CN213375190U - Massoia lactone distillation plant - Google Patents
Massoia lactone distillation plant Download PDFInfo
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- CN213375190U CN213375190U CN202120815949.2U CN202120815949U CN213375190U CN 213375190 U CN213375190 U CN 213375190U CN 202120815949 U CN202120815949 U CN 202120815949U CN 213375190 U CN213375190 U CN 213375190U
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Abstract
The utility model provides a maxolide distillation plant, including the distillation column, install at the water bath section of thick bamboo of distillation column bottom, install the heating device in the water bath section of thick bamboo and install the liquid storage pot on one side at the distillation column, be connected with the cooling tube between distillation column and the liquid storage pot. The exhaust nozzle at the top of the distillation barrel is provided with a three-way pipe, the other two ends of the three-way pipe are provided with electromagnetic valves, and one end of the cooling pipe is connected to the electromagnetic valve at one end of the three-way pipe. The cooling pipe is S-shaped, a liquid outlet nozzle is arranged on the cooling pipe at the valley bottom of the cooling pipe and faces downwards, and the liquid storage tank is connected to the liquid outlet nozzle. The cooling pipe is provided with a pressure limiting valve at the valley bottom. The S-shaped cooling pipe can realize multi-stage cooling. The pressure limiting valve on the cooling pipe can control the air pressure in the cooling pipe in a sectional manner, and the distillation efficiency of the maosolides can be effectively improved.
Description
Technical Field
The utility model relates to a maxolide production facility, especially maxolide distillation plant.
Background
The majolide is present in majoram cassia oil, fermented Cordyceps mycelium, Chinese liquor, wine, flos Osmanthi Fragrantis and cane molasses, and has antibacterial, anti-infectious and immunity regulating effects. The maosolides have creamy, coconut, spicy and celery notes and can be used as a valuable spice in the formulation of butter, cream, vanilla, peach, almond, fruit, nut and tobacco flavors. The maosolides are usually synthesized from natural raw materials, and the preparation process comprises distillation, separation and purification and drying treatment. The raw materials are crushed and then distilled, and the distillation process is time-consuming. In order to improve the distillation efficiency, the distillation temperature and the cooling air pressure are accurately controlled in the distillation process.
SUMMERY OF THE UTILITY MODEL
The utility model provides a maxolide distillation plant adopts the water bath heating distillation, and the cooling tube of S type can realize the multistage cooling to install the pressure limiting valve on the cooling tube, but the distillation efficiency of maxolide can effectively be improved to atmospheric pressure in the segmentation control cooling tube.
The technical scheme of the utility model is realized like this: the massoia lactone distilling device comprises a distilling cylinder, a water bath cylinder arranged at the bottom of the distilling cylinder, a heating device arranged in the water bath cylinder and a liquid storage tank arranged beside the distilling cylinder, wherein a cooling pipe is connected between the distilling cylinder and the liquid storage tank; a liquid inlet nozzle is arranged on one side of the distillation barrel, a slag discharging nozzle is arranged on one side of the bottom of the distillation barrel outwards, the slag discharging nozzle penetrates through the water bath barrel and extends out of the water bath barrel, and switch valves are arranged on the liquid inlet nozzle and the slag discharging nozzle; an exhaust nozzle is arranged at the top of the distillation barrel, a three-way pipe is arranged on the exhaust nozzle, electromagnetic valves are arranged at the other two ends of the three-way pipe, and one end of the cooling pipe is connected to the electromagnetic valve at one end of the three-way pipe; the cooling pipe is S-shaped, a liquid outlet nozzle is arranged on the cooling pipe at the position of the valley bottom of the cooling pipe downwards, and the liquid storage tank is connected to the liquid outlet nozzle; the cooling pipe is provided with a pressure limiting valve at the valley bottom; and a power supply assembly is arranged on one side of the water bath barrel and is electrically connected with the heating device.
Furthermore, the tail end of the cooling pipe is also connected with a return pipe; a liquid inlet three-way pipe is connected between the liquid inlet nozzle and the switch valve, the liquid inlet three-way pipe is connected with the return pipe through an air guide pipe, a branch pipe is arranged on the air guide pipe, and the branch pipe is connected to one end of the three-way pipe.
Further, the heating device comprises a plurality of annular heating wires; the water bath barrel is internally provided with a support frame, the support frame is provided with a plurality of limiting plates, and the heating wires are limited and clamped on the limiting plates.
