CN214913469U - Liquid milk rotary evaporator - Google Patents

Liquid milk rotary evaporator Download PDF

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Publication number
CN214913469U
CN214913469U CN202120717752.5U CN202120717752U CN214913469U CN 214913469 U CN214913469 U CN 214913469U CN 202120717752 U CN202120717752 U CN 202120717752U CN 214913469 U CN214913469 U CN 214913469U
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CN
China
Prior art keywords
rotary evaporator
bottle
soon
liquid milk
fixing
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Active
Application number
CN202120717752.5U
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Chinese (zh)
Inventor
杨松霖
黄诗豪
尚乐
邵世瑞
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Yunnan Yunce Quality Testing Co ltd
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Yunnan Yunce Quality Testing Co ltd
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Priority to CN202120717752.5U priority Critical patent/CN214913469U/en
Application granted granted Critical
Publication of CN214913469U publication Critical patent/CN214913469U/en
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Abstract

Liquid milk rotary evaporator relates to evaporating equipment technical field, specifically is liquid milk rotary evaporator. The utility model discloses a liquid milk rotary evaporator comprises rotary evaporator, blending machine and control system, and its characterized in that rotary evaporator's the solid fixed ring of evaporating bottle head end setting soon to and install the buckle part on the rotary evaporator connecting pipe and carry out the joint the utility model discloses a liquid milk rotary evaporator, the bottle easy to assemble soon conveniently takes off, saves time, promotes detection efficiency, and the temperature synchronization that makes the bottle of evaporating soon and heat the bath kettle is faster, and the solution that makes in the bottle of evaporating soon is heated faster.

