CN213193687U

CN213193687U - Automatic device for amino silicone oil synthesis

Info

Publication number: CN213193687U
Application number: CN202021814545.3U
Authority: CN
Inventors: 郭家勇
Original assignee: Shantou Tuoxin Silicone Technology Co ltd
Current assignee: Guangdong Tuoxin Organic Silicon Technology Co ltd
Priority date: 2020-08-27
Filing date: 2020-08-27
Publication date: 2021-05-14
Anticipated expiration: 2030-08-27

Abstract

The utility model provides a synthetic automation equipment of amino-silicone oil, including the reation kettle casing, one side fixed mounting of reation kettle casing has the fixture block, and the internally mounted of fixture block has the baffle, and one side block inside and reation kettle shells inner wall is arranged in to one side of baffle, and electric telescopic handle is installed at the top of baffle, and partly separates to be first cavity and second cavity in the reation kettle casing, and the mid-mounting of reation kettle casing opposite side has the vacuum machine, the beneficial effect of the utility model: mutually supporting of dividing through the servo motor that sets up and stirring rod is convenient for stir the amino silicone oil synthetic raw materials of first cavity 2 inside, carries out preliminary even abundant vibration to amino silicone oil synthetic raw materials and mixes to improve synthetic efficiency, through mutually supporting of the heater that sets up and vacuum machine, guarantee the inside temperature of second cavity through the heater heating, blow away moisture through the nitrogen gas of air pump output, improve the viscosity of emulsification, improve the yield of silicone oil.

Description

Automatic device for amino silicone oil synthesis

Technical Field

The utility model belongs to the technical field of chemical synthesis, concretely relates to amino silicone oil synthesis's automation equipment.

Background

The amino silicone oil is a latest generation hydrophilic and low-color-change amino silicone oil softening finishing agent modified by special amino. The fabric has soft and smooth hand feeling of the traditional amino silicone oil, can endow the fabric with excellent hydrophilicity, antistatic property, stain resistance, low color change and fluffy feeling, greatly improves the service performance of the fabric, is suitable for fabrics such as high-grade pure cotton, wool blended fabrics and terylene, and is the best choice of the latest generation of high-grade textiles. The amino silicone oil is easy to emulsify into stable and transparent microemulsion by proper surfactant. It can be used alone, also can be used with other organosilicon or organic softener complex, is suitable for the soft finishing of various textiles.

Use a lot of chemical industry raw materials in the petrochemical field, often use reation kettle in the equipment of production silicone oil, but traditional reation kettle degree of automation is low when using for the chemical properties of silicone oil can not obtain good release, and reation kettle simultaneously can't examine the temperature and the pressure of amino-silicone oil in amino-silicone oil synthetic process and control, and the synthetic speed of stirring is low.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide an amino silicone oil synthetic automation equipment aims at solving the problem that traditional amino silicone oil synthetic degree of automation among the prior art is low and can't carry out the inspection to amino silicone oil's temperature and pressure and control.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides an automatic device that amino-silicone oil is synthetic, includes the reation kettle casing, one side fixed mounting of reation kettle casing has the fixture block, the internally mounted of fixture block has the baffle, one side block inside and reation kettle shells inner wall is arranged in to one side of baffle, electric telescopic handle is installed at the top of baffle, and partly separates to first cavity and second cavity in the reation kettle casing, the mid-mounting of reation kettle casing opposite side has the vacuum machine, the inside of second cavity is arranged in to the air inlet of vacuum machine, the bottom fixed mounting of vacuum machine has the gas outlet, the bottom fixed mounting of second cavity one side has the heater, the bottom fixed mounting who states second cavity one side has the barometer, one side fixed mounting of first cavity and second cavity has the observation window.

Further, the baffle is installed to the bottom of second cavity, the fluid-discharge tube is installed to one side of second cavity, the flowing back valve is installed at the top of fluid-discharge tube, the middle part of baffle alternates and is connected with first bull stick, the outside fixed mounting of first bull stick has a plurality of puddler, the air pump is installed to the bottom of baffle, the inside of second cavity and one side fixed connection of gas pitcher are arranged respectively in to the gas outlet and the air inlet of air pump, the bottom of first bull stick and driving motor's transmission end fixed connection.

Further, servo motor is installed at the top of reation kettle casing, servo motor's transmission end fixed mounting has the second bull stick, the avris fixed mounting of second bull stick has the stirring rod, one side fixed mounting at reation kettle casing top has the pan feeding mouth, the bottom fixed mounting of pan feeding mouth has the conveying pipeline, the inside of reation kettle casing is arranged in to the one end of conveying pipeline, and the stick that vibrates is installed to the opposite side at reation kettle casing top, the top fixed mounting of the stick that vibrates has the vibrator.

Furthermore, two sides of the bottom end of the reaction kettle shell are fixedly provided with a support.

