CN212954954U - Vacuum distillation device for o-aminophenol filter cake - Google Patents
Vacuum distillation device for o-aminophenol filter cake Download PDFInfo
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- CN212954954U CN212954954U CN202021155631.8U CN202021155631U CN212954954U CN 212954954 U CN212954954 U CN 212954954U CN 202021155631 U CN202021155631 U CN 202021155631U CN 212954954 U CN212954954 U CN 212954954U
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Abstract
The utility model discloses a vacuum distillation device for an o-aminophenol filter cake, the top end of a tank body is connected with a tank cover, the tank cover is also provided with a vacuum pump and a condenser interface, the condenser interface is connected with a condenser through a condenser connecting pipe, the surface of the outer side of the tank body is provided with a jacket, the bottom end of a stirring tank is provided with a connecting channel, the lower end of the connecting channel is connected with the upper surface of a feeding screw mechanism, one end of the feeding screw mechanism is connected with the side wall of the tank body, a second stirrer comprises a main shaft, connecting rods, vertical rods and bottom rods, two sides of the main shaft are respectively connected with the vertical rods through a plurality of connecting rods, the bottom rods are arranged at the bottom ends of the vertical rods at two sides, one end of the vertical rod far away from the main shaft is connected with the inner wall of the tank body, the lower surface of the bottom, stirring distillation is carried out through the second stirrer, and the distillation effect is greatly improved.
Description
Technical Field
The utility model relates to an o aminophenol vacuum distillation equipment technical field for the filter cake specifically is a vacuum distillation device for o aminophenol filter cake.
Background
Traditional vacuum distillation equipment for ortho-aminophenol filter cake stirs only through the stirring in the retort main part, breaks up the effect relatively poor to when the stirring, the residue can be attached on the inner wall of the jar body, influences the distillation effect, also causes certain influence to the washing in later stage simultaneously, consequently, this problem that exists among the prior art is solved to a quick-witted improved technique of awaiting the opportune moment.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a vacuum distillation device for ortho-aminophenol filter cake, cross and be provided with just stirring mechanism in jar body one side, realize the first time of ortho-aminophenol filter cake and break up, after entering into a jar internal portion, stir the distillation through the second agitator, the distillation effect improves greatly, the pole setting and the sill bar of second agitator meet in the inside wall and the bottom of jar body respectively, when guaranteeing the internal portion stirring of jar, the cake sediment can not paste on the inner wall, and when the later stage washs, guarantee can not adhere to on the inner wall, with the problem of proposing in solving above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: a vacuum distillation device for an o-aminophenol filter cake comprises a main body, a primary stirring mechanism and a secondary stirring mechanism;
the main body comprises a tank body, a tank cover, a motor base, a vacuum pump, a condenser interface, a condenser connecting pipe, a condenser, supporting legs, a slag discharge port, an observation flange, a jacket, a steam outlet, a steam inlet, a condensate discharge port and a water inlet, wherein the top end of the tank body is connected with the tank cover, the motor base is arranged at the central position of the upper surface of the tank cover, the vacuum pump and the condenser interface are also arranged on the tank cover, the condenser interface is connected with the condenser connecting pipe, one end of the condenser connecting pipe, far away from the condenser connecting pipe, is connected with the condenser, the supporting legs are arranged on the outer side of the bottom end of the tank body, the slag discharge port is arranged at the central position of the bottom end of the tank body, the observation flange is arranged below the side wall of the tank body, the, a water inlet is formed in the position, above the jacket, of the upper end surface of the tank body;
the primary stirring mechanism comprises a stirring tank, a first stirring motor, a first stirrer, a feed inlet, a connecting channel and a feeding screw mechanism, wherein the first stirring motor and the feed inlet are arranged on the upper surface of the stirring tank;
the secondary stirring mechanism comprises a second stirring motor and a second stirrer, the second stirring motor is connected with the motor base on the upper surface of the tank cover, the second stirring motor is connected with the second stirrer, and the second stirrer is arranged in the tank body; the second agitator includes main shaft, connecting rod, pole setting and sill bar, the main shaft both sides link to each other with the pole setting through a plurality of connecting rods respectively, both sides the pole setting bottom is provided with the sill bar, the pole setting is kept away from main shaft one end and is met with the inner wall of the jar body, the sill bar lower surface meets with jar body bottom surface.
Preferably, the utility model provides a pair of vacuum distillation device is used to ortho-aminophenol filter cake, wherein, all be provided with the valve on interface channel and the row's cinder notch, be used for controlling unloading and ejection of compact respectively.
