CN212881874U - Sulfur melting equipment with purifying effect for producing phosphorus pentasulfide - Google Patents
Sulfur melting equipment with purifying effect for producing phosphorus pentasulfide Download PDFInfo
- Publication number
- CN212881874U CN212881874U CN202021367005.5U CN202021367005U CN212881874U CN 212881874 U CN212881874 U CN 212881874U CN 202021367005 U CN202021367005 U CN 202021367005U CN 212881874 U CN212881874 U CN 212881874U
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- China
- Prior art keywords
- sulfur
- cooler
- water
- sulfur melting
- phosphorus pentasulfide
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- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 68
- 239000011593 sulfur Substances 0.000 title claims abstract description 51
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 51
- 238000002844 melting Methods 0.000 title claims abstract description 40
- 230000008018 melting Effects 0.000 title claims abstract description 40
- CYQAYERJWZKYML-UHFFFAOYSA-N phosphorus pentasulfide Chemical compound S1P(S2)(=S)SP3(=S)SP1(=S)SP2(=S)S3 CYQAYERJWZKYML-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 230000000694 effects Effects 0.000 title claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 41
- 238000006243 chemical reaction Methods 0.000 claims abstract description 25
- 239000012528 membrane Substances 0.000 claims abstract description 17
- 230000007246 mechanism Effects 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 12
- 239000010410 layer Substances 0.000 claims description 40
- 239000003054 catalyst Substances 0.000 claims description 23
- 238000000746 purification Methods 0.000 claims description 19
- 239000005864 Sulphur Substances 0.000 claims description 16
- 238000009833 condensation Methods 0.000 claims description 15
- 230000005494 condensation Effects 0.000 claims description 15
- 238000004519 manufacturing process Methods 0.000 claims description 14
- 239000011229 interlayer Substances 0.000 claims description 13
- 238000010438 heat treatment Methods 0.000 claims description 11
- 238000004321 preservation Methods 0.000 claims description 6
- 229910001570 bauxite Inorganic materials 0.000 claims description 3
- 239000012466 permeate Substances 0.000 claims 8
- 238000007599 discharging Methods 0.000 claims 2
- 239000007789 gas Substances 0.000 abstract description 22
- 230000003197 catalytic effect Effects 0.000 abstract description 10
- 238000001816 cooling Methods 0.000 abstract description 10
- 238000000034 method Methods 0.000 abstract description 6
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract description 4
- 239000000498 cooling water Substances 0.000 abstract description 4
- 229910000037 hydrogen sulfide Inorganic materials 0.000 abstract description 4
- 230000008569 process Effects 0.000 abstract description 4
- 239000002699 waste material Substances 0.000 abstract description 2
- 230000009471 action Effects 0.000 description 3
- 239000006260 foam Substances 0.000 description 3
- 239000003595 mist Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The utility model discloses a sulfur melting device with purifying effect for producing phosphorus pentasulfide, which comprises a sulfur melting kettle and a purifying mechanism, wherein the purifying mechanism is arranged on one side of the sulfur melting kettle, sulfur in the sulfur melting kettle is heated to become mixed gas, the mixed gas is changed into liquid sulfur through a cooler, the liquid sulfur reacts with the inside of a catalytic converter to generate gaseous sulfur and water, the gaseous sulfur is cooled and formed through a solidifying pipe to become sulfur, a small part of tail gas is combusted and can be discharged to the atmosphere, so that the sulfur melting kettle has the purifying function, the natural environment is protected, a reaction layer is arranged in the catalytic converter, the reaction layer reacts with hydrogen sulfide to generate gaseous sulfur and water, the gaseous sulfur and water flow out of the catalytic converter through a permeable membrane and a water outlet, the purifying device further processes gas, the generated water can be used in other aspects, the resource waste is avoided, because of different required temperatures of gas cooling, the tail end of a condensing pipe is connected with the top of the, the cooling water in the condenser pipe can be used for cooling the inside of the cooler, so that the equipment reduces the requirement of condensed water.
Description
Technical Field
The utility model relates to a sulfur melting kettle technical field specifically is a sulfur melting equipment is used in phosphorus pentasulfide production with purifying effect.
Background
The sulfur melting kettle is a jacket container, steam is introduced into the jacket to heat sulfur foam, when the sulfur foam is heated to 70-90 ℃, the foam is broken, and tiny particles of elemental sulfur are rapidly aggregated and increased to be separated from the desulfurization solution.
