CN108169417A - A kind of swellbility Intelligent Dynamic test device and test method - Google Patents
A kind of swellbility Intelligent Dynamic test device and test method Download PDFInfo
- Publication number
- CN108169417A CN108169417A CN201711328264.XA CN201711328264A CN108169417A CN 108169417 A CN108169417 A CN 108169417A CN 201711328264 A CN201711328264 A CN 201711328264A CN 108169417 A CN108169417 A CN 108169417A
- Authority
- CN
- China
- Prior art keywords
- swellbility
- cup
- sample
- specimen cup
- intelligent dynamic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
Abstract
The invention discloses a kind of swellbility Intelligent Dynamic test devices, including vertically disposed sliding bar, the horizontal lifting pallet being connected with sliding bar by fixed knob, solution cup is provided on lifting tray, specimen cup is provided with above solution cup, specimen cup bottom is provided with liquid and penetrates into hole, displacement sensor is installed above specimen cup, displacement sensor lower part is connected with sensor test disk, specimen cup fixator is provided between displacement sensor and sensor test disk, displacement sensor is electrically connected with digital display instrument, it statistics have shown screen and control button on digital display instrument, displacement sensor also communicates with computer.The present invention also provides swellbility Intelligent Dynamic test methods.Present invention operation is simple and realizes big data quantity follow-on test, reduces cost of labor；The strong applicability of sample to be tested.
Description
Technical field
The present invention relates to the test devices and method of a kind of swellbility, and in particular to one kind is for macromolecule swellbility intelligence
Dynamic checkout unit and test method belong to high molecular chemical characters characterization technique field.
Background technology
Cross-linked polymer has swelling character, and swelling equilibrium is substantially the thermodynamical equilibrium of cross-linked network and solvent, this
Kind dynamic equilibrium can change with extraneous factors such as solvent environment, temperature.Crosslinked polymeric swellbility is measured, for research
Interaction and high molecular swellability between polymer crosslinking structure, macromolecule and solvent, which are influenced by temperature etc., all to be had
It is significant.
The swellbility test method of document report mainly has weight method and two kinds of volumetric method of amount at present, mostly using laboratory
Easily-testing lacks general standard method of test and instrument.Weight method be by the polymer of known quality within a certain period of time
It is soaked in solvent, rapid filtration under suction removes excess of solvent after it reaches swelling equilibrium, and polymerization is assessed by calculating gain in weight
The swellbility of object.This kind of procedure is complicated, and accurate testing degree is not high, it is impossible to which how solution isolates swelling body from solvent
The problem of without influencing its swelling equilibrium state, and the continuous dynamic change of swellbility at any time cannot be recorded in real time.Measure volume
Method is usually to select the graduated glass column of a fixed-caliber, and volume information is changed into elevation information, is a kind of more simple and conjunction
The test method of reason, but can not equally realize that the continuous dynamic of swellbility is tested in a manner that scale value is read in range estimation at present,
Accuracy and intelligent level be not high.Therefore, designing a kind of novel swellbility test method and device has important practicality
Value.
Invention content
The present invention overcomes the deficiencies of traditional swellbility measuring technology, provide a kind of for macromolecule swellbility Intelligent Dynamic
Test device and test method, to fill up the blank of current swellbility Intelligent Dynamic test method and instrument.
One of the objects of the present invention is to provide a kind of swellbility Intelligent Dynamic test device, including：
Vertically disposed sliding bar, the horizontal lifting pallet being connected with sliding bar by fixed knob are set on lifting tray
Solution cup is equipped with, specimen cup is provided with above solution cup, specimen cup bottom is provided with liquid and penetrates into hole, is equipped with above specimen cup
Displacement sensor, displacement sensor lower part are connected with sensor test disk, are set between displacement sensor and sensor test disk
Specimen cup fixator is equipped with, displacement sensor is electrically connected with digital display instrument, statistics have shown screen and control button on digital display instrument, displacement
Sensor also communicates with computer.
Further scheme is：In order to control temperature when swellbility is tested, temperature control is respectively arranged on solution cup
Water inlet and temperature-control water outlet mouth, temperature control water inlet are located at below temperature-control water outlet mouth.
Further scheme is：In order to keep temperature, temperature control chuck is additionally provided on the outside of solution cup.
Further scheme is：The specimen cup is smaller than solution cup size, can be put into solution cup.