The distillation barrel comprises a bottom barrel and a top barrel arranged on the bottom barrel, the slag discharge nozzle is arranged on the bottom barrel, and the liquid inlet nozzle is arranged on the top barrel; the inner bottom surface of the bottom barrel is a concave spherical surface, and the upper half part of the top barrel is a conical barrel body; and a filter plate is arranged in the top cylinder.
By adopting the technical scheme, the beneficial effects of the utility model are that:
the utility model discloses a maxolide distillation plant, including the distillation column, install at the water bath section of thick bamboo of distillation column bottom, install the heating device in the water bath section of thick bamboo and install the liquid storage pot on one side at the distillation column, be connected with the cooling tube between distillation column and the liquid storage pot. The exhaust nozzle at the top of the distillation barrel is provided with a three-way pipe, the other two ends of the three-way pipe are provided with electromagnetic valves, and one end of the cooling pipe is connected to the electromagnetic valve at one end of the three-way pipe. The cooling pipe is S-shaped, a liquid outlet nozzle is arranged on the cooling pipe at the valley bottom of the cooling pipe and faces downwards, and the liquid storage tank is connected to the liquid outlet nozzle. The cooling pipe is provided with a pressure limiting valve at the valley bottom. The S-shaped cooling pipe can realize multi-stage cooling. The pressure limiting valve on the cooling pipe can control the air pressure in the cooling pipe in a sectional manner, and the distillation efficiency of the maosolides can be effectively improved.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed to be used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without inventive exercise.
Fig. 1 is a schematic structural view of the present invention;
fig. 2 is a schematic view of the split structure of the present invention;
wherein: 1. the device comprises a distillation barrel, a water bath barrel 2, a liquid storage tank 3, a cooling pipe 4, a liquid inlet nozzle 5, a slag discharge nozzle 6, a switch valve 7, an exhaust nozzle 8, a three-way pipe 9, an electromagnetic valve 10, a liquid outlet nozzle 11, a pressure limiting valve 12, a power supply assembly 13, a return pipe 14, a liquid inlet three-way pipe 15, a gas guide pipe 16, a branch pipe 17, a heating wire 18, a support frame 19, a limit plate 20, a bottom barrel 21, a top barrel 22 and a filter plate 23.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative efforts belong to the protection scope of the present invention.
As shown in figures 1-2, the maxolide distilling apparatus comprises a distilling cylinder 1, a water bath cylinder 2 arranged at the bottom of the distilling cylinder 1, a heating device arranged in the water bath cylinder 2 and a liquid storage tank 3 arranged beside the distilling cylinder 1, wherein a cooling pipe 4 is connected between the distilling cylinder 1 and the liquid storage tank 3. A liquid inlet nozzle 5 is arranged on one side of the distillation barrel 1, a slag discharging nozzle 6 is arranged on one side of the bottom of the distillation barrel 1 outwards, the slag discharging nozzle 6 penetrates through the water bath barrel 2 and extends out of the water bath barrel 2, and switch valves 7 are arranged on the liquid inlet nozzle 5 and the slag discharging nozzle 6. An exhaust nozzle 8 is arranged at the top of the distillation barrel 1, a three-way pipe 9 is arranged on the exhaust nozzle 8, electromagnetic valves 10 are arranged at the other two ends of the three-way pipe 9, and one end of the cooling pipe 4 is connected to the electromagnetic valve 10 at one end of the three-way pipe 9. The cooling pipe 4 is S-shaped, a liquid outlet 11 is arranged on the cooling pipe 4 at the valley bottom position and faces downwards, and the liquid storage tank 3 is connected to the liquid outlet 11. The cooling pipe 4 is provided with a pressure limiting valve 12 at the valley bottom position. A power supply module 13 is mounted on one side of the water bath barrel 2, and the power supply module 13 is electrically connected with a heating device.
The return pipe 14 is also connected to the end of the cooling pipe 4 in this embodiment. A liquid inlet three-way pipe 15 is connected between the liquid inlet nozzle 5 and the switch valve 7, the liquid inlet three-way pipe 15 is connected with the return pipe 14 through a gas guide pipe 16, a branch pipe 17 is arranged on the gas guide pipe 16, and the branch pipe 17 is connected with one end of the three-way pipe 9. The cooling pipe 4 is connected with the liquid inlet nozzle 5 through a return pipe 14 and an air duct 16, and the cooled residual tail gas can flow back to the distillation barrel 1 for circular distillation, so that more maosolides can be extracted.
The heating means of the present embodiment comprises a plurality of heating wires 18 in the form of loops. A supporting frame 19 is arranged in the water bath barrel 2, a plurality of limiting plates 20 are arranged on the supporting frame 19, and the heating wires 18 are limited and clamped on the limiting plates 20. The water bath barrel 2 is filled with water, and the water is heated by the heating wire 18, so that the heating problem is convenient to control.
