CN212757541U - A crystallization filter equipment for chemical reagent preparation - Google Patents
A crystallization filter equipment for chemical reagent preparation Download PDFInfo
- Publication number
- CN212757541U CN212757541U CN202020024883.0U CN202020024883U CN212757541U CN 212757541 U CN212757541 U CN 212757541U CN 202020024883 U CN202020024883 U CN 202020024883U CN 212757541 U CN212757541 U CN 212757541U
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- Prior art keywords
- pipe
- reaction cylinder
- filter screen
- division board
- chemical reagent
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- 239000003153 chemical reaction reagent Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 238000002425 crystallisation Methods 0.000 title claims abstract description 16
- 230000008025 crystallization Effects 0.000 title claims abstract description 16
- 238000006243 chemical reaction Methods 0.000 claims abstract description 47
- 230000000694 effects Effects 0.000 claims abstract description 3
- 238000007789 sealing Methods 0.000 claims description 20
- 238000001914 filtration Methods 0.000 claims description 6
- 230000005611 electricity Effects 0.000 claims 1
- 239000013078 crystal Substances 0.000 abstract description 18
- 238000005192 partition Methods 0.000 description 9
- 239000002245 particle Substances 0.000 description 5
- 239000012295 chemical reaction liquid Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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Abstract
The utility model discloses a crystallization filter equipment for chemical reagent preparation, including the reaction cylinder, the horizontal fixedly connected with division board of inside intermediate position of reaction cylinder, the upside gomphosis activity of division board is provided with the infundibulate filter screen, the vertical upper end that is provided with pipe and pipe of division board downside intermediate position slides and passes the division board, simultaneously pipe upper end fixed connection the infundibulate filter screen, the vertical interlude of pipe top end intermediate position has closed post. The utility model discloses start electronic guide rail for electronic guide rail area pipe upwards slides and rises, then the pipe just takes the infundibulate filter screen upwards to rise to the inboard top of reaction cylinder, and final infundibulate filter screen rises to touching the position of shaking the cover along with the pipe, and the thimble is just in time contradicted the closed column upper end that the pipe upper end set up this moment, and will close the column top and impress the pipe inboard, and the pipe upper end is just opened, makes things convenient for the crystal in the infundibulate filter screen to slide into in the pipe.
Description
Technical Field
The utility model relates to a chemical reagent preparation crystal filter equipment technical field specifically is a crystallization filter equipment for chemical reagent preparation.
Background
The chemical reagent is a relative standard substance for chemical research and component analysis, is an important condition for scientific and technological progress, is widely used for synthesis, separation, qualitative and quantitative analysis of substances, and can generate crystal particles during reaction of some reagents, and the crystal particles need to be filtered and taken out;
the filtering device for preparing crystals by using general chemical reagents has the following defects: generally, when crystal particles in a reaction reagent need to be taken out, a filter screen is placed at the bottom in a reaction container in advance, so that some reaction liquid can be brought out when the crystal particles are taken out, and the reaction liquid is easy to drop to the external environment to cause pollution.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a crystallization filter equipment for chemical reagent preparation to solve the problem that proposes among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a crystallization filter equipment for chemical reagent preparation, includes the reaction cylinder, the horizontal fixedly connected with division board of inside intermediate position of reaction cylinder, the upside gomphosis activity of division board is provided with the infundibulate filter screen, the vertical upper end that is provided with pipe and pipe of division board downside intermediate position slides and passes the division board, simultaneously pipe upper end fixed connection the infundibulate filter screen, the vertical interlude of pipe upper end intermediate position has the outer wall of sealing post and pipe upper end inner wall laminates completely to the pipe lower extreme is the opening, pipe upper end inner wall encircles to bond has sealing rubber circle and sealing rubber circle tightly overlap on the sealing post outer wall, and sealing rubber circle adopts corrosion-resistant rubber material to make simultaneously, the inside lower side diameter of upper end mouth of pipe is less than pipe upper end mouth diameter, the inside lower side of upper end mouth of pipe passes through body of rod horizontal fixedly connected with go-between ring and the lower extreme slip of sealing post Cross the go-between, it has spring and spring both ends respectively fixed connection to seal post underpart cover the go-between with seal the post, division board position below the slide mechanism of the vertical fixedly connected with electric guide rail of reaction cylinder inner wall and electric guide rail is passing through body of rod fixed connection pipe lower extreme outer wall, the reaction cylinder top has set the cover, the lower terminal surface intermediate position of cover has the downside fixedly connected with shake cover of vibrator and vibrator through screw fixed mounting, the vertical fixedly connected with thimble of shake cover intermediate position downside, the position is located to the pipe division board downside is fixed to bond and is had sealed rubber sleeve and sealed rubber sleeve to tightly overlap the pipe upside.