Further scheme is：The sensor test disk size is identical with specimen cup inside cross-sectional size.
Further scheme is：The swellbility Intelligent Dynamic test device includes identical positioned at sliding bar both sides
Two covering devices.
The present invention also provides swellbility Intelligent Dynamic test methods, mainly employ the swellbility Intelligent Dynamic of the present invention
Test device, and specifically comprise the following steps：
Solid sample is hung over specimen cup on specimen cup fixator together, sensor test disk is made to be connect with solid sample
It touches, adjusts the reading of displacement sensor, zero is set.Test solution will be packed into solution cup, promoting lifting tray makes in solution cup
Test solution flow into specimen cup in, start to test immediately.Due to the swelling character of solid sample, generation shifts up, and makes sensor
Test panel experiences shift length, and displacement sensor generates displacement signal and is transmitted in computer, by control button setting
The real-time change data of time step record displacement at any time, and by computer drawing curve.
Further scheme is：
The solid sample is consistent with the diameter of specimen cup.
Further scheme is：
The solid sample is directly to be machined by bulk sample or suppressed by powder sample by hydraulic press
It forms.
Further scheme is：
It is described to be suppressed by powder sample by hydraulic press, it is as follows：
1. circular gasket with holes is put bottom in specimen cup, a filter paper is put again above；
Powder sample is taken 2. weighing in the balance, is packed into specimen cup and gently shake makes sample end face smooth；
3. pressure bar is placed in, gently rotates left and right and contacted with sample end face；
4. being placed on oil pressure machine platform, pressurizeing and maintaining constant pressure time enough, treat that sample is compressed into tablet form, open release
Valve release；
5. taking out pressure bar, the height H of sheet specimens is measured, and a filter paper is placed above in molding sheet specimens.
6. sample will be suppressed on demand, hung on hanger together with specimen cup, the test panel of sensor is pressed in sheet examination
On sample, zero is adjusted.
It should be noted that step 1. in, using circular gasket with holes, it is with holes be in order to solvent from hole penetrate into specimen cup,
Sample is infiltrated, sample infiltration could be swollen in a solvent.Hole requirement is small and more.It is to cover pad to put a filter paper simultaneously
The hole of on piece avoids powder sample from being packed into powder sample when being suppressed in specimen cup and leaks out, and solvent is to penetrate filter paper to reach sample
Product.
Step 5. in, sheet sample due to surface contact solvent and first start be swollen and become shapeless, pass through place one
Filter paper is opened, is to be pressed on sample, to ensure the smooth of sample upper surface, ensures that the displacement data tested is accurate.
Step 6. in, after suppressing sample, specimen cup, gasket, filter paper, sample are hung over as an entirety on hanger.Cause
This this device is to provide two sets of specimen cups for oneself, and test is directly hung up after pressing sample.Sheet sample is powder sample in specimen cup
Interior direct pressing molding, therefore diameter is identical with specimen cup.Disk diameter is tested no more than sample diameter, specimen cup can be put in
It is interior.
Compared with prior art, the beneficial effects of the invention are as follows：The swellbility Intelligent Dynamic test method and dress of the present invention
Put the deficiency for overcoming conventional test methodologies, realize that paperless intelligent data acquire by being connect with computer, operation it is simple and
It realizes big data quantity follow-on test, reduces cost of labor；A variety of shapes such as powder, bulk can be used in the strong applicability of sample to be tested
The sample of state；Test overall process is all not required to detach sample with solvent, operates simple and data accuracys and favorable reproducibility；Knot
Double jacketed glass cup is closed, connection temperature control device can realize the swelling character research of macromolecule at different temperatures；Using bilateral
Road can test two samples to improve testing efficiency simultaneously.
Description of the drawings
Fig. 1 is the structure diagram of swellbility Intelligent Dynamic test device of the present invention.
Fig. 2 is the swelling curve tested in embodiment 1.
Fig. 3 is the swelling curve tested in embodiment 2.
Fig. 4 is the swelling curve tested in embodiment 3.
Specific embodiment
The present invention is further illustrated in the following with reference to the drawings and specific embodiments.
