CN212152404U - A rare earth continuous precipitation device - Google Patents

A rare earth continuous precipitation device Download PDF

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CN212152404U
CN212152404U CN202020500566.1U CN202020500566U CN212152404U CN 212152404 U CN212152404 U CN 212152404U CN 202020500566 U CN202020500566 U CN 202020500566U CN 212152404 U CN212152404 U CN 212152404U
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inner shell
rare earth
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tank
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谢恒辉
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Longnan Xinhui Functional Materials Co ltd
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Abstract

本实用新型涉及稀土生产设备领域,尤其涉及一种稀土连续沉淀装置,包含溶解罐和沉降箱,所述溶解罐内部固定有内壳,所述内壳上均匀分布有贯穿内壳的过滤通孔,所述内壳底部与固定在溶解罐底部的排渣管Ⅰ固定连接,所述排渣管Ⅰ上从上往下依次固定有阀门Ⅱ和阀门Ⅲ,所述内壳上方的溶解罐罐体上分别固定有进水管、进料管和搅拌电机,搅拌电机输出端固定有转轴,所述转轴与内壳内部的搅拌叶固定连接,转轴底部还固定有螺旋叶,所述溶解罐底部通过导液管连接沉降箱,所述沉降箱内部横向固定有挡板,所述挡板上方固定有过滤板,所述挡板与过滤板将沉降箱分为过滤腔和排液腔,所述过滤腔与前述导液管相连。通过本装置可以持续对稀土矿石溶解过滤。

Figure 202020500566

The utility model relates to the field of rare earth production equipment, in particular to a rare earth continuous precipitation device, comprising a dissolving tank and a settling tank. An inner shell is fixed inside the dissolving tank, and filtering through holes penetrating the inner shell are uniformly distributed on the inner shell. , the bottom of the inner shell is fixedly connected with the slag discharge pipe I fixed at the bottom of the dissolving tank, the valve II and the valve III are fixed on the slag discharge pipe I in order from top to bottom, and the dissolving tank body above the inner shell A water inlet pipe, a feeding pipe and a stirring motor are respectively fixed on the upper part, and a rotating shaft is fixed at the output end of the stirring motor. The rotating shaft is fixedly connected with the stirring blade inside the inner shell. The bottom of the rotating shaft is also fixed with a spiral blade. The liquid pipe is connected to the settling tank, a baffle plate is fixed laterally inside the settling tank, and a filter plate is fixed above the baffle plate. The baffle plate and the filter plate divide the settling tank into a filter cavity and a liquid discharge cavity. The filter cavity Connected to the aforementioned catheter. The device can continuously dissolve and filter rare earth ores.

Figure 202020500566

Description

一种稀土连续沉淀装置A rare earth continuous precipitation device

【技术领域】【Technical field】

本实用新型涉及稀土生产设备领域,尤其涉及一种稀土连续沉淀装置。The utility model relates to the field of rare earth production equipment, in particular to a rare earth continuous precipitation device.

【背景技术】【Background technique】

中国是世界上稀土储量最多的国家,且元素分配全面。经过近40年的发展,全国已建立世界上最庞大的稀土工业,成为世界最大的稀土生产国,最大的稀土消费国和最大的稀土供应国。但是现有的稀土沉淀装置不能实现对稀土的连续沉淀,降低了稀土的生产效率,而且现有的稀土沉淀装置在稀土排出时容易出现残留在沉淀箱内部的底部。China is the country with the largest rare earth reserves in the world, and has a comprehensive distribution of elements. After nearly 40 years of development, the country has established the world's largest rare earth industry, becoming the world's largest rare earth producer, largest rare earth consumer and largest rare earth supplier. However, the existing rare earth precipitation device cannot realize the continuous precipitation of rare earth, which reduces the production efficiency of rare earth, and the existing rare earth precipitation device is likely to remain at the bottom of the sedimentation tank when the rare earth is discharged.

本实用新型即是针对现有技术的不足而研究提出的。The utility model is researched and proposed for the deficiencies of the prior art.

【实用新型内容】【Content of utility model】

本实用新型的目的是克服上述现有技术的缺点,提供了一种稀土连续沉淀装置。The purpose of the utility model is to overcome the above-mentioned shortcomings of the prior art and provide a rare earth continuous precipitation device.

