CN214810803U

CN214810803U - Improved production equipment for creatine monohydrate

Info

Publication number: CN214810803U
Application number: CN202120393604.2U
Authority: CN
Inventors: 张慧强; 张悦凯; 龚家勇; 龚家学
Original assignee: Ningxia Weiyu Biotechnology Co ltd
Current assignee: Ningxia Weiyu Biotechnology Co ltd
Priority date: 2021-02-22
Filing date: 2021-02-22
Publication date: 2021-11-23
Anticipated expiration: 2031-02-22

Abstract

The utility model discloses a modified production facility for creatine monohydrate, hold case, discharging pipe, reaction bin and circulation reaction agitating unit including supporting leg, mixed storehouse, switching-over agitating unit, support frame, sodium hydroxide, the supporting leg is evenly located under the mixed storehouse diapire, switching-over agitating unit locates in the mixed storehouse, the support frame is located on the mixed storehouse roof, the support frame is L type structure, sodium hydroxide holds the case and locates on the support frame, the reaction bin is located on the mixed storehouse lateral wall, discharging pipe one end is located the sodium hydroxide and is held under the case. The utility model belongs to the technical field of the intermediate processing of medicine, specifically indicate a direction of being convenient for to stirring leaf is adjusted, the mixing stirring, and the abundant reaction adds the mixed liquid with sodium hydroxide through circulation reaction agitating unit in, and the circulation reaction accelerates reaction rate for the modified production facility that is used for creatine monohydrate of improvement production efficiency.

Description

Improved production equipment for creatine monohydrate

Technical Field

The utility model belongs to the technical field of the processing of medical intermediate, specifically indicate a modified production facility for creatine monohydrate.

Background

Creatine monohydrate is a raw material for medicine and additive for health products. Can inhibit muscle fatigue, relieve fatigue and tension, recover physical fitness, accelerate protein synthesis of human body, make muscle firmer, enhance muscle elasticity, reduce cholesterol, blood lipid and blood sugar levels, improve muscular dystrophy of the middle aged and the elderly, and delay aging, and creatine monohydrate can be used as food additive, cosmetic surfactant, feed additive, beverage additive, medicinal raw material and health product additive, or be directly made into capsule or tablet for oral administration. The creatine monohydrate has wide application, and during the actual chemical synthesis, the aqueous solution of hydroxyacetonitrile and the aqueous solution of methylamine are utilized to carry out nucleophilic substitution reaction to generate the methylaminoacetonitrile, the temperature of the nucleophilic substitution reaction is 10-40 ℃, and the time of the nucleophilic substitution reaction is 1-6 hours; with methylamino acetonitrile reaction liquid, carry out hydrolysis under the condition that sodium hydroxide exists, obtain sarcosine sodium water solution, mix through agitating unit in traditional production facility, because its rabbling mechanism is only rotatory from a direction, the stirring is not enough even, makes solution reaction incomplete easily, causes the material waste big, and is with high costs, the addition of sodium hydroxide and mixing arrangement separately operate alone, have increased the flow, have fallen production efficiency.

SUMMERY OF THE UTILITY MODEL

In order to solve the problem, the utility model provides an utilize switching-over agitating unit to adjust the direction of stirring leaf, the mixing stirring is even, and the intensive reaction adds the mixed liquid with sodium hydroxide through circulation reaction agitating unit in, and the circulation reaction accelerates reaction rate for the modified production facility that is used for creatine monohydrate of improvement production efficiency.