Description

Liquid milk rotary evaporator
Technical Field
The utility model relates to an evaporation equipment technical field specifically is liquid milk rotary evaporator.
Background
The rotary evaporator can be used for recovering and evaporating the organic solvent. It utilizes a motor to drive the distillation flask to rotate. Because the distiller rotates continuously, zeolite can be prevented from being added and bumping is avoided. Meanwhile, due to continuous rotation, the liquid is attached to the wall of the distiller to form a layer of liquid film, so that the evaporation area is enlarged, and the evaporation speed is increased. When vacuum distillation is used, the liquid in the bottle may boil suddenly when the temperature is high and the degree of vacuum is high. At this time, the degree of vacuum should be reduced to allow distillation to proceed smoothly, and when evaporation is stopped, heating is stopped, vacuum pumping is stopped, and finally, the power supply is cut off to stop rotation.
The rotary evaporator needs to be taken down and installed to rotate the evaporation bottle back and forth when in use, the device is mostly connected by threads, inconvenient installation is realized, inconvenient taking down is realized, time is consumed, and the detection efficiency is influenced. In addition, when the water in the heating bath kettle reaches the required temperature, the rotary steaming bottle needs a certain time to reach the required temperature, and the temperature synchronization of the rotary steaming bottle and the heating bath kettle is slow, so that the solution in the rotary steaming bottle is heated slowly.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve and evaporate the inconvenient installation of bottle soon, inconvenient taking off consumes time, influences detection efficiency, evaporates the bottle soon and heats the temperature synchronization of bath kettle slower, makes the solution in evaporating the bottle soon and is heated the problem that becomes slow.
The liquid milk rotary evaporator is composed of a rotary evaporator, a blending device and a control system, and is characterized in that the inner wall of a rotary evaporation bottle of the rotary evaporator is coated with a heat conduction layer and is clamped by a fixing ring arranged at the head end of the rotary evaporation bottle and a buckle part arranged on a connecting pipe of the rotary evaporator;
the buckle component comprises a first fixing plate, a second fixing plate and a spring, wherein the first fixing plate is square, the spring is arranged at each of four corners, and the second fixing plate is fixed at the other end of the spring; the second fixing plate is provided with a hole, a fixing buckle and a telescopic rod; the second fixed plate is divided into two parts, the fixing buckles are fixed on two sides of the dividing seam of the second fixed plate and are respectively and correspondingly arranged on the front and back surfaces and the upper and lower positions of the second fixed plate, and the telescopic rod is sleeved between the two fixing buckles which are respectively and correspondingly arranged.
The utility model discloses a liquid milk rotary evaporator, second fixed plate through setting up, can pull open the second fixed plate, pass the hole with solid fixed ring again, loosen the fixed plate at last and can fix the second fixed plate on evaporating the bottle soon, through the tensile action of spring, make the second fixed plate drive evaporate the bottle soon and receive the effort to first fixed plate direction, connecting pipe and evaporate bottle fixed joint soon this moment, when needing to take off evaporate the bottle soon, it can take off to pull open the second fixed plate, evaporate bottle easy to assemble soon, conveniently take off, save time, promote detection efficiency.
In addition, this liquid milk rotary evaporation appearance through the heat-conducting layer that sets up, when making the temperature rise in the heating bath, revolves the steam bottle and contacts with the hot water, and the heat-conducting layer can be faster makes the temperature transmit to on the solution that needs the evaporation, makes the temperature of revolving the steam bottle more synchronous with the heating bath, and the solution that makes in the steam bottle soon is heated sooner.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the structure of the centrifugal tube of the present invention;
FIG. 3 is a schematic view of the top cover structure of the present invention;
FIG. 4 is a schematic diagram of a second fixing plate structure of the present invention;
fig. 5 is a schematic view of the structure of the rotary steaming bottle of the present invention.
Fig. 6 is an enlarged view of fig. 1A according to the present invention.
In the figure: 1. a base; 2. a support; 3. a lifting rod; 4. a connecting pipe; 5. a condenser; 6. a feed valve; 7. a drive motor; 8. a first fixing plate; 9. a spring; 10. a fixing ring; 11. a second fixing plate; 111. a hole; 112. a fixing buckle; 113. a telescopic rod; 12. steaming the bottle in a rotating mode; 121. a heat conductive layer; 13. heating the bath kettle; 14. an intelligent controller; 15. centrifuging the tube; 16. a top cover; 17. a servo motor; 18. sticking prevention sheets; 19. a micro-scale measuring instrument; 20. a screw rod; 21. a card slot; 22. a vortex mixer; 23. and (5) extracting the bottles.
Detailed Description
The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention.
Liquid milk rotary evaporator, including base 1, be provided with support 2 on the base 1, be provided with lifter 3 on the support 2, be provided with connecting pipe 4 on the lifter 3, 4 left ends of connecting pipe are provided with condenser 5, and 5 high-ends of condenser are provided with charge valve 6, and the low side setting is drawed bottle 23.
The middle part of the connecting pipe 4 is provided with a driving motor 7 and a first fixing plate 8. The first fixing plate 8 is square, the four corners are respectively provided with a spring 9, and the other end of the spring 9 is used for fixing a second fixing plate 11. The second fixing plate 11 is provided with a hole 111, a fixing buckle 112 and a telescopic rod 113. The second fixing plate 11 can be divided into two parts, the fixing buckles 112 are fixed on two sides of the divided seam of the second fixing plate 11 through screws, the two sides of the second fixing plate are correspondingly arranged up and down, and the telescopic rods 113 are sleeved between the two fixing buckles which are correspondingly arranged respectively. The second fixing plate is separated or combined by the telescopic rod 113.
The end of the lower end of the connecting pipe 4 is provided with a rotary steaming bottle 12, the head end of the rotary steaming bottle 12 is provided with a fixing ring 10, the inner wall is wrapped by a heat conduction layer 121, and a heating bath 13 is arranged below the inner wall. Intelligent control 14 sets up on base 1, still is provided with centrifuging tube 15 on the base 1. The heating bath 13 is electrically connected with the intelligent controller 14 through a wire, the intelligent controller 14 is externally connected with a power supply, and the rotary steaming bottle 12 can be heated through the heating bath 13.
Centrifuge tube 15 top is provided with top cap 16, is provided with servo motor 17 on the top cap 16, and servo motor 17's output passes top cap 16 and is provided with draw-in groove 21, and centrifuge tube 15 inner wall is provided with prevents that the piece 18 is prevented to prevent that solution from remaining on the inner wall. The bottom end is provided with a micro-measuring instrument 19 and a vortex mixer 22, and the weight of the solution in the centrifugal tube 15 can be detected through the micro-measuring instrument 19. The vortex mixer 22 is provided with a screw rod 20, and the screw rod 20 is clamped on the clamping groove 21, so that the servo motor 17 can drive the screw rod 20 to rotate in the centrifugal tube. The micro-measuring instrument 19 is electrically connected with the intelligent controller 14 through a lead, and can provide power for the vortex mixer 22 through the servo motor 17,
the lifting rod 3 and the connecting pipe 4 are fixedly installed through a buckle, the connecting pipe 4 and the condenser 5 are in threaded connection, and the connecting pipe 4 can ascend or descend through the lifting rod 3. The driving motor 7 is electrically connected with the intelligent controller 14 through a lead.
When the centrifugal liquid evaporator is used, firstly, the solution to be evaporated and the extracting solution are added into the centrifugal tube 15 together, the solution to be evaporated is fully mixed through the vortex mixer 22, and then the centrifugal tube 15 is started through the intelligent controller 14 to centrifuge the mixed solution. Pull open second fixed plate 11, can take off and evaporate bottle 12 soon, then add the solution that mixes in evaporating bottle 12 soon, pull open second fixed plate 11 again, will evaporate solid fixed ring 10 on the bottle 12 soon and pass hole 111, and make the mouth and the connecting pipe 4 butt joint of evaporating bottle 12 soon, closed second fixed plate 11 again, later spring 9 can stimulate second fixed plate 11, make and evaporate bottle 12 card soon between first fixed plate 8 and second fixed plate 11, connecting pipe 4 and evaporate bottle 12 fixed joint soon this moment, evaporate bottle 12 easy to assemble soon, conveniently take off, save time, promote detection efficiency. Open driving motor 7 and heating bath 13 through intelligent control ware 14, add the right amount of water in heating bath 13, and use intelligent control ware 14 control heating bath 13 to heat water, heat-conducting layer 121 can be faster make the temperature transmit to on the solution that needs the evaporation, make the temperature of evaporating bottle 12 and heating bath 13 soon more synchronous, make the solution in evaporating bottle 12 soon be heated sooner, rethread driving motor 7's rotation drives evaporating bottle 12 soon and rotates, make solution evaporate, get into after condensing steam through condenser 5 and draw bottle 23.

