CN212293482U - Industrialized simultaneous distillation and extraction device - Google Patents
Industrialized simultaneous distillation and extraction device Download PDFInfo
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- CN212293482U CN212293482U CN202020877677.4U CN202020877677U CN212293482U CN 212293482 U CN212293482 U CN 212293482U CN 202020877677 U CN202020877677 U CN 202020877677U CN 212293482 U CN212293482 U CN 212293482U
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Abstract
The utility model discloses an industrialized simultaneous distillation extraction device, the outer wall of a reaction kettle is provided with an electric heating sleeve A, the bottom of the reaction kettle is connected with a liquid inlet pipe A, the liquid inlet pipe A is provided with a control valve A, the top of the reaction kettle is connected with a steam pipe, and the reaction kettle is communicated with the distillation kettle through the steam pipe; the distillation still is internally provided with a disc condenser A and a row condenser from top to bottom in sequence, the top of the distillation still is connected with a liquid inlet pipe B, and the liquid inlet pipe B is provided with a control valve B; and so on. The utility model has the advantages that: 1. realized making the better entering into steam of rose molecule through the distillation in, rose molecule in the steam makes the better condensation of steam through disk condenser A, formula condenser again, gets into the solvent in the stills, and the solvent is extracted the rose molecule in to the steam, and distillation extraction convenient operation. 2. The simultaneous distillation and extraction are realized, the water and the solvent can be recycled, the waste is reduced, and the water vapor directly heats the organic solvent.
Description
Technical Field
The utility model relates to a distillation extraction technical field, concretely relates to distillation extraction device when industrialization.
Background
The plant natural perfume is essential oil, extract, tincture, balsam and absolute oil, such as rose oil, jasmine extract, vanilla tincture, brandy, toluol, datura resin, narcissus oil, etc. which are produced by using flowers, branches, leaves, grasses, roots, barks, stems, seeds, fruits, etc. of aromatic plants as raw materials and adopting a steam distillation method, an extraction method, a squeezing method, an absorption method, etc.
After the perfume raw materials are collected through the steps of picking and the like, the perfume raw materials can be prepared into products through the process steps of distillation, extraction and the like, and the problems that the molecules of the perfume raw materials are not easy to extract in a solvent and the like can occur during distillation and extraction.
Disclosure of Invention
An object of the utility model is to provide an extraction device distills in time of industrialization solves the difficult better problem of extracting in the solvent of spices raw materials molecule in the vapor.
In order to solve the technical problem, the utility model adopts the following technical scheme:
an industrialized simultaneous distillation extraction device comprises a reaction kettle and a distillation kettle, wherein a feeding pipe orifice is formed in the side wall of the reaction kettle, a matched pipe cover is arranged on the feeding pipe orifice, an electric heating sleeve A is arranged on the outer wall of the reaction kettle, a liquid inlet pipe A is connected to the bottom of the reaction kettle, a control valve A is arranged on the liquid inlet pipe A, a steam pipe is connected to the top of the reaction kettle, and the reaction kettle is communicated with the distillation kettle through the steam pipe;
the distillation still is internally provided with a disc condenser A and a row condenser from top to bottom in sequence, the top of the distillation still is connected with a liquid inlet pipe B, and the liquid inlet pipe B is provided with a control valve B;
a liquid return pipe is connected in the distillation still, a control valve C is arranged on the liquid return pipe, one end of the liquid return pipe is arranged inside the distillation still, the tail end of the liquid return pipe inside the distillation still is arranged to be arc-shaped, and the other end of the liquid return pipe is communicated with a steam pipe.
Further, the method comprises the following steps of; the top of the distillation kettle is connected with an output pipe, the middle of the output pipe is connected with a four-way valve, and the four-way valve is respectively connected with a middle pipe and a connecting pipe; the middle pipe is communicated with the steam pipe; the connecting pipe is connected with the evaporating pot.