In order to realize the above functions, the utility model discloses the technical scheme who takes as follows: an improved production device for creatine monohydrate comprises supporting legs, a mixing bin, a reversing stirring device, a supporting frame, a sodium hydroxide containing box, a discharging pipe, a reaction bin and a circulating reaction stirring device, wherein the supporting legs are uniformly arranged below the bottom wall of the mixing bin to play a role of fixed support, the reversing stirring device is arranged in the mixing bin, the supporting frame is arranged on the top wall of the mixing bin and is of an L-shaped structure, the sodium hydroxide containing box is arranged on the supporting frame, the reaction bin is arranged on the outer side wall of the mixing bin, one end of the discharging pipe is arranged below the sodium hydroxide containing box, the other end of the discharging pipe penetrates through the top wall of the reaction bin and is arranged in the reaction bin, so that sodium hydroxide can conveniently enter the reaction bin from the discharging pipe, and the circulating reaction stirring device is arranged in the reaction bin; the reversing stirring device comprises a motor shell I, a motor shell II, a driving motor I, a driving motor II, a stirring rod, a rotating shaft, a fixed block I, a fixed block II, a conical gear I, a conical gear II, a connecting shaft and stirring blades, wherein the motor shell II is arranged on the top wall of the mixing bin and plays a role in protecting the motor, the driving motor II is arranged in the motor shell II, the fixed block I is arranged on the bottom wall of the mixing bin, one end of the stirring rod is rotatably arranged on the fixed block I, the other end of the stirring rod penetrates through the top wall of the mixing bin to be connected with the output end of the driving motor II, the motor shell I is arranged in the stirring rod, the driving motor I is arranged in the motor shell I, the output end of the driving motor I penetrates through the bottom wall of the motor shell I to be arranged, the fixed block II is arranged on the fixed block I, one end of the rotating shaft is rotatably arranged on the fixed block II, and the other end of the rotating shaft is connected with the output end of the driving motor I, the connecting shaft penetrates through the side wall of the stirring rod, a plurality of groups of connecting shafts are arranged on the connecting shaft, the first conical gear is fixedly sleeved on the connecting shaft, the second conical gear is fixedly sleeved on the rotating shaft, the first conical gear and the second conical gear are meshed, and the stirring blades are arranged at one end, away from the conical gear, of the connecting shaft, so that the solution can be uniformly mixed; the circulation reaction stirring device comprises a protective shell, a rotary motor, a stirring shaft, a rotary rod, a liquid pumping pipe, a liquid discharging pipe, a drawing pump and a communicating pipe, wherein the drawing pump is arranged in the side wall of the mixing bin, one end of the liquid pumping pipe is arranged in the reaction bin, the other end of the liquid pumping pipe penetrates through the side wall of the mixing bin and is connected with the drawing pump, one end of the liquid discharging pipe penetrates through the side wall of the mixing bin and is connected with the drawing pump, one end of the communicating pipe penetrates through the side wall of the mixing bin and is arranged in the mixing bin, the other end of the communicating pipe penetrates through the side wall of the reaction bin and is arranged in the reaction bin, the protective shell is arranged under the bottom wall of the reaction bin and plays a role in protecting the motor, the rotary motor is arranged in the protective shell, the stirring shaft penetrates through the bottom wall of the reaction bin and is connected with the output end of the rotary motor, and the rotary rod is uniformly arranged on the outer side wall of the stirring shaft, the sodium hydroxide and the mixed solution are convenient to mix, and the reaction is more sufficient.

Further, inlay on the mixed storehouse diapire and be equipped with the switch board, be equipped with the handle on the switch board, be convenient for control mix opening and sealing in storehouse.

Further, be equipped with fixed cover block on the puddler inside wall, fixed cover block runs through the pivot setting, plays the effect of support, fixed cover block is equipped with two sets ofly.

Furthermore, a liquid outlet pipe is arranged on the outer side wall of the bottom of the mixing bin, and a liquid outlet valve is arranged on the liquid outlet pipe, so that the liquid outlet pipe can be conveniently controlled to be opened and closed.

Furthermore, a feeding pump is arranged on the discharging pipe, so that the discharging quantity at the discharging pipe can be conveniently controlled.

The utility model adopts the above structure to gain beneficial effect as follows: the utility model provides a set up of an improved production facility for creatine monohydrate through switching-over agitating unit, driving motor two drives the puddler rotation, drive stirring leaf rotation simultaneously, driving motor drives the pivot rotation, the pivot drives conical gear two rotation, conical gear two drives conical gear one rotation, conical gear drives the connecting axle rotation, the connecting axle drives stirring leaf rotation, adjust the direction of stirring leaf, be convenient for mix the solution evenly, through the setting of circulation reaction agitating unit, the mixed solution in the mixing storehouse passes through the communicating pipe and gets into in the reaction storehouse, feed pump control sodium hydroxide in the sodium hydroxide holding box falls into the reaction storehouse through the discharging pipe, the rotating motor drives the stirring shaft rotation, the stirring shaft drives the rotary rod rotation, react sodium hydroxide and mixed solution, be convenient for the abundant reaction, through the extraction pump with reaction storehouse after the solution send back to the mixing storehouse through the fluid-discharge pipe, the reaction is repeated in such a way, the utilization rate of raw materials is improved, and the production cost is saved.

Drawings

Fig. 1 is an overall structural view of an improved production apparatus for creatine monohydrate of the present invention.

The device comprises a supporting leg, a supporting frame, a sodium hydroxide containing box, a discharging tube, a reaction bin, a circulating reaction stirring device, a motor shell I, a motor shell II, a driving motor I, a driving motor 12, a driving motor II, a stirring rod 13, a stirring rod 14, a rotating shaft 15, a fixed block I, a fixed block II, a conical gear I, a conical gear II, a connecting shaft 19, a connecting shaft 20, a stirring blade 21, a protective shell 22, a rotating motor 23, a stirring shaft 24, a rotating rod 25, a liquid pumping tube 26, a liquid discharging tube 27, an extraction pump 28, a communicating tube 29, a switch plate 30, a handle 31, a fixed sleeve block 32, a liquid discharging tube 33, a liquid discharging valve 34 and a feeding pump.