The distillation column 1 of the embodiment comprises a bottom column 21 and a top column 22 arranged on the bottom column 21, wherein the slag discharge nozzle 6 is arranged on the bottom column 21, and the liquid inlet nozzle 5 is arranged on the top column 22. The inner bottom surface of the bottom cylinder 21 is a concave spherical surface, and the upper half part of the top cylinder 22 is a conical cylinder body. A filter plate 23 is installed in the top cylinder 22. The bottom surface of the bottom cylinder 21 is contacted with the water in the water bath cylinder 2, the heating surface of the bottom cylinder 21 is large, and the heating efficiency is high. The filter plate 23 can block bubbles, and steam can smoothly enter the three-way pipe 9 and the cooling pipe 4.
The utility model discloses a maxolide distillation plant, the cooling tube 4 of S type can realize multistage cooling. The pressure limiting valve 12 on the cooling pipe 4 can control the air pressure in the cooling pipe 4 in a sectional manner, and the distillation efficiency of the maosolides can be effectively improved.
The above description is only a preferred embodiment of the present invention, and should not be taken as limiting the invention, and any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (4)
1. The massoia lactone distilling device is characterized by comprising a distilling cylinder (1), a water bath cylinder (2) arranged at the bottom of the distilling cylinder (1), a heating device arranged in the water bath cylinder (2) and a liquid storage tank (3) arranged beside the distilling cylinder (1), wherein a cooling pipe (4) is connected between the distilling cylinder (1) and the liquid storage tank (3); a liquid inlet nozzle (5) is arranged on one side of the distillation barrel (1), a slag discharging nozzle (6) is arranged on one side of the bottom of the distillation barrel (1) outwards, the slag discharging nozzle (6) penetrates through the water bath barrel (2) and extends out of the water bath barrel (2), and switch valves (7) are arranged on the liquid inlet nozzle (5) and the slag discharging nozzle (6); an exhaust nozzle (8) is arranged at the top of the distillation barrel (1), a three-way pipe (9) is arranged on the exhaust nozzle (8), electromagnetic valves (10) are arranged at the other two ends of the three-way pipe (9), and one end of the cooling pipe (4) is connected to the electromagnetic valve (10) at one end of the three-way pipe (9); the cooling pipe (4) is S-shaped, a liquid outlet nozzle (11) is arranged on the cooling pipe (4) at the valley bottom position downwards, and the liquid storage tank (3) is connected to the liquid outlet nozzle (11); the cooling pipe (4) is provided with a pressure limiting valve (12) at the valley bottom; and a power supply assembly (13) is arranged on one side of the water bath barrel (2), and the power supply assembly (13) is electrically connected with the heating device.
2. The massoia lactone distillation unit according to claim 1, characterized in that the end of the cooling pipe (4) is further connected with a return pipe (14); a liquid inlet three-way pipe (15) is connected between the liquid inlet nozzle (5) and the switch valve (7), the liquid inlet three-way pipe (15) is connected with the return pipe (14) through a gas guide pipe (16), a branch pipe (17) is arranged on the gas guide pipe (16), and the branch pipe (17) is connected to one end of the three-way pipe (9).
3. The maxolide distillation unit according to claim 1 wherein said heating means comprises a plurality of annular heating wires (18); a supporting frame (19) is installed in the water bath barrel (2), a plurality of limiting plates (20) are arranged on the supporting frame (19), and the heating wires (18) are limited and clamped on the limiting plates (20).
4. The maxolide distillation unit according to claim 1, wherein the distillation column (1) comprises a bottom column (21) and a top column (22) arranged on the bottom column (21), the slag discharge nozzle (6) is arranged on the bottom column (21), and the liquid inlet nozzle (5) is arranged on the top column (22); the inner bottom surface of the bottom barrel (21) is a concave spherical surface, and the upper half part of the top barrel (22) is a conical barrel body; and a filter plate (23) is arranged in the top cylinder (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120815949.2U CN213375190U (en) | 2021-04-21 | 2021-04-21 | Massoia lactone distillation plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120815949.2U CN213375190U (en) | 2021-04-21 | 2021-04-21 | Massoia lactone distillation plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213375190U true CN213375190U (en) | 2021-06-08 |
Family
ID=76197185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120815949.2U Active CN213375190U (en) | 2021-04-21 | 2021-04-21 | Massoia lactone distillation plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213375190U (en) |
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2021
- 2021-04-21 CN CN202120815949.2U patent/CN213375190U/en active Active
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