CN213933302U - A extraction element for glycerine detects - Google Patents

A extraction element for glycerine detects Download PDF

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Publication number
CN213933302U
CN213933302U CN202022886861.8U CN202022886861U CN213933302U CN 213933302 U CN213933302 U CN 213933302U CN 202022886861 U CN202022886861 U CN 202022886861U CN 213933302 U CN213933302 U CN 213933302U
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pipe
fixedly connected
thick bamboo
extraction
carbon powder
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CN202022886861.8U
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Chinese (zh)
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任凯
陈方毅
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Wuxi Nanmu Measurement And Control Technology Co ltd
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Wuxi Nanmu Measurement And Control Technology Co ltd
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Abstract

The utility model discloses an extraction element for glycerine detects, comprising a base plate, the last fixed surface of bottom plate is connected with the heating frame, and the last fixed surface of heating frame is connected with a distillation column, two fixed plates of the last fixed surface of bottom plate are connected with, and the top fixedly connected with of fixed plate takes off a color section of thick bamboo, a plurality of space bars of both sides inner wall fixedly connected with of a color section of thick bamboo, and the bottom inner wall fixedly connected with carbon dust filter screen of a color section of thick bamboo, carbon dust filter screen are located the space bar under, the last fixed surface of a color section of thick bamboo is connected with the motor, and the one end fixedly connected with dwang of motor output shaft, the one end of dwang is passed a color section of thick bamboo, and a plurality of agitators of one side fixedly connected with of dwang, the last surface swing joint of a color section of thick bamboo has the carbon dust pipe. The utility model discloses can filter the carbon dust in the solution after the decoloration to solved the problem that can not clear away the carbon dust, improved the efficiency of the purification of glycerine.