As shown in Figure 1, one embodiment of the present of invention provides a kind of swellbility Intelligent Dynamic test device, including：It hangs down
The sliding bar 13 directly set, the horizontal lifting pallet 11 being connected with sliding bar 13 by fixed knob 12 are set on lifting tray 11
Solution cup 1 is equipped with, 1 top of solution cup is provided with specimen cup 2, has sample 15 in specimen cup 2,2 bottom of specimen cup is provided with liquid
Hole 8 is penetrated into, displacement sensor 4 is installed above specimen cup, displacement sensor lower part is connected with sensor test disk 7, in displacement
Specimen cup fixator 3 is provided between sensor 4 and sensor test disk 7, displacement sensor is electrically connected with digital display instrument, digital display instrument
On statistics have shown screen 5 and control button 6, displacement sensor also communicates with computer.
In order to control temperature when swellbility is tested, temperature control water inlet 10 and temperature-control water outlet are respectively arranged on solution cup
Mouth 9, temperature control water inlet are located at below temperature-control water outlet mouth.
In order to keep temperature, temperature control chuck 14 is additionally provided on the outside of solution cup.
The specimen cup is smaller than solution cup size, can be put into solution cup.
The sensor test disk size is identical with specimen cup inside cross-sectional size.
The swellbility Intelligent Dynamic test device includes being located at two identical covering devices of sliding bar both sides.
An alternative embodiment of the invention provides a kind of swellbility Intelligent Dynamic test method, includes the following steps:
(1) it installs
1. swellbility Intelligent Dynamic test device is placed on experiment porch (platform is horizontal shockproof, calm)；
2. host is attached, and connect power cord with computer using data-interface；
3. being inserted into optical disk of software on computers, data acquisition software is installed.
(2) temperature setting
If 1. carrying out room temperature test, the step can be omitted；
It is required numerical value by the temperature setting of water-bath 2. being connect solution cup with water-bath using hose, opens water and follow
Ring.
(3) (by taking powder sample as an example, directly mechanical processing is consistent with specimen cup diameter if bulk sample for sample preparation
Disk)
1. prepare small-sized hand-operated hydraulic press, pressure bar, specimen cup, electronic balance, stopwatch and filter paper (with specimen cup diameter one
It causes)；
2. circular gasket with holes is put bottom in specimen cup, a filter paper is put again above；
Powder sample is taken 3. weighing in the balance, is packed into specimen cup and gently shake makes sample end face smooth；
4. pressure bar is placed in, gently rotates left and right and contacted with sample end face；
5. being placed on oil pressure machine platform, pressurizeing and maintaining constant pressure time enough, treat that sample is compressed into tablet form, open release
Valve release；
6. taking out pressure bar, the height H of sheet specimens is measured, and a filter paper is placed above in molding sheet specimens.
7. sample will be suppressed on demand, hung on hanger together with specimen cup, the test panel of sensor is pressed in sheet examination
On sample, zero is adjusted.
(4) start to test
1. the host switch of swellbility Intelligent Dynamic test device is opened, on computers operation data acquisition software, setting
Good port if the 1st tunnel (corresponding left side sample) shows number on the 2nd tunnel (corresponding right side sample), illustrates equipment company at this time
It is connected into work(；
2. setting suitable data acquisition time step-length according to the swelling rate of sample, START button is clicked on the screen
Runs software；
3. being fixed after adjustment lifting tray to suitable height using fixed knob, solvent is injected into liquid cup until solvent
It is flowed into specimen cup from specimen cup top, sample starts to expand immediately at this time, computer start recording data and real-time drawing function；
4. testing after a certain period of time, swelling curve gradually tends to be horizontal, illustrates to have arrived test terminal at this time, click " end "
Button can stop testing.Value after swelling curve horizontal stable is △ H；
5. selection " exporting to EXCEL " software automatically exports to data in Microsoft Excel, data are preserved, test terminates.
(5) data analysis
Swellbility：
Q=△ V/V=△ H/H
Wherein, △ V- are swollen the volume change of terminal sample；
The initial volume of V- samples；
△ H- are swollen the height change of terminal sample, are read by device record data, i.e. highest point value；
The elemental height of H- samples is obtained by directly measuring sample size.
Below swellbility Intelligent Dynamic test method is illustrated with three more specific embodiments.
Embodiment 1：
Sample to be tested：1 tunnel：PVB；2 tunnels：CAB
Solvent：Ethyl acetate
Implementation process：
(1) it installs
1. swellbility Intelligent Dynamic test device is placed on experiment porch (platform is horizontal shockproof, calm)；
2. host is attached, and connect power cord with computer using data-interface；
3. being inserted into optical disk of software on computers, data acquisition software is installed.