Claims (2)

1. The liquid milk rotary evaporator is composed of a rotary evaporator, a blending device and a control system, and is characterized in that the inner wall of a rotary evaporation bottle of the rotary evaporator is coated with a heat conduction layer and is clamped by a fixing ring arranged at the head end of the rotary evaporation bottle and a buckle part arranged on a connecting pipe of the rotary evaporator;
the buckle component comprises a first fixing plate, a second fixing plate and a spring, wherein the first fixing plate is square, the spring is arranged at each of four corners, and the second fixing plate is fixed at the other end of the spring; the second fixing plate is provided with a hole, a fixing buckle and a telescopic rod; the second fixed plate is divided into two parts, the fixing buckles are fixed on two sides of the dividing seam of the second fixed plate and are respectively and correspondingly arranged on the front and back surfaces and the upper and lower positions of the second fixed plate, and the telescopic rod is sleeved between the two fixing buckles which are respectively and correspondingly arranged.
2. The rotary evaporator for liquid milk as claimed in claim 1, wherein the inner wall of the centrifugal tube is provided with a patch.
CN202120717752.5U 2021-04-08 2021-04-08 Liquid milk rotary evaporator Active CN214913469U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202120717752.5U CN214913469U (en) 2021-04-08 2021-04-08 Liquid milk rotary evaporator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202120717752.5U CN214913469U (en) 2021-04-08 2021-04-08 Liquid milk rotary evaporator

Publications (1)

Publication Number Publication Date
CN214913469U true CN214913469U (en) 2021-11-30

Family

ID=79044106

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202120717752.5U Active CN214913469U (en) 2021-04-08 2021-04-08 Liquid milk rotary evaporator

Country Status (1)

Country Link
CN (1) CN214913469U (en)

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Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Liquid milk rotary evaporator

Granted publication date: 20211130

Pledgee: China Merchants Bank Limited by Share Ltd. Kunming branch

Pledgor: YUNNAN YUNCE QUALITY TESTING CO.,LTD.

Registration number: Y2024530000002