Description

A extraction element for glycerine detects
Technical Field
The utility model relates to a glycerine draws technical field, especially relates to an extraction element for glycerine detects.
Background
Glycerol production processes can be divided into two main categories: the method takes natural oil as raw material, the obtained glycerol is commonly called natural glycerol, the obtained glycerol is commonly called synthetic glycerol, the natural oil is still the main raw material for producing the glycerol, the production process of the natural glycerol comprises the refining processes of purifying and concentrating to obtain crude glycerol, distilling, decoloring and deodorizing the crude glycerol, and a glycerol detection and extraction device is needed in the extraction process of the glycerol.
The extraction device for glycerin detection is a glycerin extraction device specially used for detecting the glycerin content in vegetable oil, carbon powder is needed to be decolored in the glycerin extraction process, and the common extraction device for glycerin detection cannot remove the carbon powder after being decolored by the carbon powder, so that the glycerin purification efficiency is reduced, and the extraction device for glycerin detection is urgently needed.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing an extraction device for glycerin detection.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
an extraction device for glycerin detection comprises a base plate, wherein the upper surface of the base plate is fixedly connected with a heating frame, the upper surface of the heating frame is fixedly connected with a distillation barrel, the upper surface of the base plate is fixedly connected with two fixing plates, the top end of each fixing plate is fixedly connected with a decoloring barrel, the inner walls of the two sides of the decoloring barrel are fixedly connected with a plurality of partition plates, the inner wall of the bottom of the decoloring barrel is fixedly connected with a carbon powder filter screen, the carbon powder filter screen is positioned under the partition plates, the upper surface of the decoloring barrel is fixedly connected with a motor, one end of an output shaft of the motor is fixedly connected with a rotating rod, one end of the rotating rod penetrates through the decoloring barrel, one side of the rotating rod is fixedly connected with a plurality of stirrers, the upper surface of the decoloring barrel is movably connected with a carbon powder pipe, the top end of the carbon powder pipe is fixedly connected with a funnel, one side of the decoloring barrel is movably connected with a feed pipe, the upper surface of the base plate is fixedly connected with two support plates, the top end of the supporting plate is fixedly connected with a methanol cylinder, the bottom of the methanol cylinder is movably connected with a filling pipe, and one end of the filling pipe is spliced with the decoloring cylinder.
Preferably, one side fixedly connected with connecting plate of fixed plate, the last fixed surface of connecting plate is connected with the cartridge filter, and the both sides inner wall fixedly connected with of cartridge filter has a plurality of filter.
Preferably, the upper surface of the filter cylinder is movably connected with an extraction pipe, one side of the extraction pipe is fixedly connected with a water pump, the decolorizing cylinder is inserted with the extraction pipe, and the extraction pipe penetrates through the carbon powder filter screen.
Preferably, the upper surface of the distillation cylinder is movably connected with a connecting pipe and an exhaust pipe, and one end of the connecting pipe is movably connected with a filter cylinder.
Preferably, one side of the heating frame is provided with a heating pipe, and the distillation cylinder is positioned right above the heating pipe.
Preferably, one side of the distillation barrel is movably connected with a discharge pipe, and one side of the discharge pipe is movably connected with an electromagnetic valve.
Preferably, one side of the feeding pipe and one side of the filling pipe are respectively and movably connected with a first valve and a second valve.
The utility model has the advantages that:
1. the rotating rod is driven to rotate through the motor, and then the stirrer is driven to rotate, so that the mixed liquid of carbon powder and glycerin in the decoloring barrel is stirred, the mixed liquid of carbon powder and glycerin is fully merged in and out, the color in the mixed liquid of glycerin can be removed through the carbon powder, and the purpose of decoloring is achieved.
2. Through the arrangement of the carbon powder filter screen, carbon powder in the decolorized solution can be filtered, so that the problem that the carbon powder cannot be removed is solved, and the purification efficiency of the glycerol is improved.
3. Through the setting of cartridge filter and filter, can carry out further filtration to a small amount of carbon powder that methyl alcohol solution and glycerine mixed liquid contain to guarantee that the later stage draws clean glycerine, improved the purity that glycerine drawed.
Drawings
Fig. 1 is a schematic structural view of an extraction device for glycerin detection according to the present invention;
fig. 2 is a schematic cross-sectional structural diagram of an extraction device for glycerin detection according to the present invention;
fig. 3 is a schematic view of a partial structure of an extraction device for glycerin detection according to the present invention.
In the figure: 1. a base plate; 2. a heating rack; 3. heating a tube; 4. a distillation column; 5. a filter cartridge; 6. a decolorizing drum; 7. a methanol cartridge; 8. an electromagnetic valve; 9. a discharge pipe; 10. an exhaust pipe; 11. a connecting pipe; 12. a water pump; 13. an extraction pipe; 14. a filling pipe; 15. a feed pipe; 16. a support plate; 17. a fixing plate; 18. a filter plate; 19. a carbon powder tube; 20. a funnel; 21. a motor; 22. a stirrer; 23. a partition plate; 24. carbon powder filter screen.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. It should be noted that unless otherwise explicitly stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and their meaning in the context of this patent may be understood by those skilled in the art as appropriate.