Further, one side fixed mounting of reation kettle casing has the PLC controller, electric telescopic handle, vacuum machine, heater, air pump, driving motor, servo motor and vibrator and PLC controller electric connection.

Compared with the prior art, the beneficial effects of the utility model are that: this kind of synthetic automation equipment of amino-silicone oil, mutually support through servo motor and the stirring rod that sets up, be convenient for stir the inside amino-silicone oil synthetic raw materials of first cavity, carry out preliminary even abundant vibration to amino-silicone oil synthetic raw materials and mix, thereby improve synthetic efficiency, through mutually supporting of the heater that sets up and vacuum machine, slowly begin the inside gas of evacuation second cavity, and control gas second cavity atmospheric pressure through the barometer, the inside temperature of second cavity is guaranteed in the heater heating, nitrogen gas through air pump output blows away moisture, improve the viscosity of emulsification, improve the yield of silicon oil.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:

fig. 1 is a schematic structural view of the present invention;

fig. 2 is a top view of the present invention.

In the figure: 1. a reaction kettle shell; 11. a clamping block; 111. a baffle plate; 112. an electric telescopic rod; 12. a vacuum machine; 13. a heater; 14. a barometer; 15. an observation window; 2. a first cavity; 3. a second cavity; 31. a partition plate; 32. a liquid discharge pipe; 33. a first rotating lever; 331. a stirring rod; 34. an air pump; 35. a gas tank; 36. a drive motor; 4. a servo motor; 41. a second rotating rod; 42. a stirring rod; 43. a feeding port; 431. a delivery pipe; 44. vibrating a tamper; 441. a vibrator.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-2, the present invention provides the following technical solutions: the utility model provides an amino silicone oil synthetic automation equipment, including reation kettle casing 1, one side fixed mounting of reation kettle casing 1 has fixture block 11, the internally mounted of fixture block 11 has baffle 111, one side block of inside and the reation kettle casing 1 inner wall of reation kettle casing 1 is arranged in to one side of baffle 111, electric telescopic handle 112 is installed at the top of baffle 111, and 1 internally divided of reation kettle casing is first cavity 2 and second cavity 3, the mid-mounting of reation kettle casing 1 opposite side has vacuum machine 12, the inside of second cavity 3 is arranged in to the air inlet of vacuum machine 12, the bottom fixed mounting of vacuum machine 12 has the gas outlet, the bottom fixed mounting of 3 one sides of second cavity has heater 13, state the bottom fixed mounting of 3 one sides of second cavity and have barometer 14, one side fixed mounting of first cavity 2 and second cavity 3 has observation window 15.

As an optimized mode of the utility model, baffle 31 is installed to the bottom of second cavity 3, fluid-discharge tube 32 is installed to one side of second cavity 3, the flowing back valve is installed at the top of fluid-discharge tube 32, baffle 31's middle part interlude is connected with first bull stick 33, the outside fixed mounting of first bull stick 33 has a plurality of puddler 331, air pump 34 is installed to baffle 31's bottom, second cavity 3's inside and gas pitcher 35's one side fixed connection are arranged respectively in to air pump 34's gas outlet and air inlet, the bottom of first bull stick 33 and driving motor 36's transmission end fixed connection, be convenient for separate reation kettle casing 1 inside through the baffle 31 that sets up.

As the utility model discloses an optimal mode, servo motor 4 is installed at reation kettle casing 1's top, servo motor 4's transmission end fixed mounting has second bull stick 41, the avris fixed mounting of second bull stick 41 has stirring rod 42, one side fixed mounting at reation kettle casing 1 top has pan feeding mouth 43, the bottom fixed mounting of pan feeding mouth 43 has conveying pipeline 431, reation kettle casing 1's inside is arranged in to conveying pipeline 431's one end, the stick 44 that vibrates is installed to the opposite side at reation kettle casing 1 top, the top fixed mounting of the stick 44 that vibrates has vibrator 441, the stick 44 that vibrates through the setting vibrates the silicon oil raw materials, the synthesis of the silicon oil of being convenient for.

As an optimized mode of the utility model, the both sides fixed mounting of 1 bottom of reation kettle casing has the support, supports reation kettle casing 1 through the support that sets up.

As an optimized mode of the utility model, one side fixed mounting of reation kettle casing 1 has the PLC controller, and electric telescopic handle 112, vacuum machine 12, heater 13, air pump 34, driving motor 36, servo motor 4 and vibrator 441 and PLC controller electric connection are convenient for control the electrical equipment on the synthetic automation equipment of amino-silicone oil through flush mounting plate.