Further, the method comprises the following steps of; an electric heating sleeve B is arranged on the connecting side wall of the evaporating pot, the bottom of the electric heating sleeve B is connected with a liquid discharge pipe A, and a control valve D is arranged on the liquid discharge pipe A;
the top of the evaporation tank is connected with a gas pipe, a disc condenser B is arranged on the gas pipe, and the gas pipe is communicated with the collection tank.
Further, the method comprises the following steps of; collecting tank bottom connection drain pipe B is provided with the three-way valve in the middle of the drain pipe B, and the three-way valve connection circulating pipe is provided with the gear pump on the circulating pipe.
Further, the method comprises the following steps of; a filter screen is arranged in the middle of the reaction kettle, a fixed shaft is arranged on the lower surface of the filter screen, a rotating shaft is rotatably arranged on the fixed shaft and connected with a rotating motor, and stirring paddles are arranged on the rotating shaft;
the side wall of the stirring paddle is provided with a scraper blade, and the top wall of the stirring paddle is provided with a scraping brush.
Further, the method comprises the following steps of; the distillation still lateral wall is connected the distillation tube, is provided with the water pump on the distillation tube, and distillation tube one end is connected at the distillation still lower wall, and the distillation tube other end is connected at the top of distillation still and with the spray pipe intercommunication, evenly opened on the spray pipe has the water hole, and the pipe diameter of spray pipe is less than the pipe diameter of distillation pipe.
Further, the method comprises the following steps of; a liquid level sensor is arranged in the distillation kettle and connected with a controller, and the controller is connected with an alarm.
Further, the method comprises the following steps of; and observation windows are arranged on the side walls of the reaction kettle, the distillation kettle and the evaporation tank.
Compared with the prior art, the utility model discloses an at least, have one of following beneficial effect:
1. the perfume raw material molecules are distilled to enable the perfume raw material molecules to better enter water vapor, the perfume raw material molecules in the water vapor are condensed better through the disc condenser A and the column condenser, the solvent enters the distillation kettle and is extracted from the perfume raw material molecules in the steam, and the operation of distilling and extracting the perfume raw material molecules is convenient.
2. Whole device has realized distilling extraction simultaneously, and water and solvent can recycle, reduces extravagantly, and vapor direct heating organic solvent is convenient for carry out organic solvent and extracts.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is the connection schematic diagram of the filter screen in the reaction kettle of the utility model.
Fig. 3 is a schematic view of the connection of the distillation tube of the middle distillation still of the present invention.
In the figure: reaction kettle (1), distillation kettle (2), electric heating jacket A (3), liquid inlet pipe A (4), control valve A (5), steam pipe (6), disc condenser A (7), row condenser (8), liquid inlet pipe B (9), control valve B (10), liquid return pipe (11), control valve C (12), output pipe (13), four-way valve (14), intermediate pipe (15), connecting pipe (16), evaporating pot (17), electric heating jacket B (18), liquid discharge pipe A (19), control valve D (20), gas transmission pipe (21), disc condenser B (22), collecting pot (23), liquid discharge pipe B (24), three-way valve (25), gear pump (26), filter screen (27), fixed shaft (28), rotating shaft (29), rotating motor (30), stirring paddle (31), scraper blade (32), scraping brush (33), distillation pipe (34), water pump (35), The device comprises a spraying pipe (36), a liquid level sensor (37), a controller (38), an alarm (39), a circulating pipe (40), a feeding pipe opening (41) and a pipe cover (42).