Referring to fig. 1-3, an extraction device for glycerin detection comprises a base plate 1, a heating frame 2 is fixed on the upper surface of the base plate 1 through bolts, a distillation barrel 4 is fixed on the upper surface of the heating frame 2 through bolts, two fixing plates 17 are fixed on the upper surface of the base plate 1 through bolts, a decoloring barrel 6 is fixed on the top end of each fixing plate 17 through bolts, the fixing plates 17 support the decoloring barrel 6, a plurality of partition plates 23 are fixed on the inner walls of the two sides of the decoloring barrel 6 through bolts, separation holes are formed in the partition plates 23, the partition plates 23 are designed to block a mixed solution, so that the mixed solution slowly descends, the carbon powder and a glycerin mixed solution are fully contacted, and thus the decoloring is better performed, a filter screen 24 is fixed on the inner wall of the bottom of the decoloring barrel 6 through bolts, the design of the carbon powder filter screen 24 can filter the carbon powder in the decolored solution, thereby the problem that carbon powder can not be removed is solved, the efficiency of the purification of glycerin is improved, the carbon powder filter screen 24 is positioned under the partition plate 23, the upper surface of the decoloring barrel 6 is fixed with a motor 21 through a bolt, one end of an output shaft of the motor 21 is fixed with a rotating rod through a bolt, one end of the rotating rod passes through the decoloring barrel 6, one side of the rotating rod is fixed with a plurality of stirrers 22 through bolts, the motor 21 drives the rotating rod to rotate, and further drives the stirrers 22 to rotate, thereby the mixed liquid of the carbon powder and the glycerin in the decoloring barrel 6 is stirred, the mixed liquid of the carbon powder and the glycerin is fully fused in and out, thereby the color in the mixed liquid of the glycerin can be removed by the carbon powder, the purpose of decoloring is achieved, the carbon powder pipe 19 is inserted into the upper surface of the decoloring barrel 6, the funnel 20 is welded at the top end of the carbon, the upper surface of bottom plate 1 is fixed with two backup pads 16 through the bolt, and the top of backup pad 16 is fixed with a methyl alcohol section of thick bamboo 7 through the bolt, and methyl alcohol section of thick bamboo 7 is so that add the methyl alcohol solution, and the purpose of adding methyl alcohol is for extracting glycerine in the better mixed solution of later stage, and the bottom of methyl alcohol section of thick bamboo 7 is pegged graft and is had filling pipe 14, and one end and the decoloration section of thick bamboo 6 of filling pipe 14 are pegged graft mutually.
In the utility model, one side of the fixing plate 17 is fixed with a connecting plate through bolts, the upper surface of the connecting plate is fixed with a filter cartridge 5 through bolts, the inner walls of the two sides of the filter cartridge 5 are fixed with a plurality of filter plates 18 through bolts, the design of the filter cartridge 5 and the filter plates 18 can further filter a small amount of carbon powder contained in the mixed solution of methanol solution and glycerol, thereby ensuring the clean glycerol extracted at the later stage, improving the purity of glycerol extraction, and a plurality of through holes are arranged at the joints of each filter plate 18 and the filter cartridge 5, so that the solution can flow into the connecting pipe 11, the upper surface of the filter cartridge 5 is spliced with an extraction pipe 13, one side of the extraction pipe 13 is welded with a water pump 12, the decoloration cylinder 6 is spliced with the extraction pipe 13, and the extraction pipe 13 passes through a carbon powder filter screen 24, under the working pressure of the water pump 12, so that the methanol solution and the glycerol in the carbon powder filter screen 24 flow into the filter cartridge 5 through the extraction pipe 13, connecting pipe 11 and blast pipe 10 are pegged graft to the upper surface of distillation column 4, the one end of connecting pipe 11 is pegged graft and is had cartridge filter 5, heating pipe 3 has been cup jointed to one side of heating frame 2, the joining of heating pipe 3, can heat distillation column 4, make the temperature rise in distillation column 4, under the environment of high temperature, methanol decomposition, and producing steam in heating the evaporation process to solution, steam passes through blast pipe 10 and discharges, the solution of surplus in distillation column 4 is glycerine, distillation column 4 is located heating pipe 3 directly over, one side of distillation column 4 is pegged graft and is had discharging pipe 9, one side threaded connection of discharging pipe 9 has solenoid valve 8, open solenoid valve 8, make the glycerine of drawing out discharge pipe 9 discharge, one side threaded connection has first valve and second valve respectively of feeding pipe 15 and filling pipe 14.
The working principle is as follows: when the device is used, firstly, the reacted glycerol mixed liquid is added into the decolorizing cylinder 6 through the feeding pipe 15, the reacted glycerol mixed liquid is brown, so that the glycerol mixed liquid needs to be decolorized, then, carbon powder is added into the carbon powder pipe 19 through the funnel 20 and is added into the decolorizing cylinder 6 through the carbon powder pipe 19, at the moment, the motor 21 is started, the rotating rod is driven to rotate through the motor 21, and then the stirrer 22 is driven to rotate, so that the carbon powder and the glycerol mixed liquid in the decolorizing cylinder 6 are stirred, the carbon powder and the glycerol mixed liquid are fully fused in and out, so that the carbon powder can remove the color in the glycerol mixed liquid, and the aim of decolorizing is fulfilled, in the process, the second valve is opened, so that the methanol solution in the methanol cylinder 7 flows to the decolorizing cylinder 6 through the filling pipe 14, and is mixed with the glycerol mixed liquid under the stirring of the stirrer 22, preparing for later extraction of glycerin, filtering the decolored solution through a carbon powder filter screen 24, so as to intercept carbon powder in a decoloring barrel 6, enabling a methanol solution and glycerin mixed solution to enter the carbon powder filter screen 24, starting a water pump 12, enabling the methanol solution and glycerin mixed solution in the carbon powder filter screen 24 to flow into a filter barrel 5 through an extraction pipe 13 under the working pressure of the water pump 12, and filtering a small amount of carbon powder contained in the methanol solution and glycerin mixed solution through a filter plate 18, so as to ensure the later extraction of clean glycerin, enabling the filtered methanol solution and glycerin mixed solution to enter a distillation barrel 4 through a connecting pipe 11, immediately heating the distillation barrel 4 through a heating pipe 3, so as to enable the temperature in the distillation barrel 4 to rise, decomposing methanol in a high-temperature environment, and generating steam in the process of heating and evaporating the solution, the steam is discharged through the exhaust pipe 10, the solution remaining in the distillation column 4 is glycerol, and then the electromagnetic valve 8 is opened, so that the extracted glycerol is led out through the discharge pipe 9.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims (7)

1. The utility model provides an extraction element for glycerine detects, includes bottom plate (1), its characterized in that, the last fixed surface of bottom plate (1) is connected with heating frame (2), and the last fixed surface of heating frame (2) is connected with retort (4), the last fixed surface of bottom plate (1) is connected with two fixed plates (17), and the top fixedly connected with of fixed plate (17) takes off a look section of thick bamboo (6), the both sides inner wall fixedly connected with a plurality of space bars (23) of a color taking off look section of thick bamboo (6), and the bottom inner wall fixedly connected with carbon powder filter screen (24) of a color taking off look section of thick bamboo (6), filter screen (24) are located space bar (23) under, the last fixed surface of a color taking off look section of thick bamboo (6) is connected with motor (21), the one end fixedly connected with dwang of motor (21) output shaft, and the one end of dwang passes a color taking off look section of thick bamboo (, the upper surface swing joint of a decoloration section of thick bamboo (6) has carbon powder pipe (19), the top fixedly connected with funnel (20) of carbon powder pipe (19), and one side swing joint of a decoloration section of thick bamboo (6) has inlet pipe (15), the upper surface fixed connection of bottom plate (1) has two backup pads (16), and the top fixedly connected with methyl alcohol section of thick bamboo (7) of backup pad (16), the bottom swing joint of methyl alcohol section of thick bamboo (7) have filling pipe (14), and the one end of filling pipe (14) is pegged graft mutually with a decoloration section of thick bamboo (6).
2. The extraction apparatus for glycerol detection according to claim 1, wherein a connection plate is fixedly connected to one side of the fixing plate (17), a filter cartridge (5) is fixedly connected to the upper surface of the connection plate, and a plurality of filter plates (18) are fixedly connected to the inner walls of the two sides of the filter cartridge (5).
3. The extraction device for glycerol detection according to claim 2, wherein the upper surface of the filter cartridge (5) is movably connected with an extraction pipe (13), one side of the extraction pipe (13) is fixedly connected with a water pump (12), the decoloring cartridge (6) is inserted into the extraction pipe (13), and the extraction pipe (13) passes through the carbon powder filter screen (24).
4. The extraction device for glycerol detection according to claim 3, wherein the upper surface of said distillation cylinder (4) is movably connected with a connecting pipe (11) and an exhaust pipe (10), and one end of the connecting pipe (11) is movably connected with a filter cylinder (5).
5. The extraction device for glycerol detection according to claim 1, wherein a heating tube (3) is arranged on one side of the heating frame (2), and the distillation cylinder (4) is positioned right above the heating tube (3).
6. The extraction device for glycerol detection according to claim 5, wherein a discharge pipe (9) is movably connected to one side of the distillation cylinder (4), and a solenoid valve (8) is movably connected to one side of the discharge pipe (9).
7. The extraction device for glycerol detection according to claim 1, characterized in that said feeding pipe (15) and filling pipe (14) are respectively articulated on one side with a first valve and a second valve.
CN202022886861.8U 2020-12-04 2020-12-04 A extraction element for glycerine detects Active CN213933302U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022886861.8U CN213933302U (en) 2020-12-04 2020-12-04 A extraction element for glycerine detects

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202022886861.8U CN213933302U (en) 2020-12-04 2020-12-04 A extraction element for glycerine detects

Publications (1)

Publication Number Publication Date
CN213933302U true CN213933302U (en) 2021-08-10

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202022886861.8U Active CN213933302U (en) 2020-12-04 2020-12-04 A extraction element for glycerine detects

Country Status (1)

Country Link
CN (1) CN213933302U (en)

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