CN214131715U - Steam distillation equipment - Google Patents
Steam distillation equipment Download PDFInfo
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- CN214131715U CN214131715U CN202022547785.8U CN202022547785U CN214131715U CN 214131715 U CN214131715 U CN 214131715U CN 202022547785 U CN202022547785 U CN 202022547785U CN 214131715 U CN214131715 U CN 214131715U
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Abstract
The utility model relates to a distillation technology field specifically provides a steam distillation equipment. Distillation plant includes heating vaporization equipment, condensation splitter and the cooling subassembly that condenses, heating vaporization equipment and condensation splitter pass through the pipeline intercommunication, the cooling subassembly that condenses includes cooling condensation pipeline and refrigerating plant, set up fluid drive arrangement on the cooling condensation pipeline, refrigerating plant's inlet warp the cooling condensation pipeline with heating vaporization equipment's material pipe reaches condensation splitter's coolant outlet intercommunication, refrigerating plant's liquid outlet warp the cooling condensation pipeline with condensation splitter's coolant import intercommunication. The utility model discloses utilize the sublimation of compound and the separation of azeotropic sublimation realization high purity, the coolant that relates is the best water of affinity, adopts the recycling mode, can do the minimum in the aspect of the environmental pollution, reaches energy saving and emission reduction purpose.
Description
Technical Field
The utility model relates to a distillation technical field especially relates to a steam distillation equipment.
Background
In chemical experiments, materials are often encountered which are difficult to separate or purify in high purity by conventional methods, wherein some of the materials have special properties (such as being easily sublimable by heat, azeotroping with a particular solvent, or being miscible with solvent vapor to form material vapor). In view of the special properties of the materials, the purpose of high-efficiency separation can be achieved by steam distillation by utilizing the properties of the materials, convenience can be provided for vast chemical workers, and environmental pollution caused by the use of other solvents can be reduced.
SUMMERY OF THE UTILITY MODEL
In view of the above-mentioned disadvantages of the prior art, it is an object of the present invention to provide a steam distillation apparatus for solving the problems of the prior art.
For above-mentioned purpose and other relevant purposes realize, the utility model provides a steam distillation equipment, distillation equipment includes heating vaporization equipment, condensation splitter and the cooling subassembly that condenses, heating vaporization equipment and condensation splitter pass through the pipeline intercommunication, the cooling subassembly that condenses includes the cooling pipeline and refrigerating plant that condenses, the cooling sets up fluid drive arrangement on the road, refrigerating plant's inlet warp the cooling pipeline that condenses with heating vaporization equipment's material pipe reaches condensation splitter's coolant outlet intercommunication, refrigerating plant's liquid outlet warp the cooling pipeline that condenses with condensation splitter's coolant import intercommunication.
Optionally, the heating vaporization equipment comprises a reaction kettle, a stirrer and a heating jacket, the stirrer is provided with a stirring paddle and a driving motor, the driving motor is in transmission connection with the stirring paddle to provide power for the stirring paddle, the stirring paddle is located in an inner cavity of the reaction kettle, the heating jacket is arranged on a shell of the reaction kettle, the reaction kettle is communicated with the condensation separation equipment through a pipeline, and the reaction kettle is communicated with the refrigerating device through a pipeline.
Optionally, reation kettle includes material pipe, nitrogen gas pipe, drain hole and air-blowing circle, the nitrogen gas pipe with the material pipe all is located reation kettle's upper segment, the drain hole is located reation kettle bottom, the air-blowing circle is located reation kettle's inner chamber, the air-blowing circle pass through the pipeline with the nitrogen gas pipe intercommunication.
Optionally, condensation splitter includes a jar body, sprinkling equipment and filtration equipment, the sprinkling equipment is located the upper segment of jar body inner chamber, filtration equipment is located the hypomere of jar body inner chamber, the lateral wall of the jar is equipped with steam inlet, condensation splitter warp steam inlet with heating vaporization equipment's reation kettle intercommunication, jar body bottom is located in the coolant outlet, jar body warp the coolant outlet with refrigerating plant intercommunication, the coolant inlet is located the sprinkling equipment top, the sprinkling equipment warp the coolant inlet with refrigerating plant intercommunication.
Optionally, the tank body comprises a nitrogen outlet and a material crystallization outlet, the nitrogen outlet is located at the top of the tank body, and the material crystallization outlet is located at the middle-lower section of the tank.
As mentioned above, the utility model relates to a steam distillation equipment has following beneficial effect:
1) the utility model discloses a separation mode utilizes material azeotropic sublimation or sublimation can obtain high-purity material, and this separation mode has very strong specificity.
2) The utility model discloses a cooling medium that steam distillation related is the best water of affinity, adopts the recycling mode, can do the minimum in the aspect of the environmental pollution, reaches energy saving and emission reduction purpose.
3) The material can be purified for a plurality of times in the utility model, and the yield of the material is improved.
Drawings
FIG. 1 is a schematic view showing the structure of a steam distillation apparatus.
Fig. 2 is a schematic view showing the structure of the heating vaporization apparatus.
FIG. 3 is a schematic diagram of a condensing and separating apparatus.
Description of the element reference numerals
1 heating vaporization apparatus
11 reaction kettle
111 material pipe
112 nitrogen gas pipe
113 material port
114 discharge port
115 air blowing ring
12 stirrer
121 driving motor
122 stirring paddle
2 condensation separation equipment
21 can body
211 nitrogen outlet
212 inlet for cooling medium
213 Material crystallization Outlet
214 outlet for cooling medium
215 steam inlet
22 shower device
23 Filter device
3 Cooling and condensing assembly
31 cooling condensation pipeline
32 fluid driving device
33 refrigerating device
Detailed Description
The following description of the embodiments of the present invention is provided for illustrative purposes, and other advantages and effects of the present invention will be readily apparent to those skilled in the art from the disclosure herein. The present invention can also be implemented or applied through other different specific embodiments, and various details in the present specification can be modified or changed based on different viewpoints and applications without departing from the spirit of the present invention.
Please refer to fig. 1. It should be noted that the drawings provided in the present embodiment are only for illustrating the basic idea of the invention in a schematic manner, and only the components related to the invention are shown in the drawings rather than being drawn according to the number, shape and size of the components in actual implementation, and the form, quantity and proportion of the components in actual implementation may be changed at will, and the layout of the components may be more complicated.
As shown in fig. 1, a steam distillation apparatus includes a heating vaporization apparatus 1, a condensation separation apparatus 2 and a cooling condensation assembly 3, the heating vaporization apparatus 1 and the condensation separation apparatus 2 are communicated through a pipeline, the cooling condensation assembly 3 includes a cooling condensation pipeline 31 and a refrigeration device 33, a fluid driving device 32 is arranged on the cooling condensation pipeline 31, a liquid inlet of the refrigeration device 33 is communicated with a material pipe 111 of the heating vaporization apparatus 1 and a cooling medium outlet 214 of the condensation separation apparatus 2 through the cooling condensation pipeline 31, and a liquid outlet of the refrigeration device 33 is communicated with a cooling medium inlet 212 of the condensation separation apparatus 2 through the cooling condensation pipeline 31.
The utility model discloses a heating vaporization equipment 1 can carry out heat treatment to the material and make its liter change or azeotropic sublimation. During the use, the material gets into heating vaporization equipment 1 and forms material steam, and partial material steam gets into condensation splitter 2 through the pipeline and cools off the desublimation, and the separation obtains high-purity material and separation mother liquor, and partial material steam and separation mother liquor circulate and get into condensation splitter 2 after cooling through refrigerating plant 33 together, and the separation mother liquor gets into heating vaporization equipment 1 through cooling condensation pipeline 31 and material pipe 111 and can improve the yield of material. The design of the cooling and condensing assembly 3 can improve the use efficiency of the cooling medium and the yield of the material, and also realize the high-purity separation of the material through sublimation or azeotropic sublimation. When the added material is a solid-liquid mixture, the high-purity separation of the material is realized through azeotropic sublimation.
