CN213668270U - Washing, filtering and drying integrated device for post-treatment of organic reagent - Google Patents
Washing, filtering and drying integrated device for post-treatment of organic reagent Download PDFInfo
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- CN213668270U CN213668270U CN202022204831.4U CN202022204831U CN213668270U CN 213668270 U CN213668270 U CN 213668270U CN 202022204831 U CN202022204831 U CN 202022204831U CN 213668270 U CN213668270 U CN 213668270U
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Abstract
The utility model discloses a washing, filtering and drying integrated device for organic reagent aftertreatment, include: the device comprises a vibration heating mechanism, a filtrate discharging mechanism is installed in the vibration heating mechanism, a filtrate discharging pipeline is arranged on the filtrate discharging mechanism, a switch screw is installed at the bottom of the filtrate discharging mechanism, the top end of the switch screw is blocked with the filtrate discharging pipeline, and the top surface of the vibration heating mechanism consists of four inclined surfaces which are connected end to end, inclined downwards and connected with the top end of the filtrate discharging mechanism; the receiving mechanism is arranged on the top surface of the oscillating heating mechanism and consists of a plurality of side surfaces and a top surface, and a through hole is formed in the top surface of the receiving mechanism; a connecting pipe mounted on the through hole on the top surface of the receiving mechanism; and a pressure output and input device connected with the connecting pipe. The utility model discloses be favorable to the product to separate out into powder from organic solvent, avoid operating personnel and organic reagent long-term contact.
Description
Technical Field
The utility model relates to a washing, filtering and drying integrated device for organic reagent aftertreatment.
Background
In organic routine experiments and industrial production, many substances need to be washed and separated out in organic reagents. At present, the conventional method is to pour the prepared product solution into the organic reagent under the condition of stirring, or pour the organic reagent into the product solution directly, the product prepared by the method can be agglomerated into a block due to the stirring factor, the final product needs to be reprocessed if the final product needs to be powdered, the reprocessing can influence the performance of the material, and the molecular weight can be reduced if the high molecular product is used. In addition, most organic reagents are harmful to the human body, and although the reagents used conventionally are not toxic, the reagents can be harmful to the human body even if contacted in close proximity for a long time. Therefore, the device which is beneficial to powdering of the product and avoids the close contact of people and organic reagents is greatly necessary for chemical production.
Disclosure of Invention
The utility model aims at the defect that prior art exists, provide a washing filter drying integrated device for organic reagent aftertreatment, be favorable to the product to separate out into powder from organic solvent, avoid operating personnel and organic reagent long-term contact, simple structure, occupation space is few, and it is convenient to use, provides the protection to producing the property when promoting product yield.
The purpose of the utility model is realized like this:
the utility model discloses a washing, filtering and drying integrated device for organic reagent aftertreatment, include:
the device comprises a vibration heating mechanism, a liquid storage tank, a liquid outlet pipe, a liquid outlet;
the receiving mechanism is arranged on the top surface of the oscillating heating mechanism, a sealing ring is arranged between the receiving mechanism and the top surface of the oscillating heating mechanism, the receiving mechanism consists of a plurality of side surfaces and a top surface, a through hole is arranged on the top surface of the receiving mechanism, and the receiving mechanism is positioned above the filtrate discharging mechanism;
a connecting pipe mounted on the through hole on the top surface of the receiving mechanism; and
and the pressure output and input device is connected with the connecting pipe.
The washing, filtering and drying integrated device for post-treatment of organic reagents comprises a pressure input/output device, a pressure output device and a pressure gauge, wherein the pressure input/output device comprises an input/output pipe connected with a connecting pipe, a detachable pressure input device connected with the input/output pipe, a detachable pressure output device connected with the input/output pipe and the pressure gauge arranged on the input/output pipe.
The washing, filtering and drying integrated device for the post-treatment of the organic reagent is characterized in that one end of the filtrate discharge pipeline is connected with the filtrate discharge mechanism, and the other end of the filtrate discharge pipeline is connected with the waste liquid barrel.
In the washing, filtering and drying integrated device for the post-treatment of the organic reagent, a filter paper is arranged at the top end of the filtrate discharge mechanism.
The washing, filtering and drying integrated device for the post-treatment of the organic reagent is characterized in that the pressure input device is an external supercharger, and the pressure output device is a vacuum pump.
The washing, filtering and drying integrated device for the post-treatment of the organic reagent is characterized in that the vibration heating mechanism is connected with a motor.