Detailed Description
Fig. 1 to 3 illustrate the present invention, and in order to make the objects, technical solutions and advantages of the present invention more clearly understood, the present invention will be further described in detail with reference to the accompanying drawings and examples. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1:
an industrialized simultaneous distillation extraction device comprises a reaction kettle 1 and a distillation kettle 2, wherein a feeding pipe orifice 41 is arranged on the side wall of the reaction kettle 1, a matched pipe cover 42 is arranged on the feeding pipe orifice 41, an electric heating sleeve A3 is arranged on the outer wall of the reaction kettle 1, the bottom of the reaction kettle 1 is connected with a liquid inlet pipe A4, a control valve A5 is arranged on the liquid inlet pipe A4, the top of the reaction kettle 1 is connected with a steam pipe 6, and the reaction kettle 1 is communicated with the distillation kettle 2 through the steam pipe 6;
a disc condenser A7 and a column condenser 8 are sequentially arranged in the distillation kettle 2 from top to bottom, the top of the distillation kettle 2 is connected with a liquid inlet pipe B9, and a control valve B10 is arranged on the liquid inlet pipe B9;
a liquid return pipe 11 is connected in the distillation kettle 2, a control valve C12 is arranged on the liquid return pipe 11, one end of the liquid return pipe 11 is arranged in the distillation kettle 2, the tail end of the liquid return pipe 11 in the distillation kettle 2 is arranged in an arc shape, and the other end of the liquid return pipe 11 is communicated with the steam pipe 6; perfume raw materials are fed into a reaction kettle 1 through a feeding pipe port 41, water enters the reaction kettle 1 through a liquid inlet pipe A4, the reaction kettle 1 is heated through an electric heating sleeve A3, part of the heated perfume raw materials are melted into the water, water and steam melted into perfume raw material molecules are generated through heating, the steam enters a distillation kettle 2 through a steam pipe 6, the steam in the distillation kettle 2 is condensed twice through a disc condenser A7 and a line condenser 8, the disc condenser A7 adopts refrigerating liquid for condensation, the line condenser 8 adopts water cooling, the disc condenser A7 and the line condenser 8 enable the steam to be condensed better, a solvent enters the distillation kettle 2, the solvent such as petroleum ether, normal hexane and cyclohexane is mixed with the solvent, the perfume raw materials melted into the steam are extracted and enter the solvent, meanwhile, a part of uncondensed steam in the distillation kettle 2, and the steam with the solvent enters the reaction kettle 1 through a liquid return pipe 11 again, the end of the liquid return pipe 11 is arc-shaped, so that steam of the distillation kettle 2 can better enter the reaction kettle 1, and the steam is mixed with water heated by the reaction kettle 1, so that perfume raw material molecules are fused into the solvent, and a certain extraction effect is achieved.
Example 2:
on the basis of the embodiment 1, the top of the distillation kettle 2 is connected with an output pipe 13, the middle of the output pipe 13 is connected with a four-way valve 14, and the four-way valve 14 is respectively connected with a middle pipe 15 and a connecting pipe 16; the intermediate pipe 15 is communicated with the steam pipe 6; the connecting pipe 16 is connected with the evaporating pot 17; after the perfume raw material molecules and the solvent are blended and extracted, water can be discharged through an output pipe 13, or the output pipe 13 is connected with a four-way valve 14 and then is connected with a steam pipe 6 through a middle pipe 15 to enter the reaction kettle 1 for water supplement, so that water resources are saved, and meanwhile, the part of the water removed in the distillation kettle 2 enters an evaporation tank 17 through a connecting pipe 16.
Example 3:
on the basis of the embodiment 1-2, the connecting side wall of the evaporation tank 17 is provided with an electric heating jacket B18, the bottom of the electric heating jacket B18 is connected with a liquid discharge pipe A19, and a control valve D20 is arranged on the liquid discharge pipe A19; the top of the evaporation tank 17 is connected with a gas pipe 21, a disc condenser B22 is arranged on the gas pipe 21, and the gas pipe 21 is communicated with the collection tank 23; the liquid part of the evaporation tank 17 is distilled by an electric heating jacket B18, the distilled essential oil is output by a liquid discharge pipe A19, the solvent in the evaporation tank 17 is output by an air pipe 21 during heating, and the heated solvent is cooled by a disc condenser B22.
Example 4:
on the basis of the embodiment 1-3, the bottom of the collecting tank 23 is connected with a liquid discharge pipe B24, the middle of the liquid discharge pipe B24 is provided with a three-way valve 25, the three-way valve 25 is connected with a circulating pipe 40, and the circulating pipe 40 is provided with a gear pump 26; the cooled solvent is discharged through a liquid discharge pipe B24 or enters the distillation kettle 2 through an air pipe 21 under the action of the gear pump 26, so that the recycling of the solvent is realized, and the waste is reduced.
