CN213913862U - Distillation plant is used in inspection of traditional chinese medicine chemicals - Google Patents

Distillation plant is used in inspection of traditional chinese medicine chemicals Download PDF

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Publication number
CN213913862U
CN213913862U CN202022121360.0U CN202022121360U CN213913862U CN 213913862 U CN213913862 U CN 213913862U CN 202022121360 U CN202022121360 U CN 202022121360U CN 213913862 U CN213913862 U CN 213913862U
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China
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distillation
pipe
chinese medicine
traditional chinese
cooling tube
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CN202022121360.0U
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Chinese (zh)
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宫玉婷
张燕
陈雅然
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Aksu Institute For Drug Control Of Xinjiang Uygur Autonomous Region
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Aksu Institute For Drug Control Of Xinjiang Uygur Autonomous Region
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Abstract

The utility model discloses a distillation plant is used in inspection of traditional chinese medicine chemical relates to the inspection utensil, has solved among the current traditional chinese medicine chemical test process distillation mode, has the difficult problem of clearing up of remaining dregs, and its technical scheme main points are: the cooling device comprises a distillation bottle body, wherein a water bath box is arranged at the lower end of the distillation bottle body, a sealing end cap is arranged at the upper end of the distillation bottle body, a cooling pipe body is arranged on one side of the distillation bottle body, a connecting pipe is connected between the distillation bottle body and the cooling pipe body, a feeding pipe is fixedly arranged on the other side of the distillation bottle body, the connecting pipe is communicated with the cooling pipe body, a liquid outlet pipe is arranged at the tail end of the cooling pipe body, a water injection end is arranged at one end of the outer wall of the sealing end cap, and a threaded liquid pipe is arranged inside the cooling pipe body; has the effects of filtering residue in distillation process, and has high stability and convenient use.