The existing sulfur melting equipment for phosphorus pentasulfide production has no purification device for sulfur tail gas after heating, the discharged tail gas does not meet the national standard, the environment is damaged, other components contained in the tail gas are not utilized, the waste is caused, and the amount of condensed water required by tail gas condensation is huge.
To the problem, the utility model provides a production of phosphorus pentasulfide is with melting sulphur equipment with purifying effect.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a production of phosphorus pentasulfide is with melting sulphur equipment with purifying effect, possessed tail gas purification, tail gas is recycled, reduces the advantage of the quantity of comdenstion water to solved and not had purifier among the background art, had not utilized the device to the composition in the tail gas, the big problem of comdenstion water quantity.
In order to achieve the above object, the utility model provides a following technical scheme: the sulfur melting equipment with the purification effect for producing the phosphorus pentasulfide comprises a sulfur melting kettle and a purification mechanism, wherein the purification mechanism is arranged on one side of the sulfur melting kettle, the sulfur melting kettle comprises a kettle body and an interlayer, the interlayer is arranged in the kettle body, the kettle body comprises a feed inlet and a discharge outlet, the feed inlet is arranged at the upper end of one side of the outer surface of the kettle body, the discharge outlet is arranged at the bottom end of the outer surface of the kettle body, the interlayer comprises a heating layer and a heat preservation layer, the heating layer and the heat preservation layer are arranged in the interlayer, and the heat preservation layer is arranged;
purification mechanism includes siphunculus, cooler, catalyst converter, flow tube and coagulator, and cauldron body surface upper end one side is connected to siphunculus top one side, and the cooler top is connected to the siphunculus bottom, and the catalyst converter top is connected to the cooler bottom, and flow tube bottom one side is connected in catalyst converter surface one side, and the flow tube top is connected with coagulator one end.
Preferably, the cooler includes hose, liquid outlet and connecting pipe, and the hose setting is inside the cooler, and the hose top is connected with the siphunculus bottom, and the liquid outlet setting is in the cooler bottom, and the connecting pipe bottom is connected on the cooler top.
Preferably, the catalyst converter includes reaction layer, permeable membrane, porous disk and delivery port, and the catalyst converter bottom is equipped with the delivery port, and reaction layer, permeable membrane and porous disk setting are inside the catalyst converter, and the porous disk setting is equipped with the permeable membrane at the inside lower extreme of catalyst converter on the surface top of porous disk, and the reaction layer setting is on the permeable membrane top, and the flow tube is connected in the reaction layer upper end.
Preferably, the coagulator comprises a condensation pipe, a cover, a handle and a water inlet, the condensation pipe is wound on the outer surface of the coagulator, the water inlet is formed in one end of the condensation pipe, the other end of the condensation pipe is connected with the top end of the connecting pipe, the cover is arranged at the top of the other end of the coagulator, and the handle is connected with the top end of the cover.
Preferably, the reaction layer is a member made of natural bauxite.
Compared with the prior art, the beneficial effects of the utility model are as follows:
1. the utility model provides a sulfur melting equipment is used in phosphorus pentasulfide production with purifying effect, sulfur in the sulfur melting cauldron becomes the mist through the heating, becomes liquid sulfur through the cooler, generates gaseous state sulphur and water with the inside reaction of catalyst converter, and gaseous state sulphur becomes sulfur through solidifying the pipe cooling shaping, and the atmosphere can be arranged to the fractional tail gas through burning for the sulfur melting cauldron possesses purification performance, protects natural environment.
2. The utility model provides a phosphorus pentasulfide production with melting sulphur equipment with purifying effect sets up the reaction layer inside the catalyst converter, and the reaction layer reacts with hydrogen sulfide, generates gaseous state sulphur and water, through permeating water membrane and delivery port outflow catalyst converter for clarification plant is to gaseous further processing, and the water of formation can be used to other aspects, has avoided the wasting of resources.
3. The utility model provides a phosphorus pentasulfide production is with melting sulphur equipment with purifying effect, because gas cooling's required temperature is different, is connected the condenser pipe tail end with the cooler top, and the cooling water in the condenser pipe can be used to the inside cooling that cools off of cooler for equipment has reduced the demand to the comdenstion water.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic structural view of the purifying mechanism of the present invention;
FIG. 3 is a schematic view of the catalytic converter of the present invention;
fig. 4 is a schematic structural view of the coagulator of the present invention.
