CN212524089U - Recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate - Google Patents

Recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate Download PDF

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Publication number
CN212524089U
CN212524089U CN202020893663.1U CN202020893663U CN212524089U CN 212524089 U CN212524089 U CN 212524089U CN 202020893663 U CN202020893663 U CN 202020893663U CN 212524089 U CN212524089 U CN 212524089U
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reaction kettle
kettle body
motor
rotating shaft
stirring rod
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CN202020893663.1U
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刘玉起
陈俊霞
刘景起
刘玲艳
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Jiaozuo Runyang Chemical Technology Co ltd
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Jiaozuo Runyang Chemical Technology Co ltd
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Abstract

The utility model discloses a recycling reaction kettle for producing 1-naphthylamine-4-sodium sulfonate, which comprises a reaction kettle body and a mounting rack; the reaction kettle body is fixedly arranged on the mounting frame, a motor is arranged at the middle position of the upper end surface of the reaction kettle body, the output end of the lower part of the motor is connected with a rotating shaft, the rotating shaft penetrates through the reaction kettle body and extends into the reaction kettle body, a frame type stirring rod is fixedly arranged on the outer side wall of the rotating shaft, an anchor type stirring rod is arranged at the bottom of the rotating shaft, a feeding hole is formed in the upper end surface of the reaction kettle body, and a discharging hole is arranged at the middle position of the lower; after the materials are put into the feeding hole, a power supply of a motor is switched on, so that a rotating shaft below the motor rotates along with the motor, a frame type stirring rod and an anchor type stirring rod on the rotating shaft are driven to rotate, the materials are fully and uniformly stirred, and the materials are discharged from a discharging hole; and the power supply of the water pump is switched on, the water in the water tank is conveyed to the interior of the distribution pipe by the water pump through the connecting pipeline, and then the water is sprayed out from the spray head.