Example 5:
on the basis of the embodiment 1-4, a filter screen 27 is arranged in the middle of the reaction kettle 1, a fixed shaft 28 is arranged on the lower surface of the filter screen 27, a rotating shaft 29 is rotatably arranged on the fixed shaft 28, the rotating shaft 29 is connected with a rotating motor 30, and stirring paddles 31 are arranged on the rotating shaft 29;
the side wall of the stirring paddle 31 is provided with a scraping plate 32, and the top wall of the stirring paddle 31 is provided with a scraping brush 33; the setting of filter screen 27 blocks that spices raw materials molecule is not for the spices raw materials that melts into the aquatic, and stirring rake 31 plays the stirring effect, and the better income aquatic of spices raw materials molecule of being convenient for scrapes brush 33 and makes spices raw materials paste on reation kettle 1 wall, scrapes the setting of brush 33 and waters spices raw materials and plug up filter screen 27.
Example 6:
on the basis of the embodiment 1-5, the side wall of the distillation kettle 2 is connected with a distillation pipe 34, a water pump 35 is arranged on the distillation pipe 34, one end of the distillation pipe 34 is connected with the lower wall of the distillation kettle 2, the other end of the distillation pipe 34 is connected with the top of the distillation kettle 2 and is communicated with a spray pipe 36, water holes are uniformly formed in the spray pipe 36, and the pipe diameter of the spray pipe 36 is smaller than that of the distillation pipe 34; the arrangement of the distillation tube 3 enables liquid in the distillation kettle 2 to realize circulation flow, so that spice raw material molecules can be conveniently extracted and enter a solvent, and the pipe diameter of the spray pipe 36 is smaller than that of the distillation pipe 34, so that the circulation liquid of the distillation pipe 34 can be well mixed through the spray pipe 36.
Example 7:
on the basis of the embodiments 1 to 6, a liquid level sensor 37 is arranged in the distillation kettle 2, the liquid level sensor 37 is connected with a controller 38, and the controller 38 is connected with an alarm 39; liquid level sensor 37 can monitor the liquid level of distillation still 2, and better extraction is carried out in distillation still 2.
Example 8:
on the basis of the embodiments 1 to 7, the side walls of the reaction kettle 1, the distillation kettle 2 and the evaporation tank 17 are all provided with observation windows; the arrangement of the observation window can better ensure the liquid and the reaction condition in the reaction kettle 1, the distillation kettle 2 and the evaporation tank 17.
Although the invention has been described herein with reference to a number of illustrative embodiments thereof, it should be understood that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the spirit and scope of the principles of this invention. More specifically, various variations and modifications are possible in the component parts and/or arrangements of the subject combination arrangement within the scope of the disclosure, the drawings and the appended claims. In addition to variations and modifications in the component parts and/or arrangements, other uses will also be apparent to those skilled in the art.
Claims (8)
1. An industrialized simultaneous distillation extraction device, which comprises a reaction kettle (1) and a distillation kettle (2), and is characterized in that: a feeding pipe orifice (41) is arranged on the side wall of the reaction kettle (1), a matched pipe cover (42) is arranged on the feeding pipe orifice (41), an electric heating sleeve A (3) is arranged on the outer wall of the reaction kettle (1), a liquid inlet pipe A (4) is connected to the bottom of the reaction kettle (1), a control valve A (5) is arranged on the liquid inlet pipe A (4), a steam pipe (6) is connected to the top of the reaction kettle (1), and the reaction kettle (1) is communicated with the distillation kettle (2) through the steam pipe (6);
a disc condenser A (7) and a row condenser (8) are sequentially arranged in the distillation kettle (2) from top to bottom, the top of the distillation kettle (2) is connected with a liquid inlet pipe B (9), and a control valve B (10) is arranged on the liquid inlet pipe B (9);
a liquid return pipe (11) is connected in the distillation kettle (2), a control valve C (12) is arranged on the liquid return pipe (11), one end of the liquid return pipe (11) is arranged inside the distillation kettle (2), the tail end of the liquid return pipe (11) inside the distillation kettle (2) is arranged to be arc-shaped, and the other end of the liquid return pipe (11) is communicated with a steam pipe (6).