Preferably, the utility model provides a pair of vacuum distillation device is used to ortho-aminophenol filter cake, wherein, the pay-off screw mechanism lower surface passes through the bracing support and links to each other with the jar body to improve the stability and the intensity of just stirring the mechanism.
Preferably, the utility model provides a pair of vacuum distillation device is used to adjacent aminophenol filter cake, wherein, pay-off screw rod mechanism includes a pay-off section of thick bamboo, gear motor and feeding screw, pay-off section of thick bamboo one end links to each other with the lateral wall of the jar body, the pay-off section of thick bamboo other end is provided with gear motor, gear motor links to each other with feeding screw, feeding screw sets up in a pay-off section of thick bamboo, realizes the intercommunication of agitator tank and jar body through this structure.
Preferably, the utility model provides a pair of vacuum distillation device is used to ortho-aminophenol filter cake, wherein, jar body upper end outside surface still is provided with the support, the support links to each other with the condenser, guarantees the stability of condenser.
Preferably, the utility model provides a pair of vacuum distillation device for ortho-aminophenol filter cake, wherein, every the outside of supporting leg still is provided with auxiliary stay frame, guarantees holistic stability.
Compared with the prior art, the beneficial effects of the utility model are that:
(1) through be provided with at jar body one side and just stir the mechanism, realize breaking up for the first time of ortho-aminophenol filter cake, after entering into jar internal portion, stir the distillation through the second agitator, the distillation effect improves greatly.
(2) The pole setting and the sill bar of second agitator meet in the inside wall and the bottom of jar body respectively, guarantee when jar internal portion stirring, the cake sediment can not paste on the inner wall to when later stage washs, guarantee can not adhere to on the inner wall.
(3) Be provided with the observation flange on the jar body lateral wall, firstly can carry out inside observation, secondly can open and maintain or clear up inside.
(4) All be provided with auxiliary stay frame on every supporting leg, guarantee holistic stability.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of a second agitator;
fig. 3 is a schematic structural view of a feeding screw mechanism.
In the figure: the device comprises a tank body 1, a tank cover 2, a motor base 3, a vacuum pump 4, a condenser interface 5, a condenser 6, support legs 7, a slag discharge port 8, an observation flange 9, a jacket 10, a steam outlet 11, a steam inlet 12, a condensate discharge port 13, a water inlet 14, a stirring tank 15, a first stirring motor 16, a first stirrer 17, a feed inlet 18, a connecting channel 19, a feeding screw mechanism 20, a second stirring motor 21, a second stirrer 22, an inclined support bracket 23, a support 24, an auxiliary support bracket 25, a feeding barrel 201, a speed reducing motor 202, a feeding screw 203, a main shaft 221, a connecting rod 222, an upright rod 223 and a bottom rod 224.
Detailed Description
The technical solution of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those skilled in the art without creative efforts belong to the protection scope of the present invention;
it should be noted that, in the description of the present invention, it is to be noted that the terms "inside", "outside", "upper", "lower", "both sides", "one end", "the other end", "left", "right", and the like indicate the directions or positional relationships based on the directions or positional relationships shown in the drawings, and are only for convenience of description and simplification of the present invention, and do not indicate or imply that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and thus, should not be construed as limiting the present invention.