Detailed Description

The technical solution of the present invention will be described clearly and completely with reference to the accompanying drawings, and obviously, the described embodiments are some, but not all embodiments of the present invention. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance. The present invention will be described in further detail with reference to the accompanying drawings.

As shown in fig. 1, the utility model relates to an improved production equipment for creatine monohydrate, including supporting leg 1, mixing bin 2, switching-over agitating unit 3, support frame 4, sodium hydroxide containing box 5, discharging pipe 6, reaction bin 7 and circulation reaction agitating unit 8, supporting leg 1 is evenly located under 2 bottom walls of mixing bin, switching-over agitating unit 3 is located in mixing bin 2, support frame 4 is located on 2 top walls of mixing bin, support frame 4 is an L-shaped structure, sodium hydroxide containing box 5 is located on support frame 4, reaction bin 7 is located on 2 outer side walls of mixing bin, one end of discharging pipe 6 is located under 5 sodium hydroxide containing box, the other end of discharging pipe 6 runs through 7 top walls of reaction bin and is located in 7 reaction bin, circulation reaction agitating unit 8 is located in 7 reaction bin; the reversing stirring device 3 comprises a first motor shell 9, a second motor shell 10, a first driving motor 11, a second driving motor 12, a stirring rod 13, a rotating shaft 14, a first fixed block 15, a second fixed block 16, a first conical gear 17, a second conical gear 18, a connecting shaft 19 and a stirring blade 20, wherein the second motor shell 10 is arranged on the top wall of the mixing bin 2, the second driving motor 12 is arranged in the second motor shell 10, the first fixed block 15 is arranged on the bottom wall of the mixing bin 2, one end of the stirring rod 13 is rotatably arranged on the first fixed block 15, the other end of the stirring rod 13 penetrates through the top wall of the mixing bin 2 to be connected with the output end of the second driving motor 12, the first motor shell 9 is arranged in the stirring rod 13, the first driving motor 11 is arranged in the first motor shell 9, the output end of the first driving motor 11 penetrates through the bottom wall of the first motor shell 9 to be arranged, the second fixed block 16 is arranged on the first fixed block 15, one end of the rotating shaft 14 is rotatably arranged on the second fixed block 16, the other end of the rotating shaft 14 is connected to the output end of the first driving motor 11, the connecting shaft 19 penetrates through the side wall of the stirring rod 13, a plurality of groups of connecting shafts 19 are arranged, the first conical gear 17 is fixedly sleeved on the connecting shaft 19, the second conical gear 18 is fixedly sleeved on the rotating shaft 14, the first conical gear 17 and the second conical gear 18 are meshed, and the stirring blade 20 is arranged at one end, far away from the first conical gear 17, of the connecting shaft 19; the circulation reaction stirring device 8 comprises a protective shell 21, a rotating motor 22, a stirring shaft 23, a rotating rod 24, a liquid pumping pipe 25, a liquid discharging pipe 26, an extraction pump 27 and a communicating pipe 28, wherein the extraction pump 27 is arranged in the side wall of the mixing bin 2, one end of the liquid pumping pipe 25 is arranged in the reaction bin 7, the other end of the liquid pumping pipe 25 penetrates through the side wall of the mixing bin 2 and is connected with the extraction pump 27, one end of the liquid discharging pipe 26 is arranged in the mixing bin 2, the other end of the liquid discharging pipe 26 penetrates through the side wall of the mixing bin 2 and is connected with the extraction pump 27, one end of the communicating pipe 28 penetrates through the side wall of the mixing bin 2 and is arranged in the mixing bin 2, the other end of the communicating pipe 28 penetrates through the side wall of the reaction bin 7 and is arranged in the reaction bin 7, the protective shell 21 is arranged below the bottom wall of the reaction bin 7, the stirring shaft 23 penetrates through the bottom wall of the reaction bin 7 and is connected with the output end of the rotating motor 22, the rotating rods 24 are uniformly arranged on the outer side wall of the stirring shaft 23.

The bottom wall of the mixing bin 2 is embedded with a switch plate 29, and the switch plate 29 is provided with a handle 30.

Be equipped with fixed nest block 31 on the puddler 13 inside wall, fixed nest block 31 runs through pivot 14 and sets up.

Be equipped with drain pipe 32 on the 2 bottom lateral walls in mixed storehouse, be equipped with drain valve 33 on the drain pipe 32.

A feeding pump 34 is arranged on the discharge pipe 6.