(2) temperature setting
Room temperature is tested, without set temperature.
(3) sample is suppressed
1. prepare small-sized hand-operated hydraulic press, pressure bar, specimen cup, electronic balance, stopwatch and filter paper (with specimen cup diameter one
It causes)；
2. circular gasket with holes is put bottom in specimen cup, a filter paper is put again above；
PVB and CAB powder samples are taken 3. weighing in the balance, is respectively charged into two specimen cups and gently shake puts down sample end face
It is whole；
4. pressure bar is placed in, gently rotates left and right and contacted with sample end face；
5. being placed on oil pressure machine platform, pressurizeing and maintaining constant pressure time enough, treat that sample is compressed into tablet form, open release
Valve release；
6. taking out pressure bar, the height H of sheet specimens is measured1And H2, and a filter is placed above in molding sheet specimens
Paper.
7. the sample that will be suppressed on demand, hangs over together with specimen cup on hanger, the test panel of sensor is pressed in sheet
On sample, zero is adjusted.
(4) start to test
1. the host switch of swellbility Intelligent Dynamic test device is opened, on computers operation data acquisition software, setting
Good port, the 1st tunnel show number with the 2nd road, illustrate equipment successful connection at this time；
2. it is 1min to set data acquisition time step-length, START button runs software is clicked on the screen；
3. adjustment lifting tray to suitable height after fixed using fixed knob, into liquid cup inject ethyl acetate until
Ethyl acetate is flowed into from specimen cup top in specimen cup, and sample starts to expand immediately at this time, and computer start recording data are simultaneously real
Shi Huitu, the figure of drafting is as shown in Figure 2；
4. after testing the sufficiently long time, swelling curve gradually tends to be horizontal, illustrate to have arrived test terminal at this time, click
" end " button stops test.Value after swelling curve horizontal stable is △ H1With △ H2；
5. selection " exporting to EXCEL " software automatically exports to data in Microsoft Excel, data are preserved, test terminates.
(5) data analysis
Swellbility：
QPVB- ethyl acetate=△ H1/H1
QCAB- ethyl acetate=△ H2/H2
Wherein, △ H1Reading is 2.33mm, H1Measured value is 3.99mm, and Q is calculatedPVB- ethyl acetate=58.4%；
△H2Reading is 1.94mm, H2Measured value is 3.20mm, and Q is calculatedCAB- ethyl acetate=60.6%.
Embodiment 2：
Sample to be tested：1 tunnel：PVB；2 tunnels：CAB
Solvent：Absolute ethyl alcohol
Implementation process：
(1) it installs
1. swellbility Intelligent Dynamic test device is placed on experiment porch (platform is horizontal shockproof, calm)；
2. host is attached, and connect power cord with computer using data-interface；
3. being inserted into optical disk of software on computers, data acquisition software is installed.
(2) temperature setting
Solution cup with water-bath is connect using hose, is 30 DEG C by the temperature setting of water-bath, opens water cycle.
(3) sample is suppressed
1. prepare small-sized hand-operated hydraulic press, pressure bar, specimen cup, electronic balance, stopwatch and filter paper (with specimen cup diameter one
It causes)；
2. circular gasket with holes is put bottom in specimen cup, a filter paper is put again above；
PVB and CAB powder samples are taken 3. weighing in the balance, is respectively charged into two specimen cups and gently shake puts down sample end face
It is whole；
4. pressure bar is placed in, gently rotates left and right and contacted with sample end face；
5. being placed on oil pressure machine platform, pressurizeing and maintaining constant pressure time enough, treat that sample is compressed into tablet form, open release
Valve release；
6. taking out pressure bar, the height H of sheet specimens is measured1And H2, and a filter is placed above in molding sheet specimens
Paper.
7. sample will be suppressed on demand, hung on hanger together with specimen cup, the test panel of sensor is pressed in sheet examination
On sample, zero is adjusted.