The utility model discloses following beneficial effect has:
(1) when the powder is separated out, the product can be separated out to form aggregation by using a conventional stirring method, and the powder cannot be formed after later drying, but the powder can be ensured to be formed after the product is separated out by oscillating and separating out through the connecting pipe, the receiving mechanism, the filtrate discharging mechanism and the oscillating heating mechanism;
(2) the utility model has the advantages that the integrated design can avoid the long-term contact between the operators and the organic reagent when in use, prevent the harm brought by the organic reagent, and especially avoid the harm brought by the organic reagent which is easy to volatilize and has great harm to human body;
(3) the utility model has simple structure, portable operation, wide application range and small occupied space;
(4) the utility model discloses be favorable to the product productivity to improve and produce property ability protection.
Drawings
Fig. 1 is a front view of the present invention;
fig. 2 is a top view of the oscillating heating mechanism of the present invention.
Detailed Description
The present invention will be further explained with reference to the accompanying drawings.
Referring to fig. 1 and 2, the washing, filtering and drying integrated device for post-treatment of organic reagents according to the present invention is shown, comprising:
the device comprises a vibration heating mechanism 1, wherein two limiting plates 11 are arranged on the left side and the right side of the top surface of the vibration heating mechanism 1, a filtrate discharge mechanism 2 is arranged in the vibration heating mechanism 1, a filtrate discharge pipeline 21 is arranged on the filtrate discharge mechanism 2, a switch screw 22 is arranged at the bottom of the filtrate discharge mechanism 2, the top end of the switch screw 22 blocks the filtrate discharge pipeline 21, and the top surface of the vibration heating mechanism 1 is composed of four inclined surfaces 12 which are connected end to end, inclined downwards and connected with the top end of the filtrate discharge mechanism 2;
the receiving mechanism 3 is installed on the top surface of the oscillating heating mechanism 1, a sealing ring (not shown) is arranged between the receiving mechanism 3 and the top surface of the oscillating heating mechanism 1, the sealing ring (not shown) plays a role in preventing air leakage, the receiving mechanism 3 is composed of a plurality of side surfaces and a top surface, a through hole (not shown) is formed in the top surface of the receiving mechanism 3, and the receiving mechanism 3 is positioned above the filtrate discharging mechanism 2;
a connection pipe 4 installed on a through hole (not shown) of the top surface of the receiving mechanism 3; and
a pressure output and input device 5 connected with the connecting pipe 4.
The pressure output and input device 5 includes an input and output pipe 51 connected to the connection pipe 4, a pressure input device (not shown) detachably connected to the input and output pipe 51, a pressure output device (not shown) detachably connected to the input and output pipe 51, and a pressure gauge 52 installed on the input and output pipe 51.
One end of the filtrate discharge pipe 21 is connected to the filtrate discharge mechanism 2, and the other end of the filtrate discharge pipe 21 is connected to a waste liquid tank 6.
The filtrate discharge means 2 is provided at its top end with a filter paper (not shown).
The pressure input device (not shown) is an external booster, and the pressure output device (not shown) is a vacuum pump.
The oscillating heating mechanism 1 is connected with a motor (not shown).
The utility model discloses a use, screw up switching screw 22 under the initial condition, pull down input output tube 51, open motor (not shown in the figure) afterwards, thereby start to vibrate heating mechanism 1 and make it vibrate, inject organic solvent into receiving mechanism 3 through connecting pipe 4, organic solvent flows on four inclined planes 12 and finally flows on the filter paper (not shown in the figure) on the top of filtrating discharge mechanism 2, the shared volume of organic solvent is less than or equal to two thirds of the total volume of receiving mechanism 3, at this moment pour into receiving mechanism 3 with coarse product (not shown in the figure) through connecting pipe 4, and dissolve in organic solvent, precipitate powdered product under the vibration, after the product is completely precipitated, stop vibrating, unscrew switching screw 22, connect external booster compressor (not shown in the figure) and open the pressure boost of pressure input output device 5 on connecting pipe 4, control input pressure through manometer 52, pressurizing and filtering the organic solvent, enabling filtrate to flow into the waste liquid barrel 6 through a filtrate discharge pipeline 21, tightening a switch screw 22 after pressurizing and filtering are finished, discharging pressure through an external supercharger (not shown) to enable the receiving mechanism 3 to recover normal pressure, adding the organic solvent again if the precipitated product needs to be washed, and oscillating, pressurizing, filtering and discharging pressure; after washing, the switch screw 22 is screwed down, the external supercharger (not shown) is dismounted, the vacuum pump (not shown) is connected with the input and output pipe 51, the vacuum pump (not shown) is started to vacuumize, the heating mechanism 1 is vibrated to heat and dry, after drying is finished, the normal pressure of the receiving mechanism 3 is recovered, then the pressure input and output device 5, the connecting pipe 4 and the receiving mechanism 3 are sequentially dismounted, and the separated product powder can be taken out.