Preferably, the upper end of the closed column is a convex spherical surface.
Preferably, the inner diameter of the rubber packing sleeve is gradually reduced from the upper side to the middle and then gradually increased from the middle downward.
Preferably, a storage box is placed at the bottom in the reaction cylinder and penetrates through the side wall of the reaction cylinder, and the storage box is located under the guide pipe.
Preferably, the bottom of the reaction cylinder is horizontally provided with a supporting plate, a motor is fixedly mounted above the supporting plate, and a main shaft of the motor is fixedly connected with the reaction cylinder.
Preferably, the left and right sides of backup pad is all vertically provided with support frame and support frame upper end fixed connection the reaction cylinder outer wall, simultaneously support frame lower extreme fixedly connected with pulley and pulley with the backup pad parallel and level.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the utility model discloses start electronic guide rail, make electronic guide rail take the pipe to slide upwards and rise, then the pipe just takes the infundibulate filter screen to rise upwards to reaction cylinder inboard top, and finally the infundibulate filter screen rises to the position of touching the shake cover along with the pipe, and the thimble is just in time conflicted the closed column upper end that the pipe upper end set up at this moment, and impress the closed column top into the pipe inboard, and the pipe upper end is just opened, makes things convenient for the crystal in the infundibulate filter screen to slide into in the pipe;
2. the utility model discloses the vibrator is taking the shake of infundibulate filter screen through the shake cover, promotes the crystal landing on the infundibulate filter screen in the pipe, from the pipe bottom discharge to the containing box in, starts the motor in the reaction cylinder bottom outside simultaneously for the reaction cylinder is rotatory, makes things convenient for the crystal granule on the infundibulate filter screen to slide into the pipe inboard, need not to take out the infundibulate filter screen and takes out reaction liquid and drip to the external environment and cause the pollution.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a crystallization filtering device for chemical reagent preparation according to the present invention;
FIG. 2 is an enlarged structural view of the closed column and the conduit of the crystallization filtering apparatus for chemical reagent preparation according to the present invention;
FIG. 3 is a top view of the reaction tube and the receiving box of the crystallization filtering device for chemical reagent preparation according to the present invention.
In the figure: 1. a reaction cylinder; 2. a partition plate; 3. a funnel-shaped filter screen; 4. sealing the rubber sleeve; 5. a conduit; 6. an electric rail; 7. a support frame; 8. a pulley; 9. a support plate; 10. a motor; 11. a storage box; 12. a thimble; 13. a shaking sleeve; 14. a vibrator; 15. a cylinder cover; 16. closing the column; 17. sealing the rubber ring; 18. a connecting ring; 19. a spring.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: a crystallization filtering device for chemical reagent preparation comprises a reaction cylinder 1, wherein a partition plate 2 is horizontally and fixedly connected to the middle position in the reaction cylinder 1, and the space of the reaction cylinder 1 above the partition plate 2 is a solution reaction zone; the upper side of the partition plate 2 is embedded and movably provided with a funnel-shaped filter screen 3, the middle position of the lower side of the partition plate 2 is vertically provided with a conduit 5, the upper end of the conduit 5 slides through the partition plate 2, the funnel-shaped filter screen 3 is fixedly connected with the upper end of the conduit 5, the middle position of the upper end head of the conduit 5 is vertically inserted with a closed column 16, the outer wall of the closed column 16 is completely attached to the inner wall of the upper end of the conduit 5, the lower end of the conduit 5 is an opening, the inner wall of the upper end of the conduit 5 is bonded with a sealing rubber ring 17 in a surrounding manner, the sealing rubber ring 17 is tightly sleeved on the outer wall of the closed column 16, the sealing rubber ring 17 is made of corrosion-resistant rubber material, the diameter of the inner lower side of the inner part of the upper end opening of the conduit 5 is smaller than the diameter of the upper end opening of the conduit 5, the inner lower side of the inner part of, an electric guide rail 6 is vertically and fixedly connected to the inner wall of the reaction cylinder 1 below the position of the partition plate 2, a sliding mechanism of the electric guide rail 6 is fixedly connected to the outer wall of the lower end of the guide pipe 5 through a rod body, meanwhile, the electric guide rail 6 is provided with a control switch, when crystals generated in a reaction area above the reaction cylinder 1 need to be separated from a solution, the electric guide rail 6 is started, the electric guide rail 6 drives the guide pipe 5 to upwards slide and rise, then the guide pipe 5 drives the funnel-shaped filter screen 3 to upwards rise to the top of the inner side of the reaction cylinder 1, and the crystals are filtered by the funnel-shaped filter screen; the top of the reaction cylinder 1 is provided with a cylinder cover 15, the middle position of the lower end surface of the cylinder cover 15 is fixedly provided with a vibrator 14 through a screw, the lower side of the vibrator 14 is fixedly connected with a shaking sleeve 13, the lower side of the middle position of the shaking sleeve 13 is vertically and fixedly connected with a thimble 12, when the funnel-shaped filter screen 3 rises to the position touching the shaking sleeve 13 along with the guide pipe 5, the thimble 12 just props against the upper end of the closed column 16 and pushes the closed column 16 into the inner side of the guide pipe 5, so that crystals in the funnel-shaped filter screen 3 slide into the inner side of the guide pipe 5 and are discharged from the lower end of the guide pipe 5, and the vibrator 14 drives the funnel-shaped filter screen 3 to shake through the shaking sleeve 13, thereby; the lower side of the partition plate 2 at the position of the guide pipe 5 is fixedly bonded with a sealing rubber sleeve 4, the sealing rubber sleeve 4 is tightly sleeved on the upper side of the guide pipe 5, the sealing rubber sleeve 4 is made of corrosion-resistant rubber materials, and the sealing rubber sleeve 4 is used for sealing the connection position of the guide pipe 5 and the partition plate 2.
The upper end of the closed column 16 is a convex spherical surface, so that when the closed column 16 is accommodated in the guide pipe 5, the crystal falling on the inner side of the guide pipe 5 slides away after contacting the upper end of the closed column 16.
The internal diameter of the sealing rubber sleeve 4 gradually decreases from the upper side to the middle, and then gradually increases from the middle downwards, so that when the conduit 5 slides in the sealing rubber sleeve 4, the middle position is ensured to be tightly attached to the side wall of the conduit 5 to keep sealing.
The bottom has been put in reaction cylinder 1 receiver 11 and receiver 11 passes reaction cylinder 1 lateral wall, and receiver 11 is in under pipe 5 simultaneously, and receiver 11 is used for catching the crystal that falls from pipe 5 internal slipping.
The bottom level of reaction cylinder 1 is provided with backup pad 9, and backup pad 9 top fixed mounting has motor 10 and motor 10's main shaft fixed connection reaction cylinder 1, and after funnel-shaped filter screen 3 docked on shaking cover 13, starting motor 10 for reaction cylinder 1 is rotatory, makes things convenient for crystal particle landing on funnel-shaped filter screen 3 to enter pipe 5 inboard.
The equal vertical support frame 7 and the support frame 7 upper end fixed connection of the left and right sides of backup pad 9 the outer wall of reaction cylinder 1, and 7 lower extreme fixedly connected with pulleys 8 and the 9 parallel and level of backup pad simultaneously, when backup pad 9 supports on the desktop, pulleys 8 just in time also support on the desktop, make things convenient for support frame 7 to support reaction cylinder 1, and pulley 8 rolls along the desktop when making things convenient for reaction cylinder 1 to rotate simultaneously.
The working principle is as follows: the utility model starts the electric guide rail 6, so that the electric guide rail 6 drives the guide pipe 5 to slide upwards and rise, the guide pipe 5 drives the funnel-shaped filter screen 3 to rise upwards to the top of the inner side of the reaction cylinder 1, finally the funnel-shaped filter screen 3 rises along with the guide pipe 5 to touch the position of the shaking sleeve 13, at the moment, the thimble 12 just props against the upper end of the closed column 16 arranged at the upper end of the guide pipe 5, and the closed column 16 is jacked into the inner side of the guide pipe 5, the upper end of the guide pipe 5 is opened, so that the crystals in the funnel-shaped filter screen 3 can slide into the guide pipe 5 conveniently, and the vibrator 14 drives the funnel-shaped filter screen 3 to shake through the shaking sleeve 13, so as to promote the crystals on the funnel-shaped filter screen 3 to slide into the guide pipe 5 and be discharged into the storage box 11 from the bottom of the guide pipe 5, and simultaneously starts the motor, the funnel-shaped filter screen 3 is not required to be taken out, and the reaction liquid is brought out and dropped to the external environment to cause pollution.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A crystallization filtering device for chemical reagent preparation, comprising a reaction cylinder (1), characterized in that: horizontal fixedly connected with division board (2) of inside intermediate position of reaction cylinder (1), the upside gomphosis activity of division board (2) is provided with infundibulate filter screen (3), the vertical upper end that is provided with pipe (5) and pipe (5) of division board (2) downside intermediate position slides and passes division board (2), simultaneously pipe (5) upper end fixed connection infundibulate filter screen (3), the vertical interlude of pipe (5) upper end intermediate position has closed post (16), pipe (5) upper end inner wall encircles and is provided with sealed rubber circle (17), the horizontal fixedly connected with go-between (18) of the upper end mouth inside lower side of pipe (5) and closed post (16) lower extreme slide and pass go-between (18), closed post (16) lower pot head has spring (19), division board (2) position below the vertical fixedly connected with electric guide rail (6) of reaction cylinder (1) inner wall and electricity Move guide rail (6) fixed connection pipe (5), reaction cylinder (1) top has set cover (15), the lower terminal surface intermediate position fixed mounting of cover (15) has downside fixedly connected with shake cover (13) of vibrator (14) and vibrator (14), shake the vertical fixedly connected with thimble (12) of cover (13) intermediate position downside, pipe (5) position division board (2) downside is fixed and is provided with sealed rubber sleeve (4) and sealed rubber sleeve (4) cover pipe (5) upside.
2. A crystallization filter apparatus for chemical reagent preparation according to claim 1, wherein: the upper end of the closed column (16) is a convex spherical surface.
3. A crystallization filter apparatus for chemical reagent preparation according to claim 1, wherein: the inner diameter of the sealing rubber sleeve (4) is gradually reduced from the upper side to the middle and then gradually increased from the middle downwards.
4. A crystallization filter apparatus for chemical reagent preparation according to claim 1, wherein: a storage box (11) is placed at the bottom in the reaction cylinder (1) and the storage box (11) penetrates through the side wall of the reaction cylinder (1).
5. A crystallization filter apparatus for chemical reagent preparation according to claim 1, wherein: the bottom of reaction cylinder (1) level is provided with backup pad (9), backup pad (9) top fixed mounting has motor (10) and the main shaft end fixed connection of motor (10) is in reaction cylinder (1).
6. A crystallization filter device for chemical reagent preparation according to claim 5, characterized in that: the equal vertical support frame (7) and being provided with in the left and right sides of backup pad (9) and support frame (7) upper end fixed connection is then reaction cylinder (1) outer wall, simultaneously support frame (7) lower extreme fixedly connected with pulley (8) and pulley (8) with backup pad (9) parallel and level.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020024883.0U CN212757541U (en) | 2020-01-02 | 2020-01-02 | A crystallization filter equipment for chemical reagent preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020024883.0U CN212757541U (en) | 2020-01-02 | 2020-01-02 | A crystallization filter equipment for chemical reagent preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212757541U true CN212757541U (en) | 2021-03-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202020024883.0U Expired - Fee Related CN212757541U (en) | 2020-01-02 | 2020-01-02 | A crystallization filter equipment for chemical reagent preparation |
Country Status (1)
| Country | Link |
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| CN (1) | CN212757541U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113209695A (en) * | 2021-04-19 | 2021-08-06 | 浙江中金格派锂电产业股份有限公司 | Precise filtering device for cobalt sulfate production |
-
2020
- 2020-01-02 CN CN202020024883.0U patent/CN212757541U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113209695A (en) * | 2021-04-19 | 2021-08-06 | 浙江中金格派锂电产业股份有限公司 | Precise filtering device for cobalt sulfate production |
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|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210323 |
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| CF01 | Termination of patent right due to non-payment of annual fee |