The utility model discloses a theory of operation does: when the device is used, firstly, amino silicone oil synthetic raw materials are put into a stainless steel reaction kettle along a material conveying pipe 431 through a material inlet 43, a servo motor 4 is opened through a PLC (programmable logic controller), the servo motor 4 starts to rotate to drive a second rotating rod 41 and a stirring rod 42 to stir the amino silicone oil synthetic raw materials in a first cavity 2, meanwhile, the PLC opens a vibrator 441 to drive a vibrating rod 44 to preliminarily, uniformly and fully vibrate and mix the amino silicone oil synthetic raw materials in the first cavity 2, after the mixing and stirring are completed, a baffle 111 is driven to slide out from the inside of a reaction kettle shell 1 through the stretching of an electric telescopic rod 112, the amino silicone oil synthetic raw materials in the first cavity 2 enter the inside of a second cavity 3, a catalyst is added through the material inlet 43, the baffle 111 is driven to close the inside of the reaction kettle shell 1 through the stretching of the electric telescopic rod 112 through the PLC, turning on a heater 13 to heat the inside of the second cavity 3, simultaneously turning on a driving motor 36 to drive a first rotating rod 33 to stir the inside of the second cavity 3, slowly starting to vacuumize the gas inside the second cavity 3 through a vacuum machine 12, monitoring the gas pressure of the second cavity 3 through a barometer 14, gradually increasing the vacuum degree along with stirring, normally keeping the temperature inside the second cavity 3 of the heater 13, observing the gas pressure inside the second cavity 3 through the barometer 14, conveying nitrogen inside a gas tank 35 into the second cavity 3 through an arranged gas pump 34, blowing away moisture through the nitrogen, observing for 45min through an observation window 15 until no water drops exist on the second cavity 3 basically, stopping vacuumizing, stirring for 1h at the same temperature and vacuumizing again, repeating the steps until the proper viscosity is reached, sampling and measuring the viscosity are needed, stopping vacuumizing and heating when the viscosity meets the requirement, and opening a manhole cover and a feeding hole on an end socket of the reaction kettle shell 1, stopping stirring and standing overnight, discharging materials in the next morning, reacting for 5-6 hours, and standing overnight, wherein the viscosity of the amino silicone oil can reach 6000-7000 mPa 7S.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. The utility model provides an automatic device for amino silicone oil synthesis, includes reation kettle casing (1), its characterized in that, one side fixed mounting of reation kettle casing (1) has fixture block (11), the internally mounted of fixture block (11) has baffle (111), one side of baffle (111) is arranged in one side block of inside and reation kettle casing (1) inner wall of reation kettle casing (1), electric telescopic handle (112) are installed at the top of baffle (111), and reation kettle casing (1) internal partitioning is first cavity (2) and second cavity (3), the mid-mounting of reation kettle casing (1) opposite side has vacuum machine (12), the inside of second cavity (3) is arranged in to the air inlet of vacuum machine (12), the bottom fixed mounting of vacuum machine (12) has the gas outlet, the bottom fixed mounting of second cavity (3) one side has heater (13), the bottom end of one side of the second cavity (3) is fixedly provided with a barometer (14), and one sides of the first cavity (2) and the second cavity (3) are fixedly provided with an observation window (15).

2. The automatic device for amino silicone oil synthesis according to claim 1, wherein a partition plate (31) is installed at the bottom end of the second cavity (3), a liquid discharge pipe (32) is installed on one side of the second cavity (3), a liquid discharge valve is installed at the top of the liquid discharge pipe (32), a first rotating rod (33) is connected to the middle of the partition plate (31) in an inserting manner, a plurality of stirring rods (331) are fixedly installed on the outer side of the first rotating rod (33), an air pump (34) is installed at the bottom end of the partition plate (31), an air outlet and an air inlet of the air pump (34) are respectively and fixedly connected to the inside of the second cavity (3) and one side of an air tank (35), and the bottom end of the first rotating rod (33) is fixedly connected to a transmission end of a driving motor (36).

3. The automatic device for amino silicone oil synthesis according to claim 2, wherein a servo motor (4) is installed at the top of the reaction kettle shell (1), a second rotating rod (41) is fixedly installed at the transmission end of the servo motor (4), a stirring rod (42) is fixedly installed at the side of the second rotating rod (41), a feeding port (43) is fixedly installed at one side of the top of the reaction kettle shell (1), a conveying pipeline (431) is fixedly installed at the bottom end of the feeding port (43), one end of the conveying pipeline (431) is arranged in the reaction kettle shell (1), a vibrating rod (44) is installed at the other side of the top of the reaction kettle shell (1), and a vibrator (441) is fixedly installed at the top of the vibrating rod (44).

4. The automatic amino silicone oil synthesis device according to claim 1, wherein supports are fixedly mounted on two sides of the bottom end of the reaction kettle shell (1).

5. The automatic amino silicone oil synthesis device as claimed in claim 3, wherein a PLC controller is fixedly installed on one side of the reaction kettle housing (1), and the electric telescopic rod (112), the vacuum machine (12), the heater (13), the air pump (34), the driving motor (36), the servo motor (4) and the vibrator (441) are electrically connected with the PLC controller.