(4) start to test
1. the host switch of swellbility Intelligent Dynamic test device is opened, on computers operation data acquisition software, setting
Good port, the 1st tunnel show number with the 2nd road, illustrate equipment successful connection at this time；
2. it is 30s to set data acquisition time step-length, START button runs software is clicked on the screen；
3. adjustment lifting tray to suitable height after fixed using fixed knob, into liquid cup inject absolute ethyl alcohol until
Absolute ethyl alcohol is flowed into from specimen cup top in specimen cup, and sample starts to expand immediately at this time, and computer start recording data are simultaneously real
Shi Huitu, the figure of drafting is as shown in Figure 3；
4. after testing the sufficiently long time, swelling curve gradually tends to be horizontal, illustrate to have arrived test terminal at this time, click
" end " button stops test.Value after swelling curve horizontal stable is △ H1With △ H2；
5. selection " exporting to EXCEL " software automatically exports to data in Microsoft Excel, data are preserved, test terminates.
(5) data analysis
Swellbility：
QPVB- absolute ethyl alcohols=△ H1/H1
QCAB- absolute ethyl alcohols=△ H2/H2
Wherein, △ H1Reading is 1.19mm, H1Measured value is 1.97mm, and Q is calculatedPVB- absolute ethyl alcohols=60.4%；
△H2Reading is 1.13mm, H2Measured value is 1.93mm, and Q is calculatedCAB- absolute ethyl alcohols=58.5%.
Embodiment 3：
Sample to be tested：F2314
Solvent：1 tunnel：Ethyl acetate；2 tunnels：Absolute ethyl alcohol
Implementation process：
(1) it installs
1. swellbility Intelligent Dynamic test device is placed on experiment porch (platform is horizontal shockproof, calm)；
2. host is attached, and connect power cord with computer using data-interface；
3. being inserted into optical disk of software on computers, data acquisition software is installed.
(2) temperature setting
Solution cup with water-bath is connect using hose, is 30 DEG C by the temperature setting of water-bath, opens water cycle.
(3) sample is suppressed
1. prepare small-sized hand-operated hydraulic press, pressure bar, specimen cup, electronic balance, stopwatch and filter paper (with specimen cup diameter one
It causes)；
2. circular gasket with holes is put bottom in specimen cup, a filter paper is put again above；
F2314 powder samples are taken 3. weighing in the balance, is respectively charged into two specimen cups and gently shake makes sample end face smooth；
4. pressure bar is placed in, gently rotates left and right and contacted with sample end face；
5. being placed on oil pressure machine platform, pressurizeing and maintaining constant pressure time enough, treat that sample is compressed into tablet form, open release
Valve release；
6. taking out pressure bar, the height H of sheet specimens is measured1And H2, and a filter is placed above in molding sheet specimens
Paper.
7. sample will be suppressed on demand, hung on hanger together with specimen cup, the test panel of sensor is pressed in sheet examination
On sample, zero is adjusted.
(4) start to test
1. the host switch of swellbility Intelligent Dynamic test device is opened, on computers operation data acquisition software, setting
Good port, the 1st tunnel show number with the 2nd road, illustrate equipment successful connection at this time；
2. it is 60s to set data acquisition time step-length, START button runs software is clicked on the screen；
3. being fixed after adjustment lifting tray to suitable height using fixed knob, ethyl acetate is injected in liquid cup to the left
Injection absolute ethyl alcohol is until solvent is flowed into from specimen cup top in specimen cup in liquid cup to the right simultaneously, and sample is opened immediately at this time
Begin expansion, computer start recording data and real-time drawing function, and the figure of drafting is as shown in Figure 4；
4. after testing the sufficiently long time, swelling curve gradually tends to be horizontal, illustrate to have arrived test terminal at this time, click
" end " button stops test.Value after swelling curve horizontal stable is △ H1With △ H2；
5. selection " exporting to EXCEL " software automatically exports to data in Microsoft Excel, data are preserved, test terminates.
(5) data analysis
Swellbility：
QF2314- ethyl acetate=△ H1/H1
QF2314- absolute ethyl alcohols=△ H2/H2
Wherein, △ H1Reading is 2.68mm, H1Measured value is 0.87mm, and Q is calculatedF2314- ethyl acetate=308.0%；
△H2Reading is 0mm, H2Measured value is 0.87mm, and Q is calculatedF2314- absolute ethyl alcohols=0, show F2314 in anhydrous second
Do not occur Swelling in alcohol.
