CN214075072U - External circulation evaporator easy to sample - Google Patents

External circulation evaporator easy to sample Download PDF

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Publication number
CN214075072U
CN214075072U CN202022398428.XU CN202022398428U CN214075072U CN 214075072 U CN214075072 U CN 214075072U CN 202022398428 U CN202022398428 U CN 202022398428U CN 214075072 U CN214075072 U CN 214075072U
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tank
sampling
separation tank
external circulation
easy
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CN202022398428.XU
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Chinese (zh)
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惠谦
魏哲
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Shaanxi Changtai Industrial Co ltd
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Shaanxi Changtai Industrial Co ltd
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Abstract

The utility model discloses an external circulation evaporator easy to sample, which comprises a heating tank and a separating tank, wherein a heat exchanger is arranged in the heating tank, and the bottom of the heating tank is provided with a feed liquid inlet and a concentrated liquid outlet; the upper part of the heating tank is connected with the separating tank through an upper circulating pipe, and the bottom of the heating tank is connected with the bottom of the separating tank through a lower circulating pipe; the separating tank is provided with a sampling valve. The utility model discloses technical scheme need not shut down, need not open the knockout drum after the pressure release for prior art's extrinsic cycle evaporimeter, can acquire the sample of concentrate in the knockout drum in real time in the evaporation and separation process, and then concentration detection has advantages such as detection speed is fast, do not influence production.

Description

External circulation evaporator easy to sample
Technical Field
The utility model relates to a concentrator field, concretely relates to outer circulation evaporator of easy appearance of getting.
Background
The common external circulation evaporator at present is not provided with a sampling structure, and the equipment with the structure has the following defects: the concentration of the concentrated solution can not be detected, and the phenomenon of excessive concentration is easy to occur, so that the coke tube can be blocked. The operation is inconvenient because multiple observations are needed; repeated reductions in steam pressure are required; the operation efficiency is low, resulting in unstable whole concentration operation. Whether the concentration of the concentrated solution reaches the standard or not can not be detected when the equipment works. The operation of the device is affected.
How to design an external circulation evaporator easy to sample is a technical problem which needs to be solved by the technical personnel in the field at present.
Disclosure of Invention
For solving the technical problem, the main objective of the utility model is to provide an easy appearance extrinsic cycle evaporimeter that draws a sample, the sample that can acquire the concentrate in real time in the evaporation and separation process detects concentration, prevents that concentration is excessive or concentrated not enough.
In order to achieve the above purpose, the present invention adopts the following technical solution.
An external circulation evaporator easy to sample comprises a heating tank and a separation tank, wherein a heat exchanger is arranged in the heating tank, and the bottom of the heating tank is provided with a feed liquid inlet and a concentrated liquid outlet; the upper part of the heating tank is connected with the separating tank through an upper circulating pipe, and the bottom of the heating tank is connected with the bottom of the separating tank through a lower circulating pipe; the separating tank is provided with a sampling valve.
Further, a sampling valve is positioned at the bottom of the lower circulating pipe.
Further, a sampling valve is located on the side wall of the separation tank.
Furthermore, the number of the sampling valves is three, and the sampling valves are respectively positioned at the bottom, the middle part and the upper part of the separation tank.
Further, the top of the separation tank is provided with a pressure gauge.
Further, a pressure release valve is arranged at the top of the separation tank.
Furthermore, a perspective window is arranged on the tank body of the separating tank.
Furthermore, the number of the perspective windows is three, and the perspective windows are respectively positioned at the bottom, the middle part and the upper part of the separation tank.
The utility model discloses technical scheme need not shut down, need not open the knockout drum after the pressure release for prior art's extrinsic cycle evaporimeter, can acquire the sample and the detection concentration of concentrate in the knockout drum in real time in the evaporation and separation process, have that detection speed is fast, do not influence advantages such as production.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed to be used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the structures shown in the drawings without creative efforts.
FIG. 1 is a schematic view of an external circulation evaporator for easy sampling according to the present invention;
in the above figures:
1 heating the tank; 2, separating the tank; 3, a feed liquid inlet; 4, a concentrated solution outlet; 5 an upper circulation pipe; 6 lower circulating pipes; 7 a sampling valve; 8, a pressure gauge; 9, a pressure relief valve; 10 a see-through window.
Detailed Description
In order to make the above objects, features and advantages of the present invention more comprehensible, embodiments accompanied with figures are described in detail below.
In the following description, specific details are set forth in order to provide a thorough understanding of the present invention. The invention can be implemented in a number of other ways than those described herein, and those skilled in the art will be able to make similar generalizations without departing from the spirit of the invention. The invention is therefore not limited to the specific embodiments disclosed below.
The common external circulation evaporator at present is not provided with a sampling structure, and the equipment with the structure has the following defects: the operation of the device is affected: the concentration of the concentrated solution can not be detected, and the phenomenon of excessive concentration is easy to occur, so that the coke tube can be blocked. The operation is inconvenient because multiple observations are needed; repeated reductions in steam pressure are required; the operation efficiency is low, resulting in unstable whole concentration operation. Whether the concentration of the concentrated solution reaches the standard or not can not be detected when the equipment works. The operation of the device is affected. The utility model provides an outer circulation evaporimeter of easily getting a sample.
Referring to fig. 1, an external circulation evaporator easy to sample comprises a heating tank 1 and a separation tank 2, wherein a heat exchanger is arranged in the heating tank 1, and a feed liquid inlet 3 and a concentrated liquid outlet 4 are arranged at the bottom of the heating tank 1; the upper part of the heating tank 1 is connected with the separation tank 2 through an upper circulating pipe 5, and the bottom of the heating tank 1 is connected with the bottom of the separation tank 2 through a lower circulating pipe 6; the separation tank 2 is provided with a sampling valve 7.
In the above embodiment, the evaporimeter contains heating jar 1 and knockout drum 2, sets up sample valve 7 on knockout drum 2, can obtain the concentrate sample and detect concentration in real time through opening sample valve 7 in the evaporimeter separation working process, prevents concentrated excessively or concentrated not enough, and then has avoided the mistake that stifled pipe, coke breeze pipe lead to.
Further, as an embodiment of the present invention, the sampling valve 7 is located at the bottom of the lower circulation pipe 6. Since the lower circulation pipe 6 is located at the bottom of the evaporator, the extracting solution is influenced by gravity, and the concentration of the bottom is highest, so that the maximum concentration of the sample in the whole separation tank 2 can be obtained by obtaining the sample of the concentrated solution at the bottom of the evaporator and detecting the concentration, and the concentrated solution in the whole separation tank 2 is not excessively concentrated as long as the concentration at the bottom of the separation tank 2 is not excessively concentrated.
Further, the sampling valve 7 is located on the side wall of the separation tank 2. The number of the sampling valves 7 is three, and the sampling valves are respectively positioned at the bottom, the middle part and the upper part of the separation tank 2.
In the above embodiment, in order to obtain the concentration of the concentrated solution in the whole separation tank 2, preferably, the sampling valves 7 are respectively arranged at the bottom, the middle part and the upper part of the separation tank 2, so that the average concentration in the whole separation tank 2 can be known more accurately, and the staff can conveniently grasp the concentration degree of the concentrated solution as a whole to prevent over-concentration or under-concentration.
Further, a pressure gauge 8 is arranged at the top of the separation tank 2. Preferably, the top of the separation tank 2 is provided with a pressure relief valve 9.
In the above embodiment, in order to reduce 2 internal pressures of knockout drum when taking a sample, prevent that the concentrate from spouting and hindering the people, set up manometer 8 at the top of knockout drum 2, can directly perceivedly obtain 2 internal pressures of knockout drum, if 2 internal pressures of knockout drum surpass safe sampling pressure, can release partly with 2 internal pressures of knockout drum through opening relief valve 9, treat that 2 internal pressures of knockout drum are in the safe range and open sampling valve 7 sample again.
Further, a perspective window 10 is arranged on the tank body of the separation tank 2. The number of the perspective windows 10 is three, and the perspective windows are respectively positioned at the bottom, the middle part and the upper part of the separation tank 2.
In the above embodiment, in order to facilitate the worker to know the height of the liquid level in the separation tank 2, the bottom, the middle part and the upper part of the separation tank 2 are respectively provided with the perspective windows 10, and the perspective windows 10 are made of high temperature resistant glass.
Although the invention has been described in detail in this specification with reference to specific embodiments and illustrative embodiments, it will be apparent to those skilled in the art that certain changes and modifications can be made therein without departing from the scope of the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.

Claims (8)

1. An external circulation evaporator easy to sample is characterized by comprising a heating tank (1) and a separating tank (2), wherein a heat exchanger is arranged in the heating tank (1), and a feed liquid inlet (3) and a concentrated liquid outlet (4) are arranged at the bottom of the heating tank (1); the upper part of the heating tank (1) is connected with the separation tank (2) through an upper circulating pipe (5), and the bottom of the heating tank (1) is connected with the bottom of the separation tank (2) through a lower circulating pipe (6); and a sampling valve (7) is arranged on the separation tank (2).
2. Easy-sampling external circulation evaporator according to claim 1, characterized in that the sampling valve (7) is located at the bottom of the lower circulation pipe (6).
3. Easy-sampling external circulation evaporator according to claim 1, characterized in that the sampling valve (7) is located on the side wall of the separation tank (2).
4. An easy-sampling external circulation evaporator according to claim 3, characterized in that the number of sampling valves (7) is three, respectively located at the bottom, middle and upper part of the separation tank (2).
5. Easy-sampling external circulation evaporator according to claim 1, characterized in that the top of the separation tank (2) is provided with a pressure gauge (8).
6. The external circulation evaporator with easy sampling according to claim 1 is characterized in that the top of the separation tank (2) is provided with a pressure relief valve (9).
7. The external circulation evaporator easy to sample according to claim 1, characterized in that the body of the separation tank (2) is provided with a perspective window (10).
8. The external circulation evaporator with easy sampling according to claim 7 is characterized in that the number of the perspective windows (10) is three, and the perspective windows are respectively positioned at the bottom, the middle and the upper part of the separation tank (2).
CN202022398428.XU 2020-10-26 2020-10-26 External circulation evaporator easy to sample Active CN214075072U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022398428.XU CN214075072U (en) 2020-10-26 2020-10-26 External circulation evaporator easy to sample

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202022398428.XU CN214075072U (en) 2020-10-26 2020-10-26 External circulation evaporator easy to sample

Publications (1)

Publication Number Publication Date
CN214075072U true CN214075072U (en) 2021-08-31

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202022398428.XU Active CN214075072U (en) 2020-10-26 2020-10-26 External circulation evaporator easy to sample

Country Status (1)

Country Link
CN (1) CN214075072U (en)

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