The utility model discloses a connecting pipe 4, receiving mechanism 3, filtrating discharge mechanism 2 and shock heating mechanism 1 vibrate and separate out, then can guarantee that the product becomes powder after separating out, the setting of limiting plate 11 is spacing when rocking about receiving mechanism 3, the setting of four inclined planes 12 does benefit to organic solvent and slowly flows down, and four inclined planes 12 form airtight space with receiving mechanism 3, have avoided organic solvent to shake out when vibrating heating mechanism 1 and rock; when in use, the utility model can avoid the long-term contact between the operator and the organic reagent, prevent the harm brought by the organic reagent, and especially avoid the harm brought by the organic reagent which is easy to volatilize and has great harm to human body; the utility model has simple structure, portable operation, wide application range and small occupied space; is beneficial to improving the yield of the product and protecting the product performance.
The above embodiments are provided only for the purpose of illustration, not for the limitation of the present invention, and those skilled in the relevant art can make various changes or modifications without departing from the spirit and scope of the present invention, therefore, all equivalent technical solutions should also belong to the scope of the present invention, and should be defined by the claims.
Claims (6)
1. A washing, filtering and drying integrated device for organic reagent aftertreatment, characterized in that the washing, filtering and drying integrated device comprises:
the device comprises a vibration heating mechanism, two limiting plates are arranged on the left side and the right side of the top surface of the vibration heating mechanism, a filtrate discharge mechanism is installed in the vibration heating mechanism, a filtrate discharge pipeline is arranged on the filtrate discharge mechanism, a switch screw is installed at the bottom of the filtrate discharge mechanism, the top end of the switch screw blocks the filtrate discharge pipeline, and the top surface of the vibration heating mechanism is composed of four inclined planes which are connected end to end, inclined downwards and connected with the top end of the filtrate discharge mechanism;
the receiving mechanism is arranged on the top surface of the oscillating heating mechanism, a sealing ring is arranged between the receiving mechanism and the top surface of the oscillating heating mechanism, the receiving mechanism consists of a plurality of side surfaces and a top surface, a through hole is arranged on the top surface of the receiving mechanism, and the receiving mechanism is positioned above the filtrate discharging mechanism;
a connecting pipe mounted on the through hole of the top surface of the receiving mechanism; and
and the pressure output and input device is connected with the connecting pipe.
2. The integrated washing, filtering and drying apparatus for post-treatment of organic reagents according to claim 1, wherein the pressure input/output device comprises an input/output pipe connected to the connection pipe, a pressure input unit detachably connected to the input/output pipe, a pressure output unit detachably connected to the input/output pipe, and a pressure gauge installed on the input/output pipe.
3. The integrated washing, filtering and drying device for post-treatment of organic reagents according to claim 2, wherein the pressure input device is an external pressure booster, and the pressure output device is a vacuum pump.
4. The integrated washing, filtering and drying device for post-treatment of organic reagents according to claim 1, wherein one end of the filtrate discharge pipeline is connected with the filtrate discharge mechanism, and the other end of the filtrate discharge pipeline is connected with a waste liquid barrel.
5. The integrated washing, filtering and drying device for post-treatment of organic reagents according to claim 1, wherein the top end of the filtrate discharging mechanism is provided with a filter paper.
6. The integrated washing, filtering and drying device for post-treatment of organic reagents according to claim 1, wherein the oscillating heating mechanism is connected with a motor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022204831.4U CN213668270U (en) | 2020-09-30 | 2020-09-30 | Washing, filtering and drying integrated device for post-treatment of organic reagent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022204831.4U CN213668270U (en) | 2020-09-30 | 2020-09-30 | Washing, filtering and drying integrated device for post-treatment of organic reagent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213668270U true CN213668270U (en) | 2021-07-13 |
Family
ID=76751593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022204831.4U Active CN213668270U (en) | 2020-09-30 | 2020-09-30 | Washing, filtering and drying integrated device for post-treatment of organic reagent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213668270U (en) |
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2020
- 2020-09-30 CN CN202022204831.4U patent/CN213668270U/en active Active
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