Description

Distillation plant is used in inspection of traditional chinese medicine chemicals
Technical Field
The utility model relates to a testing apparatus, more specifically say, it relates to a distillation plant is used in inspection of traditional chinese medicine chemicals.
Background
The distillation is a thermodynamic separation process, it utilizes the different boiling points of each component in the mixed liquid or liquid-solid system, make the low boiling point component evaporate, condense in order to separate the unit operation process of the whole component, it is the union of two kinds of unit operations of evaporation and condensation, compared with other separation means, such as extraction, filtering crystallization, etc., its advantage lies in not needing to use other solvents except system component, thus guarantee not to introduce new impurity, in the inspection of Chinese medicinal chemicals, use extensively, but in the course of using, there is dregs in the distillation flask, difficult to clear up, therefore, in order to solve such a kind of problem, we propose a kind of distillation plant for inspection of Chinese medicinal chemicals.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a distillation plant is used in inspection of traditional chinese medicine chemicals has the effect of filtering remaining dregs in the distillation process, and stability is higher in the use, convenient to use.
The above technical purpose of the present invention can be achieved by the following technical solutions: including the distillation flask body, the lower extreme of distillation flask body is provided with the water bath, just the upper end of distillation flask body is provided with sealed end cap, one side of distillation flask body is provided with the cooling tube body, just be connected with the connecting pipe between distillation flask body and the cooling tube body, the opposite side fixed mounting of distillation flask body has the inlet pipe, connecting pipe and cooling tube body intercommunication, the end of cooling tube body is provided with the drain pipe.
Through adopting above-mentioned technical scheme, in the device, be provided with the water bath case, in the use, mainly distill through the mode of water bath heating to be provided with sealed end cap, in distillation process, can play sealed effect, the temperature is moderate, avoids appearing the high temperature and leads to detecting the problem that the sample loses activity.
The utility model discloses further set up to: the outer wall one end of sealed end cap is provided with the end of watering, the inside of cooling tube body is provided with the screw thread liquid pipe, the one end and the sealed end cap intercommunication of screw thread liquid pipe, just the one end of cooling tube body is run through to the other end of screw thread liquid pipe.
Through adopting above-mentioned technical scheme, in distillation process, through annotating the water end to the inside cooling water that pours into of screw thread liquid pipe, screw thread liquid pipe adopts the spiral setting, prolongs the cool time, improves cooling efficiency.
The utility model discloses further set up to: the lower extreme fixed mounting of sealed end cap has the connecting block that matches with the internal diameter of distillation flask body, the central point of connecting block puts to rotate and installs central connecting axle, the part that central connecting axle is located the connecting block upper end is evenly to set up fixed mounting and has the cooperation fan blade.
By adopting the technical scheme, in the process of injecting cooling water in the distillation process, the cooling water is movably matched with the fan blades to rotate, so that the central connecting shaft is driven to rotate.
The utility model discloses further set up to: the inside of inlet pipe is provided with deposits the material pipe, deposit material pipe and inlet pipe and all be on being located the inside circumference outer wall of retort body and evenly having seted up the through-hole, just the upper end of depositing the material pipe is provided with the sealing plug.
Through adopting above-mentioned technical scheme, in distillation process, the detection sample mainly places in the inside of stock pipe, and the bottom of stock pipe and inlet pipe is provided with the through-hole, and the detection sample is at the in-process that dissolves the separation mutually, and remaining residue can stop in the stock pipe, the later stage clearance of being convenient for.
The utility model discloses further set up to: the tail end of the central connecting shaft is evenly provided with scraping and rubbing blocks in a hinged mode, and each scraping and rubbing block is matched between the setting position of the scraping and rubbing block and the bottom end of the inlet pipe.
By adopting the technical scheme, in the cooling water flowing process, the central connecting shaft drives each rubbing block to rotate in the process of driving the matched fan blades to rotate, so that on one hand, the effect of stirring the liquid in the distillation flask body is achieved, the distillation speed is accelerated, and on the other hand, the phenomenon that the internal liquid crystals are attached to the inner wall of the distillation flask in the heating process can be prevented.
The utility model discloses further set up to: the utility model discloses a water bath box, including water bath box, clamping groove piece, connecting frame pole, draw-in groove, connecting frame pole, connecting pin is buckled, the outer wall one side of water bath box is that the symmetry sets up fixed mounting has the draw-in groove piece, and is two sets of the inside slidable mounting of draw-in groove piece has the connecting frame pole, just the draw-in groove has been seted up on the draw-in groove piece, be the symmetry on the connecting frame pole and set up fixed mounting and detain with the connecting pin of draw-in groove matching.
Through adopting above-mentioned technical scheme, the connecting rod can reciprocate in the inside of draw-in groove piece, and when the connecting rod removed the top of draw-in groove piece, the connecting rod can carry out the rotation of certain angle.
The utility model discloses further set up to: the connecting frame rod is in a herringbone shape, and the upper end of the connecting frame rod is arranged into a circular ring shape matched with the distillation flask body.
Through adopting above-mentioned technical scheme, the hack lever is at the removal and the pivoted in-process to because hack lever top is the ring form, so can fix the retort body through the ring.