In the figure: 1. a sulfur melting kettle; 11. a kettle body; 111. a feed inlet; 112. a discharge port; 12. an interlayer; 121. a heating layer; 122. a heat-insulating layer; 2. a purification mechanism; 21. pipe passing; 22. a cooler; 221. a hose; 222. a liquid outlet; 223. a connecting pipe; 23. a catalyst; 231. a reaction layer; 232. a water permeable membrane; 233. a water permeable plate; 234. a water outlet; 24. a flow tube; 25. a coagulator; 251. a condenser tube; 252. a cover; 253. a handle; 254. a water inlet.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Please refer to fig. 1, a sulfur melting device for phosphorus pentasulfide production with purifying effect, comprising a sulfur melting kettle 1 and a purifying mechanism 2, wherein the purifying mechanism 2 is arranged on one side of the sulfur melting kettle 1, the sulfur melting kettle 1 comprises a kettle body 11 and an interlayer 12, the interlayer 12 is arranged inside the kettle body 11, the kettle body 11 comprises a feed inlet 111 and a discharge outlet 112, the feed inlet 111 is arranged at the upper end of one side of the outer surface of the kettle body 11, the discharge outlet 112 is arranged at the bottom end of the outer surface of the kettle body 11, the interlayer 12 comprises a heating layer 121 and a heat insulating layer 122, the heating layer 121 and the heat insulating layer 122 are arranged inside the interlayer 12, and the heat insulating layer.
Referring to fig. 2, the purification mechanism 2 includes a through pipe 21, a cooler 22, a catalyst 23, a flow pipe 24 and a coagulator 25, one side of the top end of the through pipe 21 is connected to one side of the upper end of the outer surface of the kettle 11, the bottom end of the through pipe 21 is connected to the top end of the cooler 22, the bottom end of the cooler 22 is connected to one side of the top end of the catalyst 23, one end of the flow pipe 24 is connected to one end of the coagulator 25, the cooler 22 includes a hose 221, a liquid outlet 222 and a connecting pipe 223, the hose 221 is disposed inside the cooler 22, the top end of the hose 221 is connected to the bottom end of the through pipe 21, the liquid outlet 222 is disposed at the bottom end of the cooler 22, the bottom end of the connecting pipe 223 is connected to the top end of the cooler 22, sulfur in the sulfur melting kettle 1 is heated to become mixed gas, the mixed gas is changed into liquid sulfur, a small part of tail gas can be discharged to the atmosphere after being combusted, so that the sulfur melting kettle 1 has a purification function and protects natural rings.
Referring to fig. 3, the catalytic converter 23 includes a reaction layer 231, a permeable membrane 232, a permeable plate 233 and a water outlet 234, the bottom end of the catalytic converter 23 is provided with the water outlet 234, the reaction layer 231, the permeable membrane 232 and the permeable plate 233 are disposed inside the catalytic converter 23, the permeable plate 233 is disposed at the lower end inside the catalytic converter 23, the permeable membrane 232 is disposed at the top end of the surface of the permeable plate 233, the reaction layer 231 is disposed at the top end of the permeable membrane 232, the flow pipe 24 is connected to the upper end of the reaction layer 231, the reaction layer 231 is a member made of natural bauxite, the reaction layer 231 is disposed inside the catalytic converter 23, the reaction layer 231 reacts with hydrogen sulfide to generate gaseous sulfur and water, and the gaseous sulfur and the water flow out of the catalytic converter 23 through the permeable membrane 232 and the water outlet 234, so that the purification apparatus further processes the gas, and the.
Referring to fig. 4, the condenser 25 includes a condensation pipe 251, a cover 252, a handle 253, and a water inlet 254, the condensation pipe 251 is wound around the outer surface of the condenser 25, one end of the condensation pipe 251 is provided with the water inlet 254, the other end of the condensation pipe 251 is connected to the top end of the connection pipe 223, the top end of the other end of the condenser 25 is provided with the cover 252, the top end of the cover 252 is connected to the handle 253, the tail end of the condensation pipe 251 is connected to the top of the cooler 22 due to different temperatures required for gas cooling, and cooling water in the condensation pipe 251 can be used for cooling the inside of the cooler 22, so that the.