Although reference be made herein to invention has been described for explanatory embodiment of the invention, and above-described embodiment is only this hair
Bright preferable embodiment, embodiments of the present invention are simultaneously not restricted to the described embodiments, it should be appreciated that people in the art
Member can be designed that a lot of other modifications and embodiment, these modifications and embodiment will be fallen in principle disclosed in the present application
Within scope and spirit.
Claims (10)
1. a kind of swellbility Intelligent Dynamic test device, it is characterised in that including：
Vertically disposed sliding bar, the horizontal lifting pallet being connected with sliding bar by fixed knob are provided on lifting tray
Solution cup, solution cup top are provided with specimen cup, and specimen cup bottom is provided with liquid and penetrates into hole, and displacement is equipped with above specimen cup
Sensor, displacement sensor lower part are connected with sensor test disk, are provided between displacement sensor and sensor test disk
Specimen cup fixator, displacement sensor are electrically connected with digital display instrument, statistics have shown screen and control button on digital display instrument, displacement sensing
Device also communicates with computer.
2. swellbility Intelligent Dynamic test device according to claim 1, it is characterised in that：
Temperature control water inlet and temperature-control water outlet mouth are respectively arranged on solution cup, temperature control water inlet is located at below temperature-control water outlet mouth.
3. swellbility Intelligent Dynamic test device according to claim 2, it is characterised in that：
Temperature control chuck is additionally provided on the outside of solution cup.
4. swellbility Intelligent Dynamic test device according to claim 1, it is characterised in that：
The specimen cup is smaller than solution cup size, can be put into solution cup.
5. swellbility Intelligent Dynamic test device according to claim 1, it is characterised in that：
The sensor test disk size is identical with specimen cup inside cross-sectional size.
6. swellbility Intelligent Dynamic test device according to claim 1, it is characterised in that：
The swellbility Intelligent Dynamic test device includes being located at two identical covering devices of sliding bar both sides.
7. a kind of swellbility Intelligent Dynamic test method, it is characterised in that employ described in claim 1 to 6 any claim
Swellbility Intelligent Dynamic test device, and specifically comprise the following steps：
Solid sample is hung over specimen cup on specimen cup fixator together, sensor test disk is made to be contacted with solid sample, is adjusted
The reading of whole good displacement sensor sets zero；Test solution will be packed into solution cup, promotion lifting tray makes the test solution in solution cup
It flows into specimen cup, starts to test immediately；Due to the swelling character of solid sample, generation shifts up, and makes sensor test disk
Shift length is experienced, displacement sensor generates displacement signal and is transmitted in computer, the time step set by control button
The real-time change data of long record displacement at any time, and by computer drawing curve.
8. swellbility Intelligent Dynamic test method according to claim 7, it is characterised in that：
The solid sample is consistent with the diameter of specimen cup.
9. swellbility Intelligent Dynamic test method according to claim 7, it is characterised in that：
The solid sample be directly be machined by bulk sample or by powder sample by hydraulic press suppress and
Into.
10. swellbility Intelligent Dynamic test method according to claim 9, it is characterised in that：
It is described to be suppressed by powder sample by hydraulic press, it is as follows：
1. circular gasket with holes is put bottom in specimen cup, a filter paper is put again above；
Powder sample is taken 2. weighing in the balance, is packed into specimen cup and gently shake makes sample end face smooth；
3. pressure bar is placed in, gently rotates left and right and contacted with sample end face；
4. being placed on oil pressure machine platform, pressurizeing and maintaining constant pressure time enough, treat that sample is compressed into tablet form, open pressure-relief valve and unload
Pressure；
5. taking out pressure bar, the height H of sheet specimens is measured, and a filter paper is placed above in molding sheet specimens；
6. sample will be suppressed on demand, hung on hanger together with specimen cup, the test panel of sensor be pressed on sheet specimens,
Adjust zero.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711328264.XA CN108169417B (en) | 2017-12-13 | 2017-12-13 | Intelligent dynamic swelling degree testing device and testing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711328264.XA CN108169417B (en) | 2017-12-13 | 2017-12-13 | Intelligent dynamic swelling degree testing device and testing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108169417A true CN108169417A (en) | 2018-06-15 |