To sum up, the utility model discloses following beneficial effect has: in the use, can improve distillation efficiency to have the effect of filtering dregs, the later stage clearance of being convenient for has better stability in the use.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings required for the embodiments or the prior art descriptions will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.
Fig. 1 is a schematic structural diagram of the present invention;
fig. 2 is a side view of the present invention;
FIG. 3 is a cross sectional view of the present invention;
fig. 4 is a vertical cut-away view of the present invention.
In the figure: 1. a water injection end; 2. sealing the end cap; 3. a distillation flask body; 4. a connecting frame rod; 5. A water bath tank; 6. connecting a pin buckle; 7. a liquid outlet pipe; 8. a cooling tube body; 9. a connecting pipe; 10. A sealing plug; 11. a feed pipe; 12. a slot clamping block; 13. a threaded liquid pipe; 14. connecting blocks; 15. Matching fan blades; 16. a central connecting shaft; 17. a material storage pipe; 18. scraping and rubbing blocks; 19. a clamping groove.
Detailed Description
In order to make the technical problems, technical solutions and advantageous effects to be solved by the present invention more clearly understood, the present invention is further described in detail below with reference to the accompanying drawings 1 to 4 and the embodiments.
It will be understood that when an element is referred to as being "secured to" or "disposed on" another element, it can be directly on the other element or be indirectly on the other element. When an element is referred to as being "connected to" another element, it can be directly or indirectly connected to the other element.
It will be understood that the terms "length," "width," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in an orientation or positional relationship indicated in the drawings for convenience in describing the invention and to simplify the description, and are not intended to indicate or imply that the referenced device or element must have a particular orientation, be constructed and operated in a particular orientation, and are therefore not to be considered limiting of the invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, "a plurality" means two or more unless specifically limited otherwise.
Example (b): the utility model provides a distillation plant is used in inspection of traditional chinese medicine chemicals, including distillation flask body 3, the lower extreme of distillation flask body 3 is provided with water bath 5, and the upper end of distillation flask body 3 is provided with sealed end cap 2, one side of distillation flask body 3 is provided with cooling tube body 8, and is connected with connecting pipe 9 between distillation flask body 3 and the cooling tube body 8, and the opposite side fixed mounting of distillation flask body 3 has inlet pipe 11, and connecting pipe 9 and cooling tube body 8 intercommunication, the end of cooling tube body 8 is provided with drain pipe 7.
As shown in fig. 1 and 3, a water injection end 1 is arranged at one end of the outer wall of the sealing end cap 2, a threaded liquid pipe 13 is arranged inside the cooling pipe body 8, one end of the threaded liquid pipe 13 is communicated with the sealing end cap 2, the other end of the threaded liquid pipe 13 penetrates through one end of the cooling pipe body 8, a connecting block 14 matched with the inner diameter of the distillation flask body 3 is fixedly arranged at the lower end of the sealing end cap 2, a central connecting shaft 16 is rotatably arranged at the central position of the connecting block 14, and a matching fan 15 is uniformly and fixedly arranged on the part of the central connecting shaft 16, which is positioned at the upper end of the connecting block 14.
As shown in fig. 2 and 3, a storage tube 17 is arranged inside the feeding tube 11, through holes are uniformly formed in the circumferential outer walls of the storage tube 17 and the feeding tube 11 inside the distillation flask body 3, and a sealing plug 10 is arranged at the upper end of the storage tube 17.
As shown in fig. 3, the tail end of the central connecting shaft 16 is uniformly provided and hinged with scraping blocks 18, and the setting position of each scraping block 18 is matched with the bottom end of the feeding pipe 11.
As shown in fig. 1 and 3, the outer wall of the water bath box 5 is symmetrically provided with the clamping groove blocks 12, the two groups of clamping groove blocks 12 are slidably provided with the connecting frame rods 4, the clamping grooves 12 are provided with the clamping grooves 19, the connecting frame rods 4 are symmetrically provided with the connecting pin buckles 6 matched with the clamping grooves 19, the connecting frame rods 4 are in a herringbone shape, and the upper ends of the connecting frame rods 4 are arranged in a circular ring shape matched with the distillation flask body 3.
The working principle is as follows: in the using process, the connecting frame rod 4 is moved upwards, the distillation flask body 3 is sleeved at the upper end of the connecting frame rod 4, then the distillation flask body 3 is placed on the water bath box 5, and the distillation flask body 3 has good stability due to the arrangement of the clamping groove block 12 and the connecting frame rod 4;
then placing the sample to be detected in a storage pipe 17, placing the storage pipe 17 in a feeding pipe 11, placing a solvent in the distillation flask body 3 to dissolve the solvent and the sample to be detected, closing the sealing end cap 2 and communicating the water injection end 1;
in the process that the water bath tank 5 heats the liquid inside the distillation flask body 3, the generated steam enters the cooling pipe body 8 through the connecting pipe 9, the cooling water gradually enters the interior of the threaded liquid pipe 13 through the water injection end 1, and in the flowing process of the cooling water, the matching fan sheet 15 is driven to rotate to drive the central connecting shaft 16 to rotate, so that each scraping block 18 is driven to rotate, liquid crystals inside the distillation flask body 3 can be prevented from being adhered to the inner wall of the distillation flask body 3 under the stirring effect, and the steam generated in the heating process enters the cooling pipe body 8 and flows out through the liquid outlet pipe 7 after being cooled;
after the distillation is completed, the sealing plug 10 can be opened and the storage tube 17 removed to facilitate the cleaning of the dross.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications to the present embodiment without inventive contribution as required after reading the present specification, but all of them are protected by patent laws within the scope of the claims of the present invention.