As shown in fig. 2, in an embodiment, the heating vaporization apparatus 1 includes a reaction kettle 11, a stirrer 12, and a heating jacket, where the stirrer 12 is provided with a stirring paddle 122 and a driving motor 121, the driving motor 121 is in transmission connection with the stirring paddle 122 for providing power to the stirring paddle 122, the stirring paddle 122 is located in an inner cavity of the reaction kettle 11, the heating jacket is located on a shell of the reaction kettle 11, the reaction kettle 11 is communicated with the condensation separation apparatus 2 through a pipeline, and the reaction kettle 11 is communicated with the refrigeration apparatus 33 through a pipeline.
In this embodiment, the heating jacket provides heat energy for the heating vaporization device 1, so that the temperature of the reaction kettle 11 rises until the material in the reaction kettle 11 starts to boil and vaporize, the stirrer 12 stirs the material in the reaction kettle 11, the driving motor 121 drives the stirring paddle 122 to stir the material, the material is uniformly dispersed, and the phenomenon that material crystals are retained at the bottom of the reaction kettle 11 due to too high uniform concentration is prevented.
Preferably, the paddle of the stirring paddle 122 is located at the lower section of the inner cavity of the reaction kettle 11. Is favorable for the even dispersion of the materials and prevents the materials from being retained at the bottom of the reaction kettle 11.
In an embodiment, the reaction kettle 11 includes a material pipe 111, a nitrogen gas pipe 112, a discharge port 114, and an air blowing ring 115, the nitrogen gas pipe 112 and the material pipe 111 are both located at an upper section of the reaction kettle 11, the discharge port 114 is located at the bottom of the reaction kettle 11, the air blowing ring 115 is located in an inner cavity of the reaction kettle 11, and the air blowing ring 115 is communicated with the nitrogen gas pipe 112.
In this embodiment, the material enters the inner cavity of the reaction kettle 11 through the material pipe 111, nitrogen enters the air blowing ring 115 through the nitrogen pipe 112, and is then discharged into the inner cavity of the reaction kettle 11 through the air blowing ring 115 to form an air flow, the material pipe 111 is used for feeding the material, the discharge port 114 is used for discharging distilled waste materials, the material pipe 111 is communicated with the cooling condensation pipeline 31, and the reaction kettle 11 is communicated with the refrigerating device 33 through the material pipe 111.
Preferably, the balloon 115 is provided with a plurality of holes. The plurality of air holes are convenient for slowly releasing nitrogen flow and dispersing materials, and the phenomenon that the materials splash due to the fact that the nitrogen flow speed is high because of too few air holes is prevented.
Preferably, the balloon 115 is located below the paddle 122. Is favorable for dispersing materials.
In an embodiment, the material pipe 111 is provided with a material port 113, and the material port 113 is located at an upper section of an inner cavity of the reaction kettle 11. The material enters the material pipe 111 and enters the inner cavity of the reaction kettle 11 through the material port 113.
As shown in fig. 2, in an embodiment, the condensation separation device 2 includes a tank 21, a shower device 22 and a filtering device 23, the shower device 22 is located at an upper section of an inner cavity of the tank 21, the filtering device 23 is located at a lower section of the inner cavity of the tank 21, a steam inlet 215 is provided on a side wall of the tank 21, the condensation separation device 2 is communicated with the reaction kettle 11 of the heating and vaporization device 1 through the steam inlet 215, the cooling medium outlet 214 is provided at a bottom of the tank 21, the tank 21 is communicated with the refrigeration device 33 through the cooling medium outlet 214, the cooling medium inlet 212 is located at a top of the shower device 22, and the shower device 22 is communicated with the refrigeration device 33 through the cooling medium inlet 212.