Description

Recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate
Technical Field
The utility model belongs to the technical field of reation kettle, concretely relates to cyclic utilization's reation kettle of production 1-naphthylamine-4-sodium sulfonate.
Background
1-naphthylamine-4-sodium sulfonate (common name: 4-amino-1-sodium naphthalenesulfonate, sodium 1, 4 for short) is an important azo pigment intermediate, is widely used for synthesizing direct dyes and reactive dyes, and simultaneously, sodium 1, 4 is also one of nitrite and iodine poisoning antidotes; in recent years, the amino group and the sulfonic group of the sodium 1, 4 can be well coordinated with a power supply atom, so that the sodium 1, 4 can be used as a donor of a hydrogen bond and an acceptor of the hydrogen bond, and the sodium 1, 4 can be widely applied to complexing with various metals (such as Fe, Zn, Cd, Ni and the like) and used for synthesis of toxic chemical leakage monitoring equipment, optical devices and gas absorption materials and clinical medical research; the 1, 4-sodium sulfonate can also be used in the fields of thermal switches, optical switches, information storage element materials, DNA structure probes, DNA molecular optical switches and the like, and is provided in the form of 1-naphthylamine-4-sodium sulfonate tetrahydrate in a laboratory.
However, the existing reaction kettle for producing the 1-naphthylamine-4-sodium sulfonate is not uniform enough in stirring, and the internal cleaning mode is too complicated.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects in the prior art, the utility model provides a recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate, which is characterized in that an upper end cover is opened, after materials are put into the reaction kettle from a feed inlet, at the moment, the power supply of a motor is switched on, a rotating shaft below the reaction kettle rotates along with the materials, a frame type stirring rod and an anchor type stirring rod on the rotating shaft are driven to rotate, the materials are fully and uniformly stirred, and then a lower end cover is opened, so that the materials are discharged from a discharge outlet; after the water tank is used, the upper end cover and the lower end cover are closed, a power supply of the water pump is connected, the water in the water tank is conveyed to the interior of the distribution pipe by the water pump through the connecting pipeline and then sprayed out of the spray head, the frame type stirring rod, the anchor type stirring rod and the interior of the reaction kettle body are cleaned by the sprayed water, and finally the lower end cover is opened, so that the cleaned water flows out of the discharge hole.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
a recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate comprises a reaction kettle body and a mounting rack; the reaction kettle comprises a reaction kettle body, a mounting frame, a motor, a frame type stirring rod, an anchor type stirring rod, a feed inlet, a discharge outlet and a sealing ring, wherein the reaction kettle body is fixedly mounted on the mounting frame, the motor is mounted at the middle position of the upper end surface of the reaction kettle body, the output end of the lower part of the motor is connected with a rotating shaft, the rotating shaft penetrates through the reaction kettle body and extends into the reaction kettle body, the outer side wall of the rotating shaft is fixedly provided with the frame type stirring rod, the bottom of the rotating shaft is provided with the anchor type stirring rod, the upper end; install the water tank on the mount, the water tank is located the reation kettle body outside, install the water pump in the water tank, install the distributing pipe on the reation kettle body inside wall, the distributing pipe is close to frame puddler one side equipartition and installs the shower nozzle, communicate each other between shower nozzle and the distributing pipe, the water pump in the water tank communicates each other near reation kettle body internal surface one side with the distributing pipe through connecting tube.
Further, a motor bin is installed on the outer side of the motor, and the motor is fixedly installed on the upper end face of the reaction kettle body through the motor bin.
Further, the feed inlet is hinged with an upper end cover through a first hinge, and the discharge outlet is hinged with a lower end cover through a second hinge.
Further, the connecting pipeline is of a hose structure.
Further, the diapire of reation kettle body is for leaking hopper-shaped, a plurality of spiral stirring oars are installed to the diapire both sides of reation kettle body, the spiral stirring oar is located the discharge gate outside.
Adopt above-mentioned technical scheme, the beneficial effects of the utility model are that:
a recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate is characterized in that an upper end cover is opened, materials are put into the reaction kettle from a feeding hole, then a power supply of a motor is switched on, a rotating shaft below the motor rotates along with the motor, a frame type stirring rod and an anchor type stirring rod on the rotating shaft are driven to rotate, the materials are fully and uniformly stirred, and then a lower end cover is opened, so that the materials are discharged from a discharging hole; after the water tank is used, the upper end cover and the lower end cover are closed, a power supply of the water pump is connected, the water in the water tank is conveyed to the interior of the distribution pipe by the water pump through the connecting pipeline and then sprayed out of the spray head, the frame type stirring rod, the anchor type stirring rod and the interior of the reaction kettle body are cleaned by the sprayed water, and finally the lower end cover is opened, so that the cleaned water flows out of the discharge hole.
Drawings
FIG. 1 is a schematic structural diagram of a reaction kettle for producing 1-naphthylamine-4-sodium sulfonate, which is recycled in the utility model.
Detailed Description
For making the utility model discloses the technological means, creation characteristic, achievement purpose and efficiency that realize are easily understood and are known, combine specific implementation below, further explain the utility model discloses:
therefore, the following detailed description of the embodiments of the present invention, which is provided in the accompanying drawings, is not intended to limit the scope of the invention, as claimed, but is merely representative of selected embodiments of the invention, and all other embodiments that can be obtained by one of ordinary skill in the art without any inventive effort based on the embodiments of the present invention are within the scope of the invention.
It should be noted that: like reference numbers and letters refer to like items in the following figures, and thus, once an item is defined in one figure, it need not be further defined and explained in subsequent figures.
The terms "first," "second," "third," and the like are used solely to distinguish one from another and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it should also be noted that, unless otherwise explicitly specified or limited, the terms "disposed," "mounted," "connected," and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; the two elements may be directly connected or indirectly connected through an intermediate medium, and the two elements may be connected through an intermediate medium.
In conjunction with FIG. 1: a recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate comprises a reaction kettle body 1 and a mounting rack 2; the reaction kettle comprises a reaction kettle body 1, a motor 3, a rotating shaft 4, a frame type stirring rod 5, an anchor type stirring rod 6, a feed inlet 7 and a discharge outlet 8, wherein the reaction kettle body 1 is fixedly arranged on a mounting frame 2, the motor 3 is arranged at the middle position of the upper end face of the reaction kettle body 1, the output end of the lower part of the motor 3 is connected with the rotating shaft 4, the rotating shaft 4 penetrates through the reaction kettle body 1 and extends into the reaction kettle body 1, the outer side wall of the rotating shaft 4 is fixedly provided with the frame type stirring rod 5, the bottom of the rotating shaft 4 is provided with the anchor type stirring rod 6, the upper end face of the reaction kettle; install water tank 9 on mount 2, water tank 9 is located the 1 outside of reation kettle body, install water pump 10 in the water tank 9, install distributing pipe 11 on 1 inside wall of reation kettle body, distributing pipe 11 is close to 5 one side equipartitions of frame puddler and installs shower nozzle 12, communicate each other between shower nozzle 12 and the distributing pipe 11, water pump 10 in the water tank 9 communicates each other near 1 internal surface one side of reation kettle body through connecting tube 13 and distributing pipe 11.
Further, a motor bin 20 is installed on the outer side of the motor 3, and the motor 3 is fixedly installed on the upper end face of the reaction kettle body 1 through the motor bin 20; the motor is protected, and the model number of the motor is Y160M 1-2.
Further, the feed inlet 7 is hinged with an upper end cover 22 through a first hinge 21, and the discharge outlet 8 is hinged with a lower end cover 24 through a second hinge 23.
Further, the connecting pipe 13 is of a hose structure.
Further, the diapire of reation kettle body 1 is for leaking hopper-shaped, a plurality of spiral stirring rake 31 are installed to the diapire both sides of reation kettle body 1, spiral stirring rake 31 is located the 8 outsides of discharge gate.
Wherein the model of the water pump is WNY 180.
Opening the upper end cover, putting the materials into the feeding hole, switching on a power supply of a motor at the moment, enabling a rotating shaft below the upper end cover to rotate along with the upper end cover, driving a frame type stirring rod and an anchor type stirring rod on the rotating shaft to rotate, fully and uniformly stirring the materials, and then opening the lower end cover to discharge the materials from a discharging hole; after the water tank is used, the upper end cover and the lower end cover are closed, a power supply of the water pump is connected, the water in the water tank is conveyed to the interior of the distribution pipe by the water pump through the connecting pipeline and then sprayed out of the spray head, the frame type stirring rod, the anchor type stirring rod and the interior of the reaction kettle body are cleaned by the sprayed water, and finally the lower end cover is opened, so that the cleaned water flows out of the discharge hole.
The present embodiment is not intended to limit the shape, material, structure, etc. of the present invention in any form, and all of the technical matters of the present invention belong to the protection scope of the present invention to any simple modification, equivalent change and modification made by the above embodiments.

Claims (5)

1. A recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate is characterized in that: comprises a reaction kettle body and a mounting rack; the reaction kettle comprises a reaction kettle body, a mounting frame, a motor, a frame type stirring rod, an anchor type stirring rod, a feed inlet, a discharge outlet and a sealing ring, wherein the reaction kettle body is fixedly mounted on the mounting frame, the motor is mounted at the middle position of the upper end surface of the reaction kettle body, the output end of the lower part of the motor is connected with a rotating shaft, the rotating shaft penetrates through the reaction kettle body and extends into the reaction kettle body, the outer side wall of the rotating shaft is fixedly provided with the frame type stirring rod, the bottom of the rotating shaft is provided with the anchor type stirring rod, the upper end; install the water tank on the mount, the water tank is located the reation kettle body outside, install the water pump in the water tank, install the distributing pipe on the reation kettle body inside wall, the distributing pipe is close to frame puddler one side equipartition and installs the shower nozzle, communicate each other between shower nozzle and the distributing pipe, the water pump in the water tank communicates each other near reation kettle body internal surface one side with the distributing pipe through connecting tube.
2. The recycling reaction kettle for producing the sodium 1-naphthylamine-4-sulfonate as claimed in claim 1, wherein: the motor storehouse is installed in the outside of motor, the motor passes through motor storehouse fixed mounting at reation kettle body up end.
3. The recycling reaction kettle for producing the sodium 1-naphthylamine-4-sulfonate as claimed in claim 1, wherein: the feed inlet is hinged with an upper end cover through a first hinge, and the discharge outlet is hinged with a lower end cover through a second hinge.
4. The recycling reaction kettle for producing the sodium 1-naphthylamine-4-sulfonate as claimed in claim 1, wherein: the connecting pipeline is of a hose structure.
5. The recycling reaction kettle for producing the sodium 1-naphthylamine-4-sulfonate as claimed in claim 1, wherein: the diapire of reation kettle body is for leaking hopper-shaped, a plurality of spiral stirring rake are installed to the diapire both sides of reation kettle body, the spiral stirring rake is located the discharge gate outside.
CN202020893663.1U 2020-05-25 2020-05-25 Recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate Active CN212524089U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020893663.1U CN212524089U (en) 2020-05-25 2020-05-25 Recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020893663.1U CN212524089U (en) 2020-05-25 2020-05-25 Recycled reaction kettle for producing 1-naphthylamine-4-sodium sulfonate

Publications (1)

Publication Number Publication Date
CN212524089U true CN212524089U (en) 2021-02-12

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CN (1) CN212524089U (en)

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