Claims (7)

1. The utility model provides a distillation plant is used in inspection of traditional chinese medicine chemicals, includes retort body (3), characterized by: the lower extreme of distillation flask body (3) is provided with water bath (5), just the upper end of distillation flask body (3) is provided with sealed end cap (2), one side of distillation flask body (3) is provided with cooling tube body (8), just be connected with connecting pipe (9) between distillation flask body (3) and cooling tube body (8), the opposite side fixed mounting of distillation flask body (3) has inlet pipe (11), connecting pipe (9) and cooling tube body (8) intercommunication, the end of cooling tube body (8) is provided with drain pipe (7).
2. The distillation device for inspecting traditional Chinese medicine chemicals as claimed in claim 1, wherein: the outer wall one end of sealed end cap (2) is provided with water injection end (1), the inside of cooling tube body (8) is provided with screw thread liquid pipe (13), the one end and the sealed end cap (2) intercommunication of screw thread liquid pipe (13), just the one end of cooling tube body (8) is run through to the other end of screw thread liquid pipe (13).
3. The distillation device for inspecting traditional Chinese medicine chemicals as claimed in claim 1, wherein: the lower extreme fixed mounting of sealed end cap (2) has connecting block (14) with retort body (3) internal diameter matching, the central point of connecting block (14) puts to rotate and installs central connecting axle (16), part that central connecting axle (16) are located connecting block (14) upper end is evenly to set up fixed mounting and has cooperation fan piece (15).
4. The distillation device for inspecting traditional Chinese medicine chemicals as claimed in claim 1, wherein: the inside of inlet pipe (11) is provided with deposits material pipe (17), deposit material pipe (17) and inlet pipe (11) and all be evenly to have seted up the through-hole on being located the inside circumference outer wall of retort body (3), just the upper end of depositing material pipe (17) is provided with sealing plug (10).
5. The distillation device for inspecting traditional Chinese medicine chemicals as claimed in claim 3, wherein: the tail end of the central connecting shaft (16) is uniformly hinged with scraping blocks (18), and each scraping block (18) is matched with the bottom end of the inlet pipe (11) in the setting position.
6. The distillation device for inspecting traditional Chinese medicine chemicals as claimed in claim 1, wherein: the utility model discloses a water bath cabinet, including water bath box (5), outer wall one side is the symmetry and sets up fixed mounting has draw-in groove piece (12), and is two sets of the inside slidable mounting of draw-in groove piece (12) has connecting bracket pole (4), just draw-in groove (19) have been seted up on draw-in groove piece (12), it sets up fixed mounting and detains (6) with the connecting pin that draw-in groove (19) match to be the symmetry on connecting bracket pole (4).
7. The distillation device for inspecting traditional Chinese medicine chemicals as claimed in claim 6, wherein: the connecting frame rod (4) is in a herringbone shape, and the upper end of the connecting frame rod (4) is arranged to be in a circular ring shape matched with the distillation flask body (3).
CN202022121360.0U 2020-09-24 2020-09-24 Distillation plant is used in inspection of traditional chinese medicine chemicals Active CN213913862U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022121360.0U CN213913862U (en) 2020-09-24 2020-09-24 Distillation plant is used in inspection of traditional chinese medicine chemicals

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202022121360.0U CN213913862U (en) 2020-09-24 2020-09-24 Distillation plant is used in inspection of traditional chinese medicine chemicals

Publications (1)

Publication Number Publication Date
CN213913862U true CN213913862U (en) 2021-08-10

Family

ID=77217701

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202022121360.0U Active CN213913862U (en) 2020-09-24 2020-09-24 Distillation plant is used in inspection of traditional chinese medicine chemicals

Country Status (1)

Country Link
CN (1) CN213913862U (en)

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