In this embodiment, the material is heated in the inner cavity of the reaction vessel 11 to become material vapor, and enters the inner cavity of the tank 21 of the condensation separation apparatus 2 through the steam inlet 215 via the pipeline between the reaction vessel 11 and the tank 21, the cooling water enters the shower apparatus 22 in the inner cavity of the tank 21 through the cooling condensation pipeline 31 via the cooling medium inlet 212, the shower apparatus 22 sprays the cooling water to mix with the material vapor, so as to reduce the temperature of the material vapor, a part of the material vapor can be condensed into a high-purity material and stays on the surface of the filter apparatus 23, a part of the material vapor can be liquefied into a cooling medium, and the cooling medium enters the refrigeration apparatus 33 through the cooling medium outlet 214 via the cooling condensation pipeline 31, and then circularly enters the condensation separation apparatus 2 again after being cooled by the refrigeration apparatus 33.
Preferably, the shower device 22 is located above the steam inlet 215. The cooling water sprayed by the showering device 22 is in sufficient contact with the material vapor to prevent the material vapor from escaping.
Preferably, the filtering device 23 is located below the steam inlet 215. The coagulated high purity material is collected.
In one embodiment, the tank 21 includes a nitrogen outlet 211 and a material crystallization outlet 213, wherein the nitrogen outlet 211 is located at the top of the tank 21, and the material crystallization outlet 213 is located at the middle-lower section of the tank 21. In this embodiment, the material crystallization outlet 213 is used to obtain high purity material crystals from the inside of the tank 21.
In one embodiment, the fluid driving device 32 is a pump, and the pump may be provided in plurality.
Preferably, the fluid driving device 32 is disposed between the liquid outlet of the refrigeration device 33 and the cooling medium inlet 212, and specifically, the fluid driving device 32 is a pump for driving the cooling medium into the condensation separation apparatus 2.
Preferably, a fluid driving device 32 is disposed between the cooling medium outlet 214 and the material port 113, and specifically, the fluid driving device 32 is a pump. The material steam enters the condensation separation device 2 through a pipeline for cooling and desublimation, the high-purity material and the separated mother liquor are obtained through separation, the separated mother liquor provides driving force through the fluid driving device 32, enters the inner cavity of the reaction kettle 11 through the cooling and condensation pipeline 31 and the material pipe 111 through the material port 113, the separated mother liquor and the material are changed into the material steam together, high-purity material crystallization is obtained through desublimation crystallization again, and the yield of the material is improved.
To sum up, the utility model discloses various shortcomings in the prior art have effectively been overcome and high industry value has.
The above embodiments are merely illustrative of the principles and effects of the present invention, and are not to be construed as limiting the invention. Modifications and variations can be made to the above-described embodiments by those skilled in the art without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which may be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.
Claims (10)
1. A steam distillation apparatus, characterized by: distillation plant is including heating vaporization equipment (1), condensation splitter (2) and cooling condensation subassembly (3), heating vaporization equipment (1) and condensation splitter (2) pass through the pipeline intercommunication, cooling condensation subassembly (3) are including cooling condensation pipeline (31) and refrigerating plant (33), set up fluid drive arrangement (32) on cooling condensation pipeline (31), the inlet warp of refrigerating plant (33) cooling condensation pipeline (31) with material pipe (111) of heating vaporization equipment (1) and cooling medium export (214) intercommunication of condensation splitter (2), the liquid outlet warp of refrigerating plant (33) cooling condensation pipeline (31) with cooling medium import (212) intercommunication of condensation splitter (2).
2. A steam distillation apparatus according to claim 1, wherein: heating vaporization equipment (1) includes reation kettle (11), agitator (12) and heating jacket, agitator (12) are provided with stirring rake (122) and driving motor (121), driving motor (121) are connected with stirring rake (122) transmission and provide power for stirring rake (122), stirring rake (122) are located reation kettle (11)'s inner chamber, the heating jacket is located on reation kettle (11)'s the casing, reation kettle (11) through the pipeline with condensation splitter (2) intercommunication, reation kettle (11) with refrigerating plant (33) pass through the pipeline intercommunication.
3. A steam distillation apparatus according to claim 2, wherein: the paddle of the stirring paddle (122) is positioned at the lower section of the inner cavity of the reaction kettle (11).