本实用新型可以通过以下技术方案来实现:The utility model can be realized through the following technical solutions:

本实用新型公开了一种稀土连续沉淀装置,包含溶解罐和沉降箱,所述溶解罐内部固定有内壳,所述内壳上均匀分布有贯穿内壳的过滤通孔,所述内壳底部与固定在溶解罐底部的排渣管Ⅰ固定连接,所述排渣管Ⅰ上从上往下依次固定有阀门Ⅱ和阀门Ⅲ,所述内壳上方的溶解罐罐体上分别固定有进水管、进料管和搅拌电机,所述搅拌电机输出端固定有转轴,所述转轴与内壳内部的搅拌叶固定连接,所述转轴底部还固定有螺旋叶,所述溶解罐底部通过导液管连接沉降箱,所述导液管上固定有阀门Ⅰ,所述沉降箱内部横向固定有挡板,所述挡板上方固定有过滤板,所述挡板与过滤板将沉降箱分为过滤腔和排液腔,所述过滤腔与前述导液管相连,所述过滤腔底部的沉降箱上还固定有排渣管Ⅱ,所述排渣管Ⅱ上从上往下分别固定有阀门Ⅳ和阀门Ⅴ,所述排液腔底部还通过排液管与溶液储罐相连。通过进料管往溶解罐内添加待溶解的稀土原料,通过进水管往溶解罐中添加稀土溶解液,搅拌电机驱动搅拌叶转动,对内壳内的原料进行混合搅拌,稀土溶解后无法溶解的残渣沉降到内壳底部,开启阀门Ⅱ,关闭阀门Ⅲ,无法溶解的残渣进入到阀门Ⅱ与阀门Ⅲ之间的排渣管Ⅰ中,稀土矿石溶解后开启导液管上的阀门Ⅰ,由于沉降箱的高度比溶解罐低,稀土溶液通过导液管进入到沉降箱的过滤腔中,开启阀门Ⅳ关闭阀门Ⅴ,小颗粒稀土残渣沉降到阀门Ⅴ与阀门Ⅳ之间的排渣管Ⅱ中,并且由于过滤板设置在过滤腔上方,由于过滤板过滤及无法溶解的稀土残渣自动沉降,稀土溶液进入排液腔中经过排液管进入到溶液储罐中,关闭阀门Ⅰ,继续往溶解罐中添加稀土矿石及溶解液,待阀门Ⅱ与阀门Ⅲ之间的排渣管Ⅰ中堆积满稀土残渣后,关闭阀门Ⅱ开启阀门Ⅲ,排渣管Ⅰ中的残渣从排渣管Ⅰ底部流出后输送到压滤机中压滤,当稀土残渣堆积满阀门Ⅴ与阀门Ⅳ之间的排渣管Ⅱ后,关闭阀门Ⅳ,开启阀门Ⅴ,将稀土残渣排出后输送到压滤机中压滤,通过本装置可以实现稀土矿石的有效溶解,并且可以有效将稀土溶液过滤,并且本装置可以实现连续对稀土矿石溶解过滤,进一步的提高稀土生产效率,并且通过转轴带动螺旋叶转动,可以有效避免稀土残渣堆积在溶解罐内无法排出的现象发生。The utility model discloses a rare earth continuous precipitation device, which comprises a dissolving tank and a settling tank. An inner shell is fixed inside the dissolving tank. The inner shell is evenly distributed with filtration through holes penetrating the inner shell. It is fixedly connected with the slag discharge pipe I fixed at the bottom of the dissolving tank, the valve II and the valve III are fixed on the slag discharge pipe I in order from top to bottom, and the water inlet pipe is respectively fixed on the dissolving tank above the inner shell. , a feeding pipe and a stirring motor, the output end of the stirring motor is fixed with a rotating shaft, the rotating shaft is fixedly connected with the stirring blade inside the inner shell, the bottom of the rotating shaft is also fixed with a spiral blade, and the bottom of the dissolving tank passes through a liquid conduit Connecting to the sedimentation tank, a valve I is fixed on the liquid conduit, a baffle plate is fixed laterally inside the sedimentation tank, a filter plate is fixed above the baffle plate, and the baffle plate and the filter plate divide the sedimentation tank into a filter cavity and drainage chamber, the filter chamber is connected with the aforesaid conduit pipe, the sedimentation box at the bottom of the filter chamber is also fixed with a slag discharge pipe II, and the slag discharge pipe II is respectively fixed with valves IV and Valve V, the bottom of the drainage cavity is also connected with the solution storage tank through a drainage pipe. Add rare earth raw materials to be dissolved into the dissolving tank through the feeding pipe, add rare earth dissolving liquid into the dissolving tank through the water inlet pipe, the stirring motor drives the stirring blade to rotate, and mixes and stirs the raw materials in the inner shell. The residue settles to the bottom of the inner shell. Open valve II and close valve III. The insoluble residue enters into the slag discharge pipe I between valve II and valve III. After the rare earth ore is dissolved, open valve I on the catheter. The height of the tank is lower than that of the dissolution tank. The rare earth solution enters the filter cavity of the settling tank through the catheter, and the valve IV is opened and the valve V is closed. And because the filter plate is set above the filter chamber, due to the filter plate filtering and the automatic sedimentation of the insoluble rare earth residue, the rare earth solution enters the drain chamber and enters the solution storage tank through the drain pipe, close the valve I, and continue to the dissolution tank. Add rare earth ore and dissolved solution. After the slag discharge pipe I between valve II and valve III is full of rare earth residues, close valve II and open valve III. The residue in slag discharge pipe I flows out from the bottom of slag discharge pipe I and then transported. After the rare earth residue is accumulated in the slag discharge pipe II between valve V and valve IV, close valve IV, open valve V, and discharge the rare earth residue and transport it to the filter press for pressure filtration, through The device can realize the effective dissolution of rare earth ores, and can effectively filter the rare earth solution, and the device can realize the continuous dissolution and filtration of rare earth ores, which further improves the production efficiency of rare earth, and drives the spiral blade to rotate through the rotating shaft, which can effectively avoid rare earth residues The phenomenon that the accumulation in the dissolution tank cannot be discharged occurs.