When the device is used, firstly, the switch board 29 is opened, the hydroxyl acetonitrile water solution and the methylamine water solution are poured into the mixing bin 2, the driving motor II 12 is started, the driving motor II 12 drives the stirring rod 13 to rotate and simultaneously drives the stirring blade 20 to rotate and stir, the driving motor I11 is started, the driving motor I11 drives the rotating shaft 14 to rotate, the rotating shaft 14 drives the conical gear II 18 to rotate, the conical gear II 18 drives the conical gear I17 to rotate, the conical gear I17 drives the connecting shaft 19 to rotate, the connecting shaft 19 drives the stirring blade 20 to rotate, the direction of the stirring blade 20 is adjusted, the solutions are mixed uniformly, the mixed solutions enter the reaction bin 7 through the communicating pipe 28, the feeding pump 34 controls the sodium hydroxide in the sodium hydroxide containing box 5 to fall into the reaction bin 7 through the discharging pipe 6, the rotating motor 22 is started, the rotating motor 22 drives the stirring shaft 23 to rotate, the stirring shaft 23 drives the rotating rod 24 to rotate, and (3) reacting the sodium hydroxide with the mixed solution, fully reacting, and sending the reacted solution in the reaction bin 7 back to the mixing bin 2 through a liquid discharge pipe 26 by using an extraction pump 27, repeating the steps and circularly reacting until the sodium hydroxide is completely reacted.

The present invention and the embodiments thereof have been described above, but the description is not limited thereto, and the embodiment shown in the drawings is only one of the embodiments of the present invention, and the actual structure is not limited thereto. In summary, those skilled in the art should understand that they should not be limited to the embodiments described above, and that they can design the similar structure and embodiments without departing from the spirit of the invention.

Claims

1. An improved production plant for creatine monohydrate, characterized in that: the device comprises supporting legs, a mixing bin, a reversing stirring device, a supporting frame, a sodium hydroxide containing box, a discharging pipe, a reaction bin and a circulating reaction stirring device, wherein the supporting legs are uniformly arranged below the bottom wall of the mixing bin; the reversing stirring device comprises a motor shell I, a motor shell II, a driving motor I, a driving motor II, a stirring rod, a rotating shaft, a fixed block I, a fixed block II, a conical gear I, a conical gear II, a connecting shaft and stirring blades, wherein the motor shell II is arranged on the top wall of the mixing bin, the driving motor II is arranged in the motor shell II, the fixed block I is arranged on the bottom wall of the mixing bin, one end of the stirring rod can be rotatably arranged on the fixed block I, the other end of the stirring rod penetrates through the top wall of the mixing bin to be connected with the output end of the driving motor II, the motor shell I is arranged in the stirring rod, the driving motor I is arranged in the motor shell I, the output end of the driving motor I penetrates through the bottom wall of the motor shell I to be arranged, the fixed block II is arranged on the fixed block I, one end of the rotating shaft can be rotatably arranged on the fixed block II, and the other end of the rotating shaft is connected with the output end of the driving motor I, the connecting shaft penetrates through the side wall of the stirring rod, a plurality of groups of connecting shafts are arranged on the connecting shaft, the first conical gear is fixedly sleeved on the connecting shaft, the second conical gear is fixedly sleeved on the rotating shaft, the first conical gear and the second conical gear are meshed, and the stirring blades are arranged at one end, away from the conical gear, of the connecting shaft; circulation reaction agitating unit includes protecting sheathing, rotating electrical machines, (mixing) shaft, rotary rod, liquid suction pipe, fluid-discharge tube, extraction pump and communicating pipe, the extraction pump is located in mixing the storehouse lateral wall, liquid suction pipe one end is located in the reaction storehouse, the liquid suction pipe other end runs through mixing the storehouse lateral wall and connects in the extraction pump, fluid-discharge tube one end is located in mixing the storehouse, the fluid-discharge tube other end runs through mixing the storehouse lateral wall and connects on the extraction pump, communicating pipe one end runs through mixing the storehouse lateral wall and locates in mixing the storehouse, the other end runs through the reaction storehouse lateral wall and locates in the reaction storehouse, protecting sheathing locates under the reaction storehouse diapire, rotating electrical machines locates in the protecting sheathing, the (mixing) shaft runs through reaction storehouse diapire and connects in the rotating electrical machines output, the rotary rod is evenly located on the (mixing) shaft lateral wall.

2. An improved production plant for creatine monohydrate according to claim 1, characterized in that: the bottom wall of the mixing bin is embedded with a switch board, and the switch board is provided with a handle.

3. An improved production plant for creatine monohydrate according to claim 2, characterized in that: be equipped with fixed cover block on the puddler inside wall, fixed cover block runs through the pivot setting.

4. An improved production plant for creatine monohydrate according to claim 3, characterized in that: and a liquid outlet pipe is arranged on the outer side wall of the bottom of the mixing bin, and a liquid outlet valve is arranged on the liquid outlet pipe.

5. An improved production plant for creatine monohydrate according to claim 4, characterized in that: and a feeding pump is arranged on the discharge pipe.