Referring to fig. 1, the present invention provides a technical solution: a vacuum distillation device for an o-aminophenol filter cake comprises a main body, a primary stirring mechanism and a secondary stirring mechanism; the main body comprises a tank body 1, a tank cover 2, a motor base 3, a vacuum pump 4, a condenser interface 5, a condenser 6, supporting legs 7, a slag discharge port 8, an observation flange 9, a jacket 10, a steam outlet 11, a steam inlet 12, a condensate discharge port 13 and a water inlet 14, wherein the top end of the tank body 1 is connected with the tank cover 2, the motor base 3 is arranged at the central position of the upper surface of the tank cover 2, the vacuum pump 4 and the condenser interface 5 are also arranged on the tank cover 2, the condenser interface 5 is connected through a condenser connecting pipe, one end of the condenser connecting pipe, far away from the condenser interface 5 pipe, is connected with the condenser 6, a support 24 is also arranged on the outer side surface of the upper end of the tank body 1, the supporting legs 7 are arranged on the outer side of the bottom end of the tank body 1, an auxiliary support frame 25 is also arranged on the, the outer side surface of the tank body 1 is provided with a jacket 10, the upper end of the jacket 10 is provided with a steam outlet 11, the lower surface end of the jacket 10 is provided with a steam inlet 12 and a condensate outlet 13, and the upper end surface of the tank body 1 is provided with a water inlet 14 above the jacket 10; the primary stirring mechanism comprises a stirring tank 15, a first stirring motor 16, a first stirrer 17, a feeding port 18, a connecting channel 19 and a feeding screw rod mechanism 20, the first stirring motor 16 and the feeding port 18 are arranged on the upper surface of the stirring tank 15, the first stirring motor 16 is connected with the first stirrer 17, the first stirrer 17 is arranged in the stirring tank 15, the connecting channel 19 is arranged at the bottom end of the stirring tank 15, the lower end of the connecting channel 19 is connected with the upper surface of the feeding screw rod mechanism 20, valves are arranged on the connecting channel 19 and a slag discharge port 8, one end of the feeding screw rod mechanism 20 is connected with the side wall of the tank body 1, and the lower surface of the feeding screw rod mechanism 20 is connected with the tank body 1 through an inclined support 23; the second stirring mechanism comprises a second stirring motor 21 and a second stirrer 22, the second stirring motor 21 is connected with the motor base 3 on the upper surface of the tank cover 2, the second stirring motor 21 is connected with the second stirrer 22, and the second stirrer 22 is arranged inside the tank body 1.
As shown in fig. 2, the second stirrer 22 comprises a main shaft 221, connecting rods 222, vertical rods 223 and bottom rods 224, wherein two sides of the main shaft 221 are respectively connected with the vertical rods 223 through the connecting rods 222, the bottom ends of the vertical rods 223 at two sides are provided with the bottom rods 224, one end of the vertical rod 223 far away from the main shaft 221 is connected with the inner wall of the tank body 1, and the lower surface of the bottom rod 224 is connected with the bottom end surface of the tank body 1.
As shown in fig. 3, the feeding screw mechanism 20 includes a feeding barrel 201, a speed reduction motor 202 and a feeding screw 203, one end of the feeding barrel 201 is connected to the side wall of the tank body 1, the speed reduction motor 202 is arranged at the other end of the feeding barrel 201, the speed reduction motor 202 is connected to the feeding screw 203, and the feeding screw 203 is arranged in the feeding barrel 201.
The use method and the principle are as follows: sending the o-aminophenol filter cake into stirring the jar from feed inlet 18, drive first agitator 17 through first agitator motor 16 and rotate, stir and break up the filter cake for the first time, open the valve of connecting channel 19 afterwards, the crushed aggregates enters into material feeding screw mechanism 20, enter into jar internal portion 1 through pay-off screw 203, open vacuum pump 4, with jar internal portion 1 vacuum treatment, send high temperature steam into from steam inlet 12 in pressing from both sides cover 10 again, open second agitator motor 21, second agitator motor 21 drives second agitator 22 and rotates, stir and distill the crushed aggregates of inside o-aminophenol, inside steam enters into the condenser connecting pipe from the condenser interface 5 of top, enter into condenser 6 again, the condensation obtains o-aminophenol. The utility model has reasonable structure, realizes the primary scattering of the o-aminophenol filter cake by arranging the primary stirring mechanism at one side of the tank body 1, and after entering the tank body 1, the distillation effect is greatly improved by stirring and distilling through the second stirrer 22; the upright rod 223 and the bottom rod 224 of the second stirrer 22 are respectively connected with the inner side wall and the bottom end of the tank body 1, so that the cake dregs are not attached to the inner wall when the inside of the tank body 1 is stirred, and the cake dregs are not attached to the inner wall when the later-stage cleaning is carried out; an observation flange 9 is arranged on the side wall of the tank body 1, so that the inside of the tank body can be observed, and the inside of the tank body can be maintained or cleaned by opening the tank body; all be provided with auxiliary stay frame 25 on every supporting leg 7, guarantee holistic stability.
The details of the present invention are well known to those skilled in the art.
Finally, it is to be noted that: the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to the examples, it should be understood by those skilled in the art that the technical solutions of the present invention can be modified and replaced with equivalents without departing from the spirit and scope of the technical solutions of the present invention, which should be covered by the scope of the claims of the present invention.