本实用新型与现有的技术相比有如下优点:Compared with the existing technology, the utility model has the following advantages:

1.通过本装置可以实现稀土矿石的有效溶解,并且可以有效将稀土溶液过滤。1. Through the device, the rare earth ore can be effectively dissolved, and the rare earth solution can be effectively filtered.

2.本装置可以实现连续对稀土矿石溶解过滤,进一步的提高稀土生产效率。2. The device can continuously dissolve and filter rare earth ore, and further improve the production efficiency of rare earth.

3.通过转轴带动螺旋叶转动,可以有效避免稀土残渣堆积在溶解罐内无法排出的现象发生。3. The rotating shaft drives the spiral blade to rotate, which can effectively avoid the phenomenon that rare earth residues accumulate in the dissolving tank and cannot be discharged.

【附图说明】【Description of drawings】

下面结合附图对本实用新型的具体实施方式作进一步详细说明,其中:The specific embodiments of the present utility model will be described in further detail below in conjunction with the accompanying drawings, wherein:

图1为本实用新型的结构示意图;Fig. 1 is the structural representation of the utility model;

图2为本实用新型的俯视图;Fig. 2 is the top view of the utility model;

图3为本实用新型的前视图;Fig. 3 is the front view of the utility model;

图4为图2中A-A处剖视图;Figure 4 is a sectional view at A-A in Figure 2;

图中:1、沉降箱;2、溶解罐;3、进水管;4、进料管;5、搅拌电机;6、排渣管Ⅰ;7、导液管;8、阀门Ⅰ;9、排渣管Ⅱ;10、阀门Ⅱ;11、阀门Ⅲ;12、阀门Ⅳ;13、阀门Ⅴ;14、转轴;15、搅拌叶;16、螺旋叶;17、挡板;18、过滤板;19、排液管;20、内壳;In the figure: 1. Settling tank; 2. Dissolving tank; 3. Water inlet pipe; 4. Feeding pipe; 5. Stirring motor; 6. Slag discharge pipe I; 7. Liquid conduit; 8. Valve I; Slag pipe II; 10, valve II; 11, valve III; 12, valve IV; 13, valve V; 14, rotating shaft; 15, stirring blade; 16, spiral blade; 17, baffle plate; 18, filter plate; 19, Drain pipe; 20. Inner shell;

【具体实施方式】【Detailed ways】

下面结合附图对本实用新型的实施方式作详细说明:Embodiments of the present utility model are described in detail below in conjunction with the accompanying drawings:

如图1至图4所示,本实用新型公开了一种稀土连续沉淀装置,包含溶解罐2和沉降箱1,溶解罐2内部固定有内壳20,内壳20上均匀分布有贯穿内壳20的过滤通孔,内壳20底部与固定在溶解罐2底部的排渣管Ⅰ6固定连接,排渣管Ⅰ6上从上往下依次固定有阀门Ⅱ10和阀门Ⅲ11,内壳20上方的溶解罐2罐体上分别固定有进水管3、进料管4和搅拌电机5,搅拌电机5输出端固定有转轴14,转轴14与内壳20内部的搅拌叶15固定连接,转轴14底部还固定有螺旋叶16,溶解罐2底部通过导液管7连接沉降箱1,导液管7上固定有阀门Ⅰ8,沉降箱1内部横向固定有挡板17,挡板17上方固定有过滤板18,挡板17与过滤板18将沉降箱1分为过滤腔和排液腔,过滤腔与导液管7相连,过滤腔底部的沉降箱1上还固定有排渣管Ⅱ9,排渣管Ⅱ9上从上往下分别固定有阀门Ⅳ12和阀门Ⅴ13,排液腔底部还通过排液管19与溶液储罐(未图示)相连。通过进料管4往溶解罐2内添加待溶解的稀土原料,通过进水管3往溶解罐2中添加稀土溶解液,搅拌电机5驱动搅拌叶15转动,对内壳20内的原料进行混合搅拌,稀土溶解后无法溶解的残渣沉降到内壳20底部,开启阀门Ⅱ10,关闭阀门Ⅲ11,无法溶解的残渣进入到阀门Ⅱ10与阀门Ⅲ11之间的排渣管Ⅰ6中,稀土矿石溶解后开启导液管7上的阀门Ⅰ8,由于沉降箱1的高度比溶解罐2低,稀土溶液通过导液管7进入到沉降箱1的过滤腔中,开启阀门Ⅳ12关闭阀门Ⅴ13,小颗粒稀土残渣沉降到阀门Ⅴ13与阀门Ⅳ12之间的排渣管Ⅱ9中,并且由于过滤板18设置在过滤腔上方,由于过滤板18过滤及无法溶解的稀土残渣自动沉降,稀土溶液进入排液腔中经过排液管19进入到溶液储罐中,关闭阀门Ⅰ8,继续往溶解罐2中添加稀土矿石及溶解液,待阀门Ⅱ10与阀门Ⅲ11之间的排渣管Ⅰ6中堆积满稀土残渣后,关闭阀门Ⅱ10开启阀门Ⅲ11,排渣管Ⅰ6中的残渣从排渣管Ⅰ6底部流出后输送到压滤机中压滤,当稀土残渣堆积满阀门Ⅴ13与阀门Ⅳ12之间的排渣管Ⅱ9后,关闭阀门Ⅳ12,开启阀门Ⅴ13,将稀土残渣排出后输送到压滤机中压滤,通过本装置可以实现稀土矿石的有效溶解,并且可以有效将稀土溶液过滤,并且本装置可以实现连续对稀土矿石溶解过滤,进一步的提高稀土生产效率,并且通过转轴14带动螺旋叶16转动,可以有效避免稀土残渣堆积在溶解罐2内无法排出的现象发生。As shown in FIGS. 1 to 4 , the present invention discloses a rare earth continuous precipitation device, which includes a dissolving tank 2 and a settling tank 1 . An inner shell 20 is fixed inside the dissolving tank 2 , and the inner shell 20 is evenly distributed with penetrating inner shells. 20, the bottom of the inner shell 20 is fixedly connected with the slag discharge pipe I6 fixed at the bottom of the dissolving tank 2, the slag discharge pipe I6 is fixed with valve II10 and valve III11 from top to bottom in order, and the dissolving tank above the inner shell 20 2. A water inlet pipe 3, a feeding pipe 4 and a stirring motor 5 are respectively fixed on the tank body. The output end of the stirring motor 5 is fixed with a rotating shaft 14. The rotating shaft 14 is fixedly connected with the stirring blade 15 inside the inner shell 20, and the bottom of the rotating shaft 14 is also fixed with Spiral blade 16, the bottom of the dissolving tank 2 is connected to the sedimentation tank 1 through a liquid conduit 7, a valve I8 is fixed on the liquid conduit 7, a baffle plate 17 is fixed laterally inside the sedimentation tank 1, and a filter plate 18 is fixed above the baffle plate 17. The plate 17 and the filter plate 18 divide the sedimentation tank 1 into a filter chamber and a liquid discharge chamber. The filter chamber is connected with the liquid conduit 7. The sedimentation tank 1 at the bottom of the filter chamber is also fixed with a slag discharge pipe II9. The valve IV12 and the valve V13 are respectively fixed from top to bottom, and the bottom of the liquid discharge chamber is also connected to the solution storage tank (not shown) through a liquid discharge pipe 19 . The rare earth raw material to be dissolved is added into the dissolving tank 2 through the feeding pipe 4, the rare earth dissolving liquid is added into the dissolving tank 2 through the water inlet pipe 3, the stirring motor 5 drives the stirring blade 15 to rotate, and the raw materials in the inner shell 20 are mixed and stirred After the rare earth is dissolved, the insoluble residue settles to the bottom of the inner shell 20, open the valve II10, close the valve III11, the insoluble residue enters the slag discharge pipe I6 between the valve II10 and the valve III11, after the rare earth ore is dissolved, open the liquid guide The valve I8 on the pipe 7, because the height of the sedimentation tank 1 is lower than the dissolution tank 2, the rare earth solution enters the filter cavity of the sedimentation tank 1 through the conduit 7, opens the valve IV12 and closes the valve V13, and the small particle rare earth residue settles into the valve. In the slag discharge pipe II9 between V13 and valve IV12, and because the filter plate 18 is set above the filter chamber, the rare earth solution enters the discharge chamber and passes through the discharge pipe 19 because the filter plate 18 filters and the insoluble rare earth residue automatically settles. Enter into the solution storage tank, close valve I8, continue to add rare earth ore and dissolving liquid into dissolving tank 2, and after the slag discharge pipe I6 between valve II10 and valve III11 is full of rare earth residues, close valve II10 and open valve III11 , the residue in the slag discharge pipe I6 flows out from the bottom of the slag discharge pipe I6 and is transported to the filter press for pressure filtration. When the rare earth residue accumulates in the slag discharge pipe II9 between the valve V13 and the valve IV12, close the valve IV12 and open the valve. Ⅴ13. After the rare earth residue is discharged, it is transported to the filter press for pressure filtration. Through this device, the rare earth ore can be effectively dissolved, and the rare earth solution can be effectively filtered, and the device can continuously dissolve and filter the rare earth ore, which further improves the Rare earth production efficiency is improved, and the rotating shaft 14 drives the spiral blades 16 to rotate, which can effectively avoid the phenomenon that rare earth residues accumulate in the dissolving tank 2 and cannot be discharged.