In summary, the following steps: the utility model provides a sulfur melting equipment is used in phosphorus pentasulfide production with purifying effect, sulphur in sulfur melting cauldron 1 becomes the mist through the heating, become liquid sulphur through cooler 22, react with catalyst 23 inside and generate gaseous state sulphur and water, gaseous state sulphur becomes sulphur through coagulator 25 cooling forming, the small part tail gas is through burning, can arrange to the atmosphere, make sulfur melting cauldron 1 possess the purification performance, the natural environment is protected, catalyst 23 inside sets up reaction layer 231, reaction layer 231 reacts with hydrogen sulfide, generate gaseous state sulphur and water, flow out catalyst 23 through permeable membrane 232 and delivery port 234, make purifying equipment further handle gas, the water that generates can be used in other aspects, the wasting of resources has been avoided, because the required temperature of gas cooling is different, be connected condenser 251 tail end and cooler 22 top, the cooling water in the condenser can be used for the inside cooling of cooler 251, so that the device has a reduced need for condensate water.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (5)
1. The utility model provides a production of phosphorus pentasulfide with purifying effect is with melting sulphur equipment, includes melting sulphur cauldron (1) and purification mechanism (2), and purification mechanism (2) set up in melting sulphur cauldron (1) one side, its characterized in that: the sulfur melting kettle (1) comprises a kettle body (11) and an interlayer (12), the interlayer (12) is arranged inside the kettle body (11), the kettle body (11) comprises a feeding hole (111) and a discharging hole (112), the feeding hole (111) is arranged at the upper end of one side of the outer surface of the kettle body (11), the discharging hole (112) is arranged at the bottom end of the outer surface of the kettle body (11), the interlayer (12) comprises a heating layer (121) and a heat preservation layer (122), the heating layer (121) and the heat preservation layer (122) are arranged inside the interlayer (12), and the heat preservation layer (122) is arranged on the outer surface of the heating layer; purification mechanism (2) are including siphunculus (21), cooler (22), catalyst converter (23), flow tube (24) and coagulator (25), and siphunculus (21) top one side is connected cauldron body (11) surface upper end one side, and cooler (22) top is connected to siphunculus (21) bottom, and catalyst converter (23) top is connected to cooler (22) bottom, and flow tube (24) bottom one side is connected in catalyst converter (23) surface one side, and flow tube (24) top is connected with coagulator (25) one end.
2. The sulfur melting equipment with purification effect for phosphorus pentasulfide production according to claim 1, wherein: cooler (22) include hose (221), liquid outlet (222) and connecting pipe (223), and hose (221) set up inside cooler (22), and hose (221) top is connected with siphunculus (21) bottom, and liquid outlet (222) set up in cooler (22) bottom, and connecting pipe (223) bottom is connected on cooler (22) top.
3. The sulfur melting equipment with purification effect for phosphorus pentasulfide production according to claim 1, wherein: catalyst converter (23) is including reaction layer (231), permeate water membrane (232), permeate water board (233) and delivery port (234), catalyst converter (23) bottom is equipped with delivery port (234), reaction layer (231), permeate water membrane (232) and permeate water board (233) set up inside catalyst converter (23), permeate water board (233) set up at the inside lower extreme of catalyst converter (23), permeate water board (233) surface top is equipped with permeate water membrane (232), reaction layer (231) set up on permeate water membrane (232) top, flow tube (24) are connected in reaction layer (231) upper end.
4. The sulfur melting equipment with purification effect for phosphorus pentasulfide production according to claim 1, wherein: the condenser (25) comprises a condensation pipe (251), a cover (252), a handle (253) and a water inlet (254), the condensation pipe (251) is wound on the outer surface of the condenser (25), the water inlet (254) is formed in one end of the condensation pipe (251), the other end of the condensation pipe (251) is connected with the top end of the connecting pipe (223), the cover (252) is arranged on the top of the other end of the condenser (25), and the handle (253) is connected with the top end of the cover (252).
5. The sulfur melting equipment with purification effect for phosphorus pentasulfide production according to claim 3, wherein: the reaction layer (231) is a member made of natural bauxite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021367005.5U CN212881874U (en) | 2020-07-13 | 2020-07-13 | Sulfur melting equipment with purifying effect for producing phosphorus pentasulfide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021367005.5U CN212881874U (en) | 2020-07-13 | 2020-07-13 | Sulfur melting equipment with purifying effect for producing phosphorus pentasulfide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212881874U true CN212881874U (en) | 2021-04-06 |
Family
ID=75285144
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021367005.5U Expired - Fee Related CN212881874U (en) | 2020-07-13 | 2020-07-13 | Sulfur melting equipment with purifying effect for producing phosphorus pentasulfide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212881874U (en) |
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2020
- 2020-07-13 CN CN202021367005.5U patent/CN212881874U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210406 |