystallization device comprises a reaction kettle (1), a heating rod (5), a temperature sensor (7), a control console (8) and a motor (9), and is characterized in that a first cavity (2) and a second cavity (10) are arranged inside the reaction kettle (1), the heating rod (5) is fixedly arranged in the first cavity (2) through a fixing block (4), the heating rod (5) is U-shaped, the temperature sensor (7) is fixedly arranged on one side, close to the second cavity (10), of the first cavity (2), the control console (8) is fixedly arranged at one end of the outer wall of the reaction kettle (1), the motor (9) is fixedly arranged at the center of the top of the reaction kettle (1), an output shaft of the motor (9) is connected with a rotating roller (19), and the outer wall of the rotating roller (19) is provided with a first stirring blade (11), be provided with on first stirring vane (11) and disturb the mechanism, reation kettle (1) bottom center is provided with row material pipe (17), arrange material pipe (17) top with first cavity (2) are put through mutually, live-rollers (19) one end extends to arrange the part in material pipe (17) and be provided with second stirring vane (20).

2. The temperature-controllable dynamic crystallization device as claimed in claim 1, wherein the disturbing mechanism comprises a round bar (12), the round bar (12) is fixed on the first stirring blade (11), a rotating sleeve (13) is rotatably connected to the outer wall of one end of the round bar (12), the outer wall of the rotating sleeve (13) is provided with disturbing blades (14), and the disturbing blades (14) are symmetrically arranged.

3. The temperature-controllable dynamic crystallization equipment as claimed in claim 1, characterized in that a heat insulation layer (3) is arranged on one side of the first cavity (2) close to the outer wall of the reaction kettle (1), and a material guide platform (16) is arranged at the bottom end inside the second cavity (10).

4. A temperature-controlled dynamic crystallization apparatus according to claim 1, wherein the temperature sensor (7), the heating rod (5) and the motor (9) are electrically connected to the console (8).

5. A temperature-controllable dynamic crystallization apparatus as claimed in claim 1, wherein a feed pipe (15) is provided at one end of the top of the reaction vessel (1).

6. A temperature-controlled dynamic crystallization apparatus as claimed in claim 1, characterized in that the discharge pipe (17) is provided with a switching valve (18) at one end of its outer wall.

7. The temperature-controllable dynamic crystallization device as claimed in claim 1, wherein the two ends of the bottom of the reaction kettle (1) are provided with legs (6), and the legs (6) are symmetrically arranged.