以上所述仅是本实用新型的优选实施方式,应当指出,对于本技术领域的普通技术人员来说,在不脱离本实用新型技术原理的前提下,可以对这些实施例进行多种变化、修改、替换和变型,这些变化、修改、替换和变型,也应视为本实用新型的保护范围。The above are only the preferred embodiments of the present invention. It should be pointed out that for those skilled in the art, various changes and modifications can be made to these embodiments without departing from the technical principles of the present invention. , replacements and modifications, these changes, modifications, replacements and modifications should also be regarded as the protection scope of the present invention.

Claims (1)

1. A rare earth continuous precipitation device comprises a dissolving tank and a sedimentation tank, and is characterized in that an inner shell is fixed inside the dissolving tank, filter through holes penetrating through the inner shell are uniformly distributed on the inner shell, the bottom of the inner shell is fixedly connected with a slag discharge pipe I fixed at the bottom of the dissolving tank, a valve II and a valve III are sequentially fixed on the slag discharge pipe I from top to bottom, a water inlet pipe, a feed pipe and a stirring motor are respectively fixed on a dissolving tank body above the inner shell, a rotating shaft is fixed at the output end of the stirring motor and fixedly connected with stirring blades inside the inner shell, spiral blades are further fixed at the bottom of the rotating shaft, the bottom of the dissolving tank is connected with the sedimentation tank through a liquid guide pipe, the valve I is fixed on the liquid guide pipe, a baffle is transversely fixed inside the sedimentation tank, a filter plate is fixed above the baffle, and the sedimentation tank is divided into a filter cavity and a liquid discharge cavity, the filter cavity is connected with the liquid guide pipe, a slag discharge pipe II is further fixed on the settling tank at the bottom of the filter cavity, a valve IV and a valve V are respectively fixed on the slag discharge pipe II from top to bottom, and the bottom of the liquid discharge cavity is further connected with a solution storage tank through a liquid discharge pipe.
CN202020500566.1U 2020-04-08 2020-04-08 A rare earth continuous precipitation device Expired - Fee Related CN212152404U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113373327A (en) * 2021-06-11 2021-09-10 河北地质大学 Rare earth element extraction element in mineral

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113373327A (en) * 2021-06-11 2021-09-10 河北地质大学 Rare earth element extraction element in mineral
CN113373327B (en) * 2021-06-11 2023-01-17 河北地质大学 A device for extracting rare earth elements in minerals

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