| CN108169417B CN108169417B (en) | 2020-05-22 |
Family
ID=62525848
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711328264.XA Active CN108169417B (en) | 2017-12-13 | 2017-12-13 | Intelligent dynamic swelling degree testing device and testing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108169417B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111965090A (en) * | 2020-09-15 | 2020-11-20 | 天津市捷威动力工业有限公司 | Device for measuring swelling characteristic of high polymer for lithium battery and characterization method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2124471U (en) * | 1991-12-27 | 1992-12-09 | 南开大学 | Swelling capacity tester |
| CN102313756A (en) * | 2010-07-09 | 2012-01-11 | 中科合成油技术有限公司 | Automatic swelling measuring device and swelling measuring method for coal |
| US9557315B2 (en) * | 2013-07-29 | 2017-01-31 | Schlumberger Technology Corporation | Confining pressure measurement for zonal isolation evaluation |
| CN106969995A (en) * | 2017-02-27 | 2017-07-21 | 江苏天和制药有限公司 | A kind of solid powder swellbility detection method |
-
2017
- 2017-12-13 CN CN201711328264.XA patent/CN108169417B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2124471U (en) * | 1991-12-27 | 1992-12-09 | 南开大学 | Swelling capacity tester |
| CN102313756A (en) * | 2010-07-09 | 2012-01-11 | 中科合成油技术有限公司 | Automatic swelling measuring device and swelling measuring method for coal |
| US9557315B2 (en) * | 2013-07-29 | 2017-01-31 | Schlumberger Technology Corporation | Confining pressure measurement for zonal isolation evaluation |
| CN106969995A (en) * | 2017-02-27 | 2017-07-21 | 江苏天和制药有限公司 | A kind of solid powder swellbility detection method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111965090A (en) * | 2020-09-15 | 2020-11-20 | 天津市捷威动力工业有限公司 | Device for measuring swelling characteristic of high polymer for lithium battery and characterization method |
| CN111965090B (en) * | 2020-09-15 | 2023-08-18 | 天津市捷威动力工业有限公司 | Measurement device and characterization method for swelling characteristics of high polymer for lithium battery |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108169417B (en) | 2020-05-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108593883A (en) | Strain type lateral expansion force testing device and measuring method | |
| CA1054395A (en) | Process and apparatus for capillary-viscosimetric determination of inhomogeneous liquids | |
| CN104165797B (en) | The shaft model testing equipment of pile-soil interface three under the conditions of seepage flow | |
| WO2005045635A3 (en) | Method and apparatus to reject electrical interference in a capacitive liquid level sensor system | |
| JPH07198583A (en) | Water permeability measuring apparatus and water permeability measuring method using the same | |
| CN207991970U (en) | Grain heap compressive deformation and grain heap-bulkhead interfacial pressure test device | |
| CN102901695A (en) | Rock sample porosity determination method | |
| CN107389530A (en) | A kind of Dispersion Test equipment suitable for hypotonicity soil | |
| CN108051054A (en) | It is a kind of in hospital can intelligent measure height and weight measuring instrument | |
| CN108287121B (en) | Device and method for measuring moisture characteristic curve of soil in dehumidification and moisture absorption processes | |
| CN110057669A (en) | A kind of pipe tobacco pliability detection method and pipe tobacco pliability detector | |
| CN205898567U (en) | Check out test set of capsule granules intensity and deformation volume for cigarette | |
| CN108169417A (en) | A kind of swellbility Intelligent Dynamic test device and test method | |
| CN103616317B (en) | Full-automatic equipment and method for measuring helium diffusion coefficient of material for reactor | |
| CN108896743B (en) | Multifunctional visual combined consolidation apparatus device | |
| CN202442942U (en) | Device for measuring seepage of porous medium | |
| CN205562330U (en) | Be applicable to core sample stripping gas measuring equipment | |
| CN203732397U (en) | Rapid emulsion explosive density detector | |
| CN107132298B (en) | A method of high hydroscopic resin water absorption rate is measured using tracer Headspace-Gas Chromatography | |
| CN203025067U (en) | Low-osmosis rock sample permeability tester | |
| CN207020049U (en) | A kind of Dispersion Test equipment suitable for hypotonicity soil | |
| CN212621789U (en) | Self-adaptive powder sample compactor | |
| CN105092404A (en) | Self-absorption experimental instrument and experimental detection method | |
| CN206281739U (en) | A kind of novel intelligent penetron | |
| CN109406758A (en) | Swelled ground three-dimensional expansion rate of water absorption and expansion force tester |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |