CN214597303U

CN214597303U - Distillation plant is used in processing of trimethyl phosphate

Info

Publication number: CN214597303U
Application number: CN202022316131.4U
Authority: CN
Inventors: 张�杰; 蔡兴爽; 谭成俊; 鲁建明
Original assignee: Shiyan Yuchen Biotechnology Co ltd
Current assignee: Shiyan Yuchen Biotechnology Co ltd
Priority date: 2020-10-18
Filing date: 2020-10-18
Publication date: 2021-11-05
Anticipated expiration: 2030-10-18

Abstract

The utility model relates to the technical field of distillation, and discloses a distillation device for trimethyl phosphate processing, which comprises an installation table, wherein the top of the installation table is fixedly connected with a distillation box, the top of the distillation box is provided with an exhaust port, the bottom of an agitator is fixedly provided with a motor, the rotating end of the motor runs through the bottom of the agitator, the distillation box and the inner part of the outer wall of the condensing box are respectively provided with a mounting groove, the top of the condensing box is provided with a condensed water inlet, the right side of the condensing box is provided with a condensed water outlet, the top of the condensing pipe is connected with the condensed water inlet, the bottom of the condensing pipe is connected with the condensed water outlet, the bottom of the condensing box is fixedly connected with a discharging pipe, the novel proposal can directly filter raw materials in the process of flowing to the distillation box by pouring the raw materials into a filter valve, thereby improving the distillation quality and improving the working efficiency.

Description

Distillation plant is used in processing of trimethyl phosphate

Technical Field

The utility model belongs to the technical field of the distillation, specifically be a distillation plant is used in trimethyl phosphate processing.

Background

The separation of different boiling point materials is realized through the method of distillation in the production process to current chemical industry enterprise and pharmacy enterprise, need use distillation plant in the distillation separation process, and traditional distillation plant structural design is reasonable inadequately, and in distillation process, adopt the distillation method to separate to the high boiling point impurity of easy separation, adopt the rectification method to separate to the low boiling point impurity of separating more difficult.

In the use process of the existing distillation device, the sealing cover is complicated in steps when being sealed, air tightness needs to be checked repeatedly, an installer is prone to making mistakes when being sealed, normal use of the distillation device is affected, continuous distillation cannot be carried out on the distillation device, and therefore the overall working efficiency of the distillation device is reduced.

SUMMERY OF THE UTILITY MODEL

To the above situation, for overcoming prior art's defect, the utility model provides a distillation plant is used in trimethyl phosphate processing, the effectual current distillation plant of having solved is in the use, because sealed lid is loaded down with trivial details when sealed, and needs the repeated check gas tightness, and the installer makes mistakes easily when sealed, influences distillation plant's normal use, and distillation plant can't carry out the distillation of continuity, leads to the problem that the holistic work efficiency of distillation plant reduces.

In order to achieve the above object, the utility model provides a following technical scheme: a distillation device for trimethyl phosphate processing comprises an installation table, wherein a distillation box is fixedly connected to the top of the installation table, an exhaust port is formed in the top of the distillation box, a stirring barrel is arranged inside the distillation box, a motor is fixedly installed at the bottom of the stirring barrel, the rotating end of the motor penetrates through the bottom of the stirring barrel, a stirring rod is rotatably connected inside the stirring barrel, a stirring blade is fixedly connected to the outer wall of the stirring rod, the transmission end of the motor is connected with the bottom end of the stirring rod, a filter valve is fixedly connected to the left side of the distillation box, a steam distributor is fixedly connected to the top of the inner cavity of the distillation box, a condensation box is fixedly connected to the top of the installation table, a flow transmission pipe is fixedly connected to the viewing side of the distillation box and the condensation box, and installation grooves are formed in the outer walls of the distillation box and the condensation box, the inner chamber of condensing box is provided with the condenser pipe, the comdenstion water import has been seted up at the top of condensing box, the comdenstion water export has been seted up on the right side of condensing box, the top of condenser pipe with the comdenstion water import is connected, the bottom of condenser pipe with the comdenstion water export is connected, the bottom fixedly connected with discharging pipe of condensing box.

Preferably, the exhaust port and the top of the filter valve are both movably connected with sealing covers, and the outer wall of the flow transmission pipe is provided with an adjusting valve.

Preferably, the agitator with the inside mounting groove that all is equipped with of condensation box outer wall, the inside of mounting groove evenly is equipped with the electromagnetic shaker.

Preferably, the inside of the filter valve is movably connected with a filter barrel, the outer wall of the filter barrel is uniformly provided with filter holes, and the bottom of the filter valve is connected with a valve cover in a threaded manner.

Preferably, the steam diffuser is uniformly and fixedly connected inside the steam diffuser, and the outer wall of the steam diffuser is uniformly provided with steam nozzles.

Preferably, the top end of the distillation box is inserted with a heat conduction pipe, and the top of the heat conduction pipe is fixedly connected with a thermometer.

Compared with the prior art, the beneficial effects of the utility model are that:

1. through pouring the raw materials into the filtering valve, make its raw materials at the in-process that flows to the distillation case, directly filter to improve the quality of distillation, improve work efficiency.

2. Make steam pass through steam jet blowout through starting steam distributor to make in the rapid distilling box that is full of steam, through starter motor, make the puddler rotate, stir the raw materials, thereby obtain abundant volatilizing, make it turn into gas rapidly, thereby improve work efficiency.

3. Make gaseous inflow condensing box in through opening the governing valve, through pouring into the condensate into to the condenser pipe to react gas through the condenser pipe, thereby make gaseous rapid condensation for liquid, thereby make the liquid of condensing box inner wall drop through starting the electromagnetic shaker, thereby more abundant collection is collected liquid through opening the discharging pipe at last.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention.

In the drawings:

fig. 1 is a schematic structural view of the present invention;

FIG. 2 is a cross-sectional view of the filter valve of the present invention;

fig. 3 is a schematic structural view of the steam dispenser of the present invention.

In the figure: 100. installing a table; 200. a distillation box; 201. an exhaust port; 202. a stirring barrel; 203. a motor; 204. a stirring rod; 205. stirring blades; 206. mounting grooves; 207. a vibrator; 300. a filter valve; 301. A filter vat; 302. a valve cover; 400. a vapor emanator; 401. a vapor diffusion tube; 402. a steam nozzle; 500. a flow transfer tube; 501. adjusting a valve; 600. a condenser tank; 700. a condenser tube; 701. a condensed water inlet; 702. a condensed water outlet; 703. a discharge pipe; 800. a heat conducting pipe.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments; based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

In the first embodiment, as shown in fig. 1, 2 and 3, the present invention includes a mounting table 100, a distillation tank 200 is fixedly connected to the top of the mounting table 100, an exhaust port 201 is formed at the top of the distillation tank 200, a stirring barrel 202 is disposed inside the distillation tank 200, a motor 203 is fixedly mounted at the bottom of the stirring barrel 202, a rotating end of the motor 203 penetrates through the bottom of the stirring barrel 202, a stirring rod 204 is rotatably connected to the inside of the stirring barrel 202, a stirring blade 205 is fixedly connected to the outer wall of the stirring rod 204, a driving end of the motor 203 is connected to the bottom end of the stirring rod 204, a filter valve 300 is fixedly connected to the left side of the distillation tank 200, a steam emitter 400 is fixedly connected to the top of the inner cavity of the distillation tank 200, a condensing tank 600 is fixedly connected to the top of the mounting table 100, a flow transmission pipe 500 is fixedly connected to the viewing side of the distillation tank 200 and the condensing tank 600, mounting grooves 206 are formed inside the outer walls of the distillation tank 200 and the condensing tank 600, the inner chamber of condensing box 600 is provided with condenser pipe 700, and condensate inlet 701 has been seted up at the top of condensing box 600, and condensate outlet 702 has been seted up on the right side of condensing box 600, and the top of condenser pipe 700 is connected with condensate inlet 701, and the bottom of condenser pipe 700 is connected with condensate outlet 702, and the bottom fixedly connected with discharging pipe 703 of condensing box 600.

In the second embodiment, on the basis of the first embodiment, as shown in fig. 1, sealing covers are movably connected to the top portions of the exhaust port 201 and the filter valve 300, and an adjusting valve 501 is disposed on the outer wall of the flow pipe 500, so that a user can control the flow of gas more easily.

Third embodiment, on the basis of the first embodiment, as shown in fig. 1, the inner portions of the outer walls of the stirring barrel 202 and the condensing box 600 are both provided with mounting grooves 206, and vibrators 207 are uniformly arranged inside the mounting grooves 206, so that the inner wall of the stirring barrel 202 and the inner wall of the condensing box 600 are vibrated, and the excess material on the inner wall is convenient to fall down.

In the fourth embodiment, based on the first embodiment, as shown in fig. 2, a filter barrel 301 is movably connected inside the filter valve 300, filter holes are uniformly formed in the outer wall of the filter barrel 301, a valve cover 302 is screwed to the bottom of the filter valve 300, the valve cover 302 can be opened, and the filter barrel 301 can be taken out and cleaned, so that the expected filtering rate is increased.

Fifth embodiment, on the basis of the first embodiment, as shown in fig. 3, a steam diffusion pipe 401 is uniformly and fixedly connected to the inside of the steam distributor 400, and steam nozzles 402 are uniformly formed on the outer wall of the steam diffusion pipe 401, so that steam is sprayed more uniformly, and the distillation rate is increased.

Sixth embodiment, as shown in fig. 1, in addition to the first embodiment, the heat conducting pipe 800 is inserted into the top of the distillation box 200, and the thermometer is fixedly connected to the top of the heat conducting pipe 800, so that the temperature inside the distillation box 200 can be more intuitively reflected, and a user can more intuitively control the temperature of the distillation box 200.

The working principle is as follows: when the novel scheme is implemented, the raw material is poured into the filter valve 300, the raw material is directly filtered in the process of flowing to the distillation box 200, so that the distillation quality is improved, the working efficiency is improved, steam is sprayed out through the steam nozzle 402 by starting the steam distributor 400, so that the steam is quickly filled in the inner cavity of the distillation box 200, the stirring rod 204 is rotated by starting the motor 203 to stir the raw material, so that the raw material is fully volatilized and quickly changed into gas, so that the working efficiency is improved, the gas flows into the condensation box 600 by opening the regulating valve 501, the condensate is injected into the condensation pipe 700, so that the gas is cooled and reacted through the condensation pipe 700, so that the gas is quickly condensed into liquid, the liquid on the inner wall of the condensation box 600 is quickly dropped by starting the vibrator 207, so that more sufficient collection can be realized, finally, the liquid is collected by opening the outlet pipe 703.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A trimethyl phosphate processing distillation plant which is characterized in that: comprises a mounting table (100), a distillation box (200) is fixedly connected to the top of the mounting table (100), an exhaust port (201) is formed in the top of the distillation box (200), a stirring barrel (202) is arranged in the distillation box (200), a motor (203) is fixedly mounted at the bottom of the stirring barrel (202), the rotating end of the motor (203) penetrates through the bottom of the stirring barrel (202), a stirring rod (204) is rotatably connected to the inside of the stirring barrel (202), a stirring blade (205) is fixedly connected to the outer wall of the stirring rod (204), the transmission end of the motor (203) is connected with the bottom end of the stirring rod (204), a filter valve (300) is fixedly connected to the left side of the distillation box (200), a steam distributor (400) is fixedly connected to the top of the inner cavity of the distillation box (200), and a condensing box (600) is fixedly connected to the top of the mounting table (100), distillation case (200) with what condensing case (600) looked looks side fixedly connected with flow tube (500), distillation case (200) with inside mounting groove (206) that all is equipped with of condensing case (600) outer wall, the inner chamber of condensing case (600) is provided with condenser pipe (700), condensate inlet (701) have been seted up at the top of condensing case (600), condensate outlet (702) have been seted up on the right side of condensing case (600), the top of condenser pipe (700) with condensate inlet (701) are connected, the bottom of condenser pipe (700) with condensate outlet (702) are connected, the bottom fixedly connected with discharging pipe (703) of condensing case (600).

2. The distillation apparatus for trimethyl phosphate processing according to claim 1, wherein: the exhaust port (201) and the top of the filter valve (300) are movably connected with sealing covers, and the outer wall of the flow transmission pipe (500) is provided with an adjusting valve (501).

3. The distillation apparatus for trimethyl phosphate processing according to claim 1, wherein: the stirring barrel (202) and the interior of the outer wall of the condensing box (600) are both provided with mounting grooves (206), and vibrators (207) are uniformly arranged in the mounting grooves (206).

4. The distillation apparatus for trimethyl phosphate processing according to claim 1, wherein: the inside swing joint of filter valve (300) has filter vat (301), the outer wall of filter vat (301) has evenly seted up the filtration hole, the bottom spiro union of filter valve (300) has valve gap (302).

5. The distillation apparatus for trimethyl phosphate processing according to claim 1, wherein: the inside of the steam distributor (400) is uniformly and fixedly connected with a steam diffusion pipe (401), and the outer wall of the steam diffusion pipe (401) is uniformly provided with steam nozzles (402).

6. The distillation apparatus for trimethyl phosphate processing according to claim 1, wherein: the top end of the distillation box (200) is inserted with a heat conduction pipe (800), and the top of the heat conduction pipe (800) is fixedly connected with a thermometer.