2. An industrial simultaneous distillation extraction apparatus according to claim 1, wherein: the top of the distillation kettle (2) is connected with an output pipe (13), the middle of the output pipe (13) is connected with a four-way valve (14), and the four-way valve (14) is respectively connected with a middle pipe (15) and a connecting pipe (16); the middle pipe (15) is communicated with the steam pipe (6); the connecting pipe (16) is connected with the evaporating pot (17).
3. An industrial simultaneous distillation extraction apparatus according to claim 2, wherein: an electric heating sleeve B (18) is arranged on the connecting side wall of the evaporating pot (17), the bottom of the electric heating sleeve B (18) is connected with a liquid discharge pipe A (19), and a control valve D (20) is arranged on the liquid discharge pipe A (19); the top of the evaporation tank (17) is connected with a gas pipe (21), a disc condenser B (22) is arranged on the gas pipe (21), and the gas pipe (21) is communicated with a collecting tank (23).
4. An industrial simultaneous distillation extraction apparatus according to claim 3, wherein: the bottom of the collecting tank (23) is connected with a liquid discharge pipe B (24), a three-way valve (25) is arranged in the middle of the liquid discharge pipe B (24), the three-way valve (25) is connected with a circulating pipe (40), and a gear pump (26) is arranged on the circulating pipe (40).
5. An industrial simultaneous distillation extraction apparatus according to claim 1, wherein: a filter screen (27) is arranged in the middle of the reaction kettle (1), a fixed shaft (28) is arranged on the lower surface of the filter screen (27), a rotating shaft (29) is rotatably arranged on the fixed shaft (28), the rotating shaft (29) is connected with a rotating motor (30), and stirring paddles (31) are arranged on the rotating shaft (29); the side wall of the stirring paddle (31) is provided with a scraping plate (32), and the top wall of the stirring paddle (31) is provided with a scraping brush (33).
6. An industrial simultaneous distillation extraction apparatus according to claim 1, wherein: still (2) lateral wall connection distillation tube (34), be provided with water pump (35) on distillation tube (34), distillation tube (34) one end is connected at distillation still (2) lower wall, and distillation tube (34) other end is connected at the top of distillation still (2) and with spray pipe (36) intercommunication, evenly opens on spray pipe (36) and has the water hole, and the pipe diameter of spray pipe (36) is less than the pipe diameter of distillation tube (34).
7. An industrial simultaneous distillation extraction apparatus according to claim 1, wherein: a liquid level sensor (37) is arranged in the distillation kettle (2), the liquid level sensor (37) is connected with a controller (38), and the controller (38) is connected with an alarm (39).
8. An industrial simultaneous distillation extraction apparatus according to claim 1, wherein: and observation windows are arranged on the side walls of the reaction kettle (1), the distillation kettle (2) and the evaporation tank (17).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020877677.4U CN212293482U (en) | 2020-05-22 | 2020-05-22 | Industrialized simultaneous distillation and extraction device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020877677.4U CN212293482U (en) | 2020-05-22 | 2020-05-22 | Industrialized simultaneous distillation and extraction device |
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| Publication Number | Publication Date |
|---|---|
| CN212293482U true CN212293482U (en) | 2021-01-05 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202020877677.4U Withdrawn - After Issue CN212293482U (en) | 2020-05-22 | 2020-05-22 | Industrialized simultaneous distillation and extraction device |
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| CN (1) | CN212293482U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115433637A (en) * | 2022-09-29 | 2022-12-06 | 东莞市鸿馥生物科技有限公司 | Preparation method of green tea spice |
-
2020
- 2020-05-22 CN CN202020877677.4U patent/CN212293482U/en not_active Withdrawn - After Issue
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115433637A (en) * | 2022-09-29 | 2022-12-06 | 东莞市鸿馥生物科技有限公司 | Preparation method of green tea spice |
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| AV01 | Patent right actively abandoned |
Granted publication date: 20210105 Effective date of abandoning: 20230829 |