Claims (6)
1. The utility model provides an ortho-aminophenol vacuum distillation plant for filter cake which characterized in that: comprises a main body, a primary stirring mechanism and a secondary stirring mechanism;
the main body comprises a tank body (1), a tank cover (2), a motor base (3), a vacuum pump (4), a condenser interface (5), a condenser connecting pipe, a condenser (6), supporting legs (7), a slag discharge port (8), an observation flange (9), a jacket (10), a steam outlet (11), a steam inlet (12), a condensate discharge port (13) and a water inlet (14), wherein the top end of the tank body (1) is connected with the tank cover (2), the motor base (3) is arranged at the central position of the upper surface of the tank cover (2), the vacuum pump (4) and the condenser interface (5) are also arranged on the tank cover (2), the condenser interface (5) is connected with the condenser connecting pipe, one end, away from the condenser interface (5), of the condenser connecting pipe is connected with the condenser (6), and the supporting legs (7) are arranged on the outer, a slag discharge port (8) is formed in the center of the bottom end of the tank body (1), an observation flange (9) is arranged below the side wall of the tank body (1), a jacket (10) is arranged on the outer side surface of the tank body (1), a steam outlet (11) is formed in the upper end of the jacket (10), a steam inlet (12) and a condensate discharge port (13) are formed in the lower surface end of the jacket (10), and a water inlet (14) is formed in the position, above the jacket (10), of the upper end surface of the tank body (1);
the preliminary stirring mechanism comprises a stirring tank (15), a first stirring motor (16), a first stirrer (17), a feeding port (18), a connecting channel (19) and a feeding screw rod mechanism (20), wherein the first stirring motor (16) and the feeding port (18) are arranged on the upper surface of the stirring tank (15), the first stirring motor (16) is connected with the first stirrer (17), the first stirrer (17) is arranged in the stirring tank (15), the connecting channel (19) is arranged at the bottom end of the stirring tank (15), the lower end of the connecting channel (19) is connected with the upper surface of the feeding screw rod mechanism (20), and one end of the feeding screw rod mechanism (20) is connected with the side wall of the tank body (1);
the secondary stirring mechanism comprises a second stirring motor (21) and a second stirrer (22), the second stirring motor (21) is connected with the motor base (3) on the upper surface of the tank cover (2), the second stirring motor (21) is connected with the second stirrer (22), and the second stirrer (22) is arranged in the tank body (1); second agitator (22) includes main shaft (221), connecting rod (222), pole setting (223) and sill bar (224), main shaft (221) both sides are continuous with pole setting (223) through a plurality of connecting rods (222) respectively, both sides pole setting (223) bottom is provided with sill bar (224), main shaft (221) one end is kept away from in pole setting (223) meets with the inner wall of jar body (1), sill bar (224) lower surface meets with jar body (1) bottom surface.
2. The vacuum distillation apparatus for the filter cake of ortho-aminophenol according to claim 1, wherein: valves are arranged on the connecting channel (19) and the slag discharging port (8).
3. The vacuum distillation apparatus for the filter cake of ortho-aminophenol according to claim 1, wherein: the lower surface of the feeding screw rod mechanism (20) is connected with the tank body (1) through an inclined strut bracket (23).
4. The vacuum distillation apparatus for the filter cake of ortho-aminophenol according to claim 1, wherein: the feeding screw mechanism (20) comprises a feeding barrel (201), a speed reducing motor (202) and a feeding screw (203), one end of the feeding barrel (201) is connected with the side wall of the tank body (1), the speed reducing motor (202) is arranged at the other end of the feeding barrel (201), the speed reducing motor (202) is connected with the feeding screw (203), and the feeding screw (203) is arranged in the feeding barrel (201).
5. The vacuum distillation apparatus for the filter cake of ortho-aminophenol according to claim 1, wherein: the outer side surface of the upper end of the tank body (1) is further provided with a support (24), and the support (24) is connected with the condenser (6).
6. The vacuum distillation apparatus for the filter cake of ortho-aminophenol according to claim 1, wherein: and the outer side of each supporting leg (7) is also provided with an auxiliary supporting frame (25).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021155631.8U CN212954954U (en) | 2020-06-21 | 2020-06-21 | Vacuum distillation device for o-aminophenol filter cake |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021155631.8U CN212954954U (en) | 2020-06-21 | 2020-06-21 | Vacuum distillation device for o-aminophenol filter cake |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212954954U true CN212954954U (en) | 2021-04-13 |
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ID=75387430
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021155631.8U Active CN212954954U (en) | 2020-06-21 | 2020-06-21 | Vacuum distillation device for o-aminophenol filter cake |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212954954U (en) |
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2020
- 2020-06-21 CN CN202021155631.8U patent/CN212954954U/en active Active
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