CN115253839A - Production equipment for creatine monohydrate - Google Patents
Production equipment for creatine monohydrate Download PDFInfo
- Publication number
- CN115253839A CN115253839A CN202210941148.XA CN202210941148A CN115253839A CN 115253839 A CN115253839 A CN 115253839A CN 202210941148 A CN202210941148 A CN 202210941148A CN 115253839 A CN115253839 A CN 115253839A
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- CN
- China
- Prior art keywords
- box
- shaft
- stirring
- mixing
- mixing box
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- MEJYXFHCRXAUIL-UHFFFAOYSA-N 2-[carbamimidoyl(methyl)amino]acetic acid;hydrate Chemical compound O.NC(=N)N(C)CC(O)=O MEJYXFHCRXAUIL-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 229960004826 creatine monohydrate Drugs 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- 238000003756 stirring Methods 0.000 claims abstract description 76
- 238000006243 chemical reaction Methods 0.000 claims abstract description 46
- 230000005540 biological transmission Effects 0.000 claims abstract description 13
- 238000001035 drying Methods 0.000 claims abstract description 10
- 230000000903 blocking effect Effects 0.000 claims description 3
- 230000000149 penetrating effect Effects 0.000 claims description 2
- 239000007788 liquid Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 description 13
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000010534 nucleophilic substitution reaction Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- LTYRAPJYLUPLCI-UHFFFAOYSA-N glycolonitrile Chemical compound OCC#N LTYRAPJYLUPLCI-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- PVVRRUUMHFWFQV-UHFFFAOYSA-N 2-(methylamino)acetonitrile Chemical compound CNCC#N PVVRRUUMHFWFQV-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/836—Mixing plants; Combinations of mixers combining mixing with other treatments
- B01F33/8362—Mixing plants; Combinations of mixers combining mixing with other treatments with chemical reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/50—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle
- B01F25/53—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle in which the mixture is discharged from and reintroduced into a receptacle through a recirculation tube, into which an additional component is introduced
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C277/00—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
- C07C277/08—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention discloses production equipment for creatine monohydrate, belonging to the technical field of creatine monohydrate processing; the method comprises the following steps: reaction box, the mixing box, the drying cabinet, mixing box bottom symmetry sets up four group's landing legs, this top cap is articulated at mixing box top, first (mixing) shaft rotates to be connected and arranges in the mixing box, the vertical direction setting of first (mixing) shaft, the output shaft and the first (mixing) shaft of the first motor of mixing box top are arranged in to first motor, the first (mixing) shaft outside is arranged in to the driving pipe cover, set up the awl tooth on the first (mixing) shaft, it is connected with the connecting axle to rotate on the driving pipe lateral wall, the connecting axle runs through the driving pipe, and the connecting axle passes through awl tooth and first (mixing) shaft transmission, utilize the pump body to send the reaction box with the mixed liquid in the mixing box once more in, make mixed liquid reaction thorough, make the mixed liquid after the reaction repeatedly circulate in reaction box and mixing box, and improve stirring effect, high durability and convenient use, and high utilization ratio.
Description
Technical Field
The invention relates to a production device for creatine monohydrate, belonging to the technical field of creatine monohydrate processing.
Background
Creatine monohydrate is a raw material for medicine and additive for health products. The creatine monohydrate is produced by utilizing a hydroxyacetonitrile aqueous solution and a methylamine aqueous solution to carry out nucleophilic substitution reaction to generate methylaminoacetonitrile, wherein the temperature of the nucleophilic substitution reaction is 10-40 ℃, the time of the nucleophilic substitution reaction is 1-6 hours, the conventional production equipment reacts in a reaction box, mixes in the mixing box and finally enters a drying box, and the reaction box and the mixing box are relatively independent, so that the mixed solution of the reaction box does not reach the reaction and enters the mixing box, and the mixed solution in the mixing box is discharged without fully stirring, thereby causing incomplete solution reaction and causing great material waste.
Disclosure of Invention
The production equipment for creatine monohydrate can solve the problems that the mixed liquor in the reaction box is not ready to react and then enters the mixing box, and the mixed liquor in the mixing box is discharged without being fully stirred, so that the solution cannot react completely, and the material waste is large.
In order to solve the above problems, the present invention provides the following technical solutions: a production facility for creatine monohydrate comprising: the stirring device comprises a reaction box, a mixing box and a drying box, wherein four groups of support legs are symmetrically arranged at the bottom of the mixing box, the top of the mixing box is hinged to a top cover, a first stirring shaft is rotatably connected and arranged in the mixing box, the first stirring shaft is arranged in the vertical direction, a first motor is arranged at the top of the mixing box, the output shaft of the first motor is connected with the first stirring shaft, a transmission pipe sleeve is arranged outside the first stirring shaft, a bevel gear is arranged on the first stirring shaft, a connecting shaft is rotatably connected onto the side wall of the transmission pipe and penetrates through the transmission pipe, the connecting shaft is in transmission with the first stirring shaft through the bevel gear, the two groups of connecting shafts are symmetrically arranged based on the first stirring shaft, a plurality of groups of bevel gears are equidistantly arranged on the first stirring shaft, stirring pieces are arranged at the end part of the connecting shaft, an outlet pipe is arranged at the bottom of the mixing box and communicated with the drying box, a suction pipe is arranged at the bottom of the mixing box, the reaction box is arranged on the side wall of the mixing box, a pump body is connected with the suction pipe and communicated with the reaction box, a second motor is arranged at the top of the reaction box, a second motor is arranged at the top of the reaction box, a disconnected cylinder, the connecting pipe is arranged between the disconnected part of the reaction box, and is arranged between the disconnected connecting pipe, and communicated with the disconnected connecting pipe, and is arranged between the disconnected connecting pipe, and connected with the disconnected connecting pipe;
four groups of connecting rods are arranged on the inner wall of the intermittent cylinder at equal angles, the intermittent cylinder is externally connected with a driving motor, the connecting rods are fixed with an output shaft of an external motor, and the rotating speed of the external motor is one tenth of that of the first motor;
the stirring piece comprises connecting blocks, stirring strips and transverse strips, wherein the connecting blocks are connected to two ends of each stirring strip respectively, the stirring strips are arranged in an arc shape, a plurality of groups of stirring strips are arranged at equal angles, and the transverse strips are arranged between two adjacent groups of stirring strips;
the end part of the connecting pipe is provided with an arc groove, and the side wall of the discontinuous cylinder is attached to the arc groove of the connecting pipe to form a blocking structure;
the central angle corresponding to the arc length of the discontinuous hole is not less than 90 degrees;
gaps are reserved between the two ends of the intermittent cylinder and the inner wall of the reaction box;
the height of the pump body is higher than that of the stirring rod, and the height of the connecting pipe on the mixing box is higher than that of the suction pipe;
the discharge pipe is provided with an electromagnetic valve.
The invention has the beneficial effects that:
1. the pump body is utilized to send the mixed liquid in the mixing box into the reaction box again, so that the mixed liquid can react thoroughly;
2. the mixed solution after reaction is repeatedly circulated in the reaction box and the stirring box, so that the stirring effect is improved;
3. convenient to use improves the utilization ratio.
Drawings
Fig. 1 is a schematic diagram of a production apparatus for creatine monohydrate according to the present invention.
Fig. 2 is a schematic structural diagram of a reaction box of a production device for creatine monohydrate according to the present invention.
Fig. 3 is a schematic structural diagram of an intermittent cylinder of a production device for creatine monohydrate according to the present invention.
Fig. 4 is a front view of a stirring member of a manufacturing apparatus for creatine monohydrate according to the present invention.
