CN2124471U - Swelling capacity tester - Google Patents

Swelling capacity tester Download PDF

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Publication number
CN2124471U
CN2124471U CN 91232995 CN91232995U CN2124471U CN 2124471 U CN2124471 U CN 2124471U CN 91232995 CN91232995 CN 91232995 CN 91232995 U CN91232995 U CN 91232995U CN 2124471 U CN2124471 U CN 2124471U
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CN
China
Prior art keywords
swelling behavior
behavior analyzer
sample
swelling
dial gauge
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 91232995
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Chinese (zh)
Inventor
左榘
乔凤军
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Nankai University
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Nankai University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nankai University filed Critical Nankai University
Priority to CN 91232995 priority Critical patent/CN2124471U/en
Publication of CN2124471U publication Critical patent/CN2124471U/en
Granted legal-status Critical Current

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Abstract

The utility model belongs to a device which adopts mechanical stress to test the strength performance of solid materials. The utility model mainly comprises a tensile and press stress sensor, a dial test indicator, a compressed sample slot matched with a constant temperature jacket, a worktable, a magnetic base, etc. The device can be used for accurately measuring the equilibrium swelling modulus of a polymer material sample, and can constantly track and record the swelling kinetic process and the stress relaxation process of the polymer material sample. The utility model has the advantages of wide test range and favorable accuracy and data repeatability.

Description

Swelling capacity tester
The utility model belongs to the device with mechanical stress test solid material strength characteristics.
The test of macromolecular material swelling behavior is to adopt to be interrupted the swelling sample of weighing at first, or in a graduated tube, read the method that cumulative volume increases, this class methods complex operation, error are big, more can not note the adding solvent swelling behavior of moment at any time, can not be used for detecting the size of macromolecular material swelling stress.Document [ 1 ] has been introduced a kind of working sample that is used at the device of solvent swelling state with the birefringent variation of the generation that stretches, and is one of assembly in the photoelastic experiment device.K.L.Wun adds in said apparatus with altimeter test sample product change in size and surveys solvent swelling state sample balance modulus in compression (2), but this also is one of assembly in a whole set of experimental provision.Shanghai nonmetal testing machine factory produces a kind of SC-40 type compression stress relaxation instrument that is used to measure rubbery sample compression deformation STRESS VARIATION.Above-mentioned existing device all can only be used for measuring a kind of data of single performance, can not temperature control, thereby can not study performance to dependence on temperature.SC-40 type compression stress relaxation instrument is not to measure under the condition of the constant deformation of strict guarantee, and design concept is improper.In addition, do not see as yet about carrying out the swelling dynamics of macromolecular material and the report of swelling sample stress relaxation behavior measure with similar device yet.
The purpose of this utility model provide a kind of multi-functional, can control temperature, and can be later on continuous digital data recording system in succession, be used for testing the device of various macromolecular material swelling behaviors separately.
The purpose of this utility model is achieved in that this swelling behavior analyzer mainly wraps and knows tension and compression strain gauge (measurement range is at 1~2 kilogram), dial gauge, constrictor and constrictor head, the compression sample groove of being furnished with constant temperature jacket, magnet base, worktable, adjusting fine thread leading screw and 8 parts of pilot lamp.Its principle of operation is as follows: the portion that sample is placed spill sample cell [ 16 ], and the power supply of connection sensor [ 11 ], rotating adjusting fine thread screw mandrel [ 1 ] moves down sensor [ 11 ], the constrictor [ 7 ] and the constrictor head [ 8 ] that are connected on the dial gauge bottom simultaneously press down, pilot lamp [ 15 ] circuit when sample in the groove contacts is connected and is lighted when [ 8 ], when continuing to press down again, the force of compression of sample is exported to the independently register system that is connected with this analyzer by [ 11 ], write down stress value, meanwhile on dial gauge [ 6 ], read strain value synchronously.When pilot lamp [ 15 ] is bright, inject sweller, constantly the variation of track record swelling stress also can keep a constant strain value, notes stress relaxation in time.
[ 16 ] be made of transparent material, be convenient to observe, spill is particularly conducive to the placement and the compression of sample, have above band for liquid or gas pass in and out the lid of two apertures of usefulness respectively.[ 16 ] dispose a constant temperature jacket [ 17 ] outside, with the recirculated water temperature control.Worktable [ 10 ] is (the passing through screw rod) of adjustment height, after sample test finishes, can reduce height of table fast, takes off sample cell.Control the very fine tuning and steady of lifting of [ 11 ] with regulating fine thread leading screw [ 1 ].[ 6 ] be connected with magnet base [ 19 ] with magnetic force dial gauge support [ 18 ] by dial gauge sliding bar shell [ 5 ], can guarantee that [ 6 ] are motionless in test process.
The advantage that the utility model compared with prior art has is that function is many: but both equilibrium swelling modulus of working sample, and the swelling dynamic process of track record dry sample at any time again can also constantly be followed the tracks of and do or the stress relaxation process of swelling sample; Applied range: sample can be a dry sample, also can be the swelling sample, allows the rigidity of sample to change within a bigger scope, and test performance is good: sensitivity and degree of accuracy height, accuracy and data good reproducibility (for details see attached table 1 and accompanying drawing 5)
Subordinate list 1 tune-up data table
(A face standard working curve determination data table)
F Outward(g): 0-50.0-100.0-205.0-255.0-305.0-355.0
V(mv):-1.08 -1.51 -1.91 -2.80 -3.22 -3.63 -4.05
Return: F Outward=119.6V (mv)+129.5 (g) r=0.999986
F Outward(g): 0-50.0-100.0-205.0-255.0-305.0-355.0
V(mv):-1.12 -1.51 -1.91 -2.82 -3.23 -3.63 -4.05
Return: F Outward=120.4V (mv)+132.8 (g) r=0.999917
F Outward(g): 0-50.0-100.0-205.0-255.0-305.0
V(mv):-1.10 -1.51 -1.93 -2.80 -3.23 -3.65
Return: F Outward=119.6V (mv)+130.9 (g) r=0.999985
Standard working curve: F Outward=120.0V (mv)+131.0 (g)
F in the table OutwardBe the known external force that applies, V is an output signal, and r is a linear regression coeffficient.The downward power of hypothesis is negative in the test, and this moment, output signal also was negative, and vice versa.External force is to obtain by go up the counterweight that hangs Different Weight at sensor semi-girder [ 12 ].
The drawing of accompanying drawing is described as follows:
Accompanying drawing 1. overall apparatus front views
Accompanying drawing 2. overall apparatus side views
Accompanying drawing 3. overall apparatus vertical views
Swelling kinetic curve under accompanying drawing 4. different temperatures
Accompanying drawing 5. stress relaxation curves
Component part numbers is as follows:
[ 1 ] regulates fine thread leading screw, [ 2 ] rail plate built-in beam [ 3 ] rail plate [ 4 ] sliding beam [ 5 ] dial gauge sliding bar shell [ 6 ] dial gauge [ 7 ] constrictor [ 8 ] constrictor head [ 9 ] sample [ 10 ] workbench [ 11 ] tension and compression strain gauge [ 12 ] sensor cantilever beam [ 13 ] probe power and output interface [ 14 ] power transmission connecting rod [ 15 ] indicator lamp [ 16 ] compression sample groove [ 17 ] constant temperature jacket [ 18 ] magnetic force dial indicator bracket [ 19 ] magnet base [ 20 ] support base plate

Claims (7)

1, a kind of swelling behavior analyzer, it is characterized in that this device comprise tension and compression strain gauge [11], dial gauge [6], constrictor [7] and constrictor head [8], be furnished with constant temperature jacket [17] compression sample groove [16], magnet base [19], worktable [10], regulate fine thread leading screw [1] and pilot lamp [15], [7] and [8] directly are connected the bottom of [6].
2,, it is characterized in that the measurement range of tension and compression strain gauge [ 11 ] is chosen in the 1-2 kilogram according to the said swelling behavior analyzer of claim 1.
3, according to the said swelling behavior analyzer of claim 1, it is characterized in that compression sample groove [ 16 ] made by transparent material, the top have band for liquid or gas pass in and out the lid of two apertures of usefulness respectively.
4, according to the said swelling behavior analyzer of claim 1, it is characterized in that connecting when the circuit of constrictor head [ 8 ] pilot lamp [ 15 ] when contacting with sample, pilot lamp is lighted.
5,, it is characterized in that dial gauge [ 6 ] is connected with magnet base [ 19 ] with magnetic force dial gauge support [ 18 ] by dial gauge sliding bar shell [ 5 ] according to the said swelling behavior analyzer of claim 1.
6,, it is characterized in that constant temperature jacket [ 17 ] is to use the recirculated water temperature control according to the said swelling behavior analyzer of claim 1.
7,, it is characterized in that the height of worktable [ 10 ] can be regulated by screw rod according to the said swelling behavior analyzer of claim 1.
CN 91232995 1991-12-27 1991-12-27 Swelling capacity tester Granted CN2124471U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 91232995 CN2124471U (en) 1991-12-27 1991-12-27 Swelling capacity tester

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 91232995 CN2124471U (en) 1991-12-27 1991-12-27 Swelling capacity tester

Publications (1)

Publication Number Publication Date
CN2124471U true CN2124471U (en) 1992-12-09

Family

ID=4937926

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 91232995 Granted CN2124471U (en) 1991-12-27 1991-12-27 Swelling capacity tester

Country Status (1)

Country Link
CN (1) CN2124471U (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102346123A (en) * 2011-07-18 2012-02-08 上海化工研究院 Method for analyzing swelling performance of ultrahigh-molecular-weight polyethylene resin
CN101363834B (en) * 2007-08-07 2013-07-10 宝理塑料株式会社 Prediction method of equilibrium swelling quantity for two-componnet mixed physic liquor of resin
CN105928643A (en) * 2016-04-26 2016-09-07 西南科技大学 Bentonite two-way swelling force measuring instrument
CN107860677A (en) * 2017-10-23 2018-03-30 合肥国轩高科动力能源有限公司 A kind of test device and method of testing for being used to detect lithium electric material swellbility
CN108169417A (en) * 2017-12-13 2018-06-15 中国工程物理研究院化工材料研究所 A kind of swellbility Intelligent Dynamic test device and test method
CN110080746A (en) * 2019-05-24 2019-08-02 北京爱地地质勘察基础工程公司 A kind of compression test equipment and its application method in situ of drilling

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101363834B (en) * 2007-08-07 2013-07-10 宝理塑料株式会社 Prediction method of equilibrium swelling quantity for two-componnet mixed physic liquor of resin
CN102346123A (en) * 2011-07-18 2012-02-08 上海化工研究院 Method for analyzing swelling performance of ultrahigh-molecular-weight polyethylene resin
CN102346123B (en) * 2011-07-18 2013-04-24 上海化工研究院 Method for analyzing swelling performance of ultrahigh-molecular-weight polyethylene resin
CN105928643A (en) * 2016-04-26 2016-09-07 西南科技大学 Bentonite two-way swelling force measuring instrument
CN105928643B (en) * 2016-04-26 2018-06-29 西南科技大学 The two-way expansion force measuring instrument of bentonite
CN107860677A (en) * 2017-10-23 2018-03-30 合肥国轩高科动力能源有限公司 A kind of test device and method of testing for being used to detect lithium electric material swellbility
CN108169417A (en) * 2017-12-13 2018-06-15 中国工程物理研究院化工材料研究所 A kind of swellbility Intelligent Dynamic test device and test method
CN108169417B (en) * 2017-12-13 2020-05-22 中国工程物理研究院化工材料研究所 Intelligent dynamic swelling degree testing device and testing method
CN110080746A (en) * 2019-05-24 2019-08-02 北京爱地地质勘察基础工程公司 A kind of compression test equipment and its application method in situ of drilling

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