4. A steam distillation apparatus according to claim 2, wherein: reation kettle (11) include material pipe (111), nitrogen gas pipe (112), drain hole (114) and air-blowing circle (115), nitrogen gas pipe (112) with material pipe (111) all are located reation kettle (11)'s upper segment, drain hole (114) are located reation kettle (11)'s bottom, air-blowing circle (115) are located reation kettle (11)'s inner chamber, air-blowing circle (115) with nitrogen gas pipe (112) intercommunication.
5. A steam distillation apparatus according to claim 4, comprising one or more of the following features: the balloon (115) is provided with a plurality of holes;
the material pipe (111) is provided with a material port (113), and the material port (113) is located at the upper section of the inner cavity of the reaction kettle (11).
6. A steam distillation apparatus according to claim 4, wherein: the air blowing ring (115) is positioned below the paddle (122) of the stirring paddle.
7. A steam distillation apparatus according to claim 1, wherein: the condensation separation equipment (2) comprises a tank body (21), sprinkling equipment (22) and filtering equipment (23), the shower equipment (22) is positioned at the upper section of the inner cavity of the tank body (21), the filtering equipment (23) is positioned at the lower section of the inner cavity of the tank body (21), the side wall of the tank body (21) is provided with a steam inlet (215), the condensation separation equipment (2) is communicated with a reaction kettle (11) of the heating vaporization equipment (1) through the steam inlet (215), the cooling medium outlet (214) is arranged at the bottom of the tank body (21), the tank body (21) is communicated with the refrigerating device (33) through the cooling medium outlet (214), the cooling medium inlet (212) is located at the top of the shower device (22), the shower device (22) communicates with the refrigeration device (33) via the cooling medium inlet (212).
8. A steam distillation apparatus according to claim 7, wherein: the tank body (21) comprises a nitrogen outlet (211) and a material crystallization outlet (213), the nitrogen outlet (211) is positioned at the top of the tank body (21), and the material crystallization outlet (213) is positioned at the middle lower section of the tank body (21).
9. A steam distillation apparatus according to claim 1, wherein: the fluid drive device (32) is a pump, and the pump may be provided in plurality.
10. A steam distillation apparatus according to claim 5, comprising one or more of the following features:
the fluid driving device (32) is arranged between the liquid outlet of the refrigerating device (33) and the cooling medium inlet (212);
the fluid driving device (32) is arranged between the cooling medium outlet (214) and the material port (113).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022547785.8U CN214131715U (en) | 2020-11-06 | 2020-11-06 | Steam distillation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022547785.8U CN214131715U (en) | 2020-11-06 | 2020-11-06 | Steam distillation equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214131715U true CN214131715U (en) | 2021-09-07 |
Family
ID=77562449
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022547785.8U Active CN214131715U (en) | 2020-11-06 | 2020-11-06 | Steam distillation equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214131715U (en) |
-
2020
- 2020-11-06 CN CN202022547785.8U patent/CN214131715U/en active Active
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP02 | Change in the address of a patent holder | ||
| CP02 | Change in the address of a patent holder |
Address after: 243000 About 100 meters south of the intersection of Dianye Road and Tianmen Avenue, Cihu High tech Zone, Ma'anshan City, Anhui Province Patentee after: Anhui Haoyuan Pharmaceutical Co.,Ltd. Address before: 243000 No. 1669, North Section of Huolishan Avenue, Cihu High-tech Zone, Ma'anshan City, Anhui Province Patentee before: Anhui Haoyuan Pharmaceutical Co.,Ltd. |
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| CP02 | Change in the address of a patent holder | ||
| CP02 | Change in the address of a patent holder |
Address after: 243000 No. 1107, North Section of Tianmen Avenue, Cihu High tech Zone, Ma'anshan City, Anhui Province Patentee after: Anhui Haoyuan Pharmaceutical Co.,Ltd. Address before: 243000 About 100 meters south of the intersection of Dianye Road and Tianmen Avenue, Cihu High tech Zone, Ma'anshan City, Anhui Province Patentee before: Anhui Haoyuan Pharmaceutical Co.,Ltd. |