1. A first motor; 2. a mixing box; 3. a stirring member; 4. a drying oven; 5. a discharge pipe; 6. a support leg; 7. a first stirring shaft; 8. a drive tube; 9. a connecting shaft; 10. a straw; 11. a pump body; 12. a filling pipe; 13. a second motor; 14. a reaction box; 15. a top cover; 16. a connecting pipe; 17. a stirring rod; 18. an interrupting cylinder; 19. a second stirring shaft; 20. a connecting rod; 21. a discontinuous hole; 22. connecting blocks; 23. stirring strips; 24. and (4) transverse strips.
Detailed Description
The invention is further described below with reference to the accompanying drawings.
It should be noted that the terms "front," "back," "left," "right," "upper" and "lower" used in the following description refer to directions in fig. 1, and the terms "inner" and "outer" refer to directions toward and away from, respectively, the geometric center of a particular component.
According to the illustrations of FIGS. 1-4: the invention provides a production device for creatine monohydrate, which comprises: the reaction box 14, the mixing box 2 and the drying box 4, four groups of supporting legs 6 are symmetrically arranged at the bottom of the mixing box 2, the top cover 15 is hinged at the top of the mixing box 2, the first stirring shaft 7 is rotatably connected and arranged in the mixing box 2, the first stirring shaft 7 is arranged in the vertical direction, the first motor 1 is arranged at the top of the mixing box 2, the output shaft of the first motor 1 is connected with the first stirring shaft 7, the transmission pipe 8 is sleeved outside the first stirring shaft 7, the first stirring shaft 7 is provided with bevel teeth, the side wall of the transmission pipe 8 is rotatably connected with a connecting shaft 9, the connecting shaft 9 penetrates through the transmission pipe 8, the connecting shaft 9 is in transmission with the first stirring shaft 7 through the bevel teeth, two groups of connecting shafts 9 are symmetrically arranged based on the first stirring shaft 7, the first stirring shaft 7 is equidistantly provided with a plurality of groups of bevel teeth, the end part of the connecting shaft 9 is provided with a stirring part 3, the bottom of the mixing box 2 is provided with an outlet pipe, the outlet pipe is communicated with the drying box 4, the bottom of the mixing box 2 is provided with a suction pipe 10, the reaction box 14 is arranged on the side wall of the mixing box 2, the side wall of the reaction box 14 is provided with a pump body 11, the pump body 11 is connected with the suction pipe 10, the pump body 11 is communicated with the reaction box 14, the second motor 13 is arranged at the top of the reaction box 14, the output of the second motor 13 is connected with a second stirring shaft 19, the second stirring shaft 19 extends into the reaction box 14, the side wall of the second stirring shaft 19 is provided with a stirring rod 17, the top of the reaction box 14 is provided with a filling pipe 12, the side wall of the bottom of the reaction box 14 is provided with a connecting pipe 16, the connecting pipe 16 is communicated with the stirring box, the intermittent cylinder 18 is rotatably connected and arranged in the reaction box 14, the intermittent cylinder 18 is positioned at the end part of the connecting pipe 16, the intermittent cylinder 18 is of a structure with two ends penetrating through, and the side wall of the intermittent cylinder 18 is provided with intermittent holes 21;
four groups of connecting rods 20 are arranged on the inner wall of the intermittent cylinder 18 at equal angles, the intermittent cylinder 18 is externally connected with a driving motor, the connecting rods 20 are fixed with an output shaft of an externally connected motor, and the rotating speed of the externally connected motor is one tenth of that of the first motor 1;
the stirring piece 3 comprises connecting blocks 22, stirring strips 23 and transverse strips 24, the connecting blocks 22 are respectively connected to two ends of each stirring strip 23, the stirring strips 23 are arranged in an arc shape, a plurality of groups of stirring strips 23 are arranged at equal angles, and the transverse strips 24 are arranged between two adjacent groups of stirring strips 23;
the end part of the connecting pipe 16 is provided with an arc groove, and the side wall of the intermittent cylinder 18 is attached to the arc groove of the connecting pipe 16 to form a blocking structure;
the central angle corresponding to the arc length of the intermittent hole 21 is not less than 90 degrees;
gaps are reserved between the two ends of the intermittent cylinder 18 and the inner wall of the reaction box 14;
the height of the pump body 11 is higher than that of the stirring rod 17, and the height of the connecting pipe 16 on the mixing box 2 is higher than that of the suction pipe 10;
the discharge pipe 5 is provided with an electromagnetic valve.
The principle of the invention is as follows: when the device is used, the top cover 15 is opened, the hydroxy acetonitrile aqueous solution and the methylamine aqueous solution are poured into the mixing box 2, the second motor 13 drives the stirring shaft to rotate, the connecting shaft 9 is driven to rotate through the bevel gear, the stirring piece 3 is enabled to stir the mixed solution, the pump body 11 is used for conveying the mixed solution into the reaction box 14 through the suction pipe 10, sodium hydroxide is filled into the filling pipe 12, the second motor 13 drives the stirring rod 17 on the second stirring shaft 19 to stir the mixed solution, the reaction is accelerated, the motor drives the intermittent barrel 18 to rotate, the mixed solution enters the intermittent barrel 18 from two ends of the intermittent barrel 18, when the intermittent hole 21 corresponds to the connecting pipe 16, the mixed solution enters the connecting pipe 16 and enters the mixing box 2, after repeated times, the mixed solution completely reacts, the electromagnetic valve of the discharge pipe 5 is opened, the mixed solution enters the drying box 4 to be dried, the mixed solution in the mixing box 2 is conveyed into the reaction box 14 again through the pump body 11, the mixed solution is dried thoroughly, the mixed solution after reaction is repeatedly circulated in the reaction box 14 and the stirring effect is improved.
The present invention and its embodiments have been described above, and the description is not intended to be limiting, and the drawings show only one embodiment of the present invention, and the actual structure is not limited thereto. In summary, those skilled in the art should appreciate that they can readily use the disclosed conception and specific embodiments as a basis for designing or modifying other structures for carrying out the same purposes of the present invention without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (8)
1. A production facility for creatine monohydrate, characterized in that: comprises a reaction box (14), a mixing box (2) and a drying box (4), wherein four groups of supporting legs (6) are symmetrically arranged at the bottom of the mixing box (2), the top cover (15) is hinged at the top of the mixing box (2), a first stirring shaft (7) is rotatably connected and arranged in the mixing box (2), the first stirring shaft (7) is arranged in the vertical direction, an output shaft of a first motor (1) at the top of the mixing box (2) is connected with the first stirring shaft (7), a transmission pipe (8) is sleeved outside the first stirring shaft (7), conical teeth are arranged on the first stirring shaft (7), a connecting shaft (9) is rotatably connected on the side wall of the transmission pipe (8), the connecting shaft (9) penetrates through the transmission pipe (8), the connecting shaft (9) is in transmission with the first stirring shaft (7) through the conical teeth, two groups of the connecting shaft (9) are symmetrically arranged based on the first stirring shaft (7), a plurality of groups of conical teeth are equidistantly arranged on the first stirring shaft (7), the end part of the connecting shaft (9) is provided with a stirring connecting shaft (3), the bottom of the mixing box (2) is provided with a drying box (4), a suction pipe (11) is arranged on the side wall of the mixing box (14), and a side wall of the mixing box (10) is provided with a suction pipe (10), the pump body (11) is connected with the suction pipe (10), the pump body (11) is communicated with the reaction box (14), the top of the reaction box (14) is arranged in the second motor (13), the output of the second motor (13) is connected with a second stirring shaft (19), the second stirring shaft (19) extends into the reaction box (14), a stirring rod (17) is arranged on the side wall of the second stirring shaft (19), the top of the reaction box (14) is provided with a filling pipe (12), the side wall of the bottom of the reaction box (14) is provided with a connecting pipe (16), the connecting pipe (16) is communicated with the stirring box, the intermittent cylinder (18) is rotatably connected and arranged in the reaction box (14), the intermittent cylinder (18) is positioned at the end part of the connecting pipe (16), the intermittent cylinder (18) is of a structure with two ends penetrating, and the side wall of the intermittent cylinder (18) is provided with an intermittent hole (21).
2. A production apparatus for creatine monohydrate according to claim 1, characterized in that: four groups of connecting rods (20) are arranged on the inner wall of the intermittent cylinder (18) at equal angles, the intermittent cylinder (18) is externally connected with a driving motor, the connecting rods (20) are fixed with an output shaft of an external motor, and the rotating speed of the external motor is one tenth of that of the first motor (1).
3. A production plant for creatine monohydrate according to claim 1, characterized in that: stirring piece (3) are connected with connecting block (22) respectively including connecting block (22), stirring strip (23), horizontal bar (24) at stirring strip (23) both ends, and stirring strip (23) are circular-arc setting, multiunit stirring strip (23) wait angle setting, and be provided with horizontal bar (24) between two sets of adjacent stirring strip (23).
4. A production plant for creatine monohydrate according to claim 1, characterized in that: the end part of the connecting pipe (16) is provided with an arc groove, and the side wall of the intermittent cylinder (18) is attached to the arc groove of the connecting pipe (16) to form a blocking structure.
5. A production plant for creatine monohydrate according to claim 1, characterized in that: the central angle corresponding to the arc length of the discontinuous hole (21) is not less than 90 degrees.
6. A production plant for creatine monohydrate according to claim 1, characterized in that: gaps are reserved between the two ends of the intermittent cylinder (18) and the inner wall of the reaction box (14).
7. A production plant for creatine monohydrate according to claim 1, characterized in that: the height of the pump body (11) is higher than that of the stirring rod (17), and the height of the connecting pipe (16) on the mixing box (2) is higher than that of the suction pipe (10).
8. A production plant for creatine monohydrate according to claim 1, characterized in that: the discharge pipe (5) is provided with an electromagnetic valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210941148.XA CN115253839A (en) | 2022-08-08 | 2022-08-08 | Production equipment for creatine monohydrate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210941148.XA CN115253839A (en) | 2022-08-08 | 2022-08-08 | Production equipment for creatine monohydrate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN115253839A true CN115253839A (en) | 2022-11-01 |
Family
ID=83749365
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210941148.XA Pending CN115253839A (en) | 2022-08-08 | 2022-08-08 | Production equipment for creatine monohydrate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115253839A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5642940A (en) * | 1995-03-21 | 1997-07-01 | Tecnorama S.R.L | Apparatus for the preparation of mixtures, especially dye solutions |
| CN209828844U (en) * | 2019-04-08 | 2019-12-24 | 登封市汇联磨料磨具有限公司 | Smelting device of semi-brittle corundum abrasive material |
| CN214810803U (en) * | 2021-02-22 | 2021-11-23 | 宁夏享誉生物科技有限公司 | Improved production equipment for creatine monohydrate |
| CN216572851U (en) * | 2021-12-13 | 2022-05-24 | 铁岭艾克斯农业科技有限公司 | Reaction extraction equipment of fulvic acid chelated fertilizer |
-
2022
- 2022-08-08 CN CN202210941148.XA patent/CN115253839A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5642940A (en) * | 1995-03-21 | 1997-07-01 | Tecnorama S.R.L | Apparatus for the preparation of mixtures, especially dye solutions |
| CN209828844U (en) * | 2019-04-08 | 2019-12-24 | 登封市汇联磨料磨具有限公司 | Smelting device of semi-brittle corundum abrasive material |
| CN214810803U (en) * | 2021-02-22 | 2021-11-23 | 宁夏享誉生物科技有限公司 | Improved production equipment for creatine monohydrate |
| CN216572851U (en) * | 2021-12-13 | 2022-05-24 | 铁岭艾克斯农业科技有限公司 | Reaction extraction equipment of fulvic acid chelated fertilizer |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Gong Jiayong Inventor after: Gong Jiaxue Inventor after: Cheng Xuerui Inventor before: Zhang Yuekai Inventor before: Gong Jiayong |
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| CB03 | Change of inventor or designer information |