CN212092247U

CN212092247U - Rotary methyl phenyl silicon reaction tank

Info

Publication number: CN212092247U
Application number: CN202020320878.4U
Authority: CN
Inventors: 李婷; 降伟明
Original assignee: Jilin Donghu Silicone Co ltd
Current assignee: Jilin Donghu Silicone Co ltd
Priority date: 2020-03-16
Filing date: 2020-03-16
Publication date: 2020-12-08
Anticipated expiration: 2030-03-16

Abstract

The utility model discloses a rotation type methyl phenyl silicon retort, include: the retort still includes: the reaction tank comprises a semicircular hollow shell, a plurality of hollow pipelines, a folded rotating frame, a driving device, a sealing cover, an arc-shaped heating plate, a feeding pipeline and a discharging pipeline, wherein the cross section of the reaction tank is circular, the semicircular hollow shell is positioned in the reaction tank, and the outer end face of the semicircular hollow shell is in lap joint with the inner wall of the reaction tank. This rotation type methyl phenyl silicon retort is one kind through peripheral rotatory, heats and stirs the reactant, makes its reaction good, is convenient for to the different positions sample, is convenient for carry out the device of clearance to the inner wall.

Description

Rotary methyl phenyl silicon reaction tank

Technical Field

The utility model relates to a retort field provides a rotation type methyl phenyl silicon retort very much.

Background

The reaction tank is a device for carrying a plurality of reactants and making the reactants react inside the reaction tank.

In order to make the reaction proceed well, it is necessary to mix the reactants uniformly, in order to promote the reaction, the interior of the reaction tank needs to be heated, the traditional heating position is fixed, the area is large, and therefore, the energy consumption is high, and the traditional heating and stirring are separated, so the structure is more complex, in order to monitor the reaction, the reactants on different positions need to be sampled and detected, conventionally, a tool is held to extend into different positions for sampling for many times, the sampling can not be carried out simultaneously, the time interval is provided, the sampling condition is different, if solid reactants are generated in the reaction and stick on the inner wall of the reaction tank, the solid reactants are conventionally cleaned manually, which is troublesome, therefore, in order to solve the above problems, it is necessary to design a reaction tank capable of rotating to heat and stir and simultaneously sampling at multiple positions.

SUMMERY OF THE UTILITY MODEL

In view of the above, in order to solve the above problems, the present invention is directed to a rotary methyl phenyl silicon reaction tank.

The utility model provides a technical scheme is: a retort that fully reacts, includes the retort, still including: the cross section of the reaction tank is circular, the semicircular hollow shell is positioned in the reaction tank, the outer end face of the semicircular hollow shell is lapped on the inner wall of the reaction tank, the arc heating plate is positioned on the upper surface of the reaction tank and used for shielding the upper part of the reaction tank, the lower end face of the folding rotary frame is fixedly connected at the center of the upper surface of the semicircular hollow shell, the upper end of the folding rotary frame penetrates through the center of the upper surface of the sealing cover, the folding rotary frame is internally of a hollow structure and communicated with the inside of the semicircular hollow shell, the hollow pipelines are positioned at the center of the inner side surface of the semicircular hollow shell and are uniformly communicated with the inside of the semicircular hollow shell, and a sealing bearing is arranged at the joint of the folding rotary frame and the sealing cover, the driving device is located on the upper surface of the sealing cover and used for driving the folded rotating frame to vertically rotate, the feeding pipeline is located at one end of the upper surface of the sealing cover, and the discharging pipeline is located on the side surface of the lower end of the reaction tank and used for overall drainage.

Preferably, the upper surface of the sealing cover is provided with a plurality of through holes, a plurality of multi-fork suction pipes are arranged in the through holes, the lower end face of each fork in each multi-fork suction pipe corresponds to the end face of the hollow pipeline one by one, each through hole is internally provided with a sealing ring for sealing the hollow pipeline end face and the sealing ring between the multi-fork suction pipes, the upper end of each fork in each multi-fork suction pipe is provided with a discharge pipeline, and each discharge pipeline is provided with a control valve.

Preferably, the end faces of the hollow pipelines are uniformly positioned on the same vertical line and coincide with the vertical central axis of the reaction tank.

Preferably, the upper end face of the folded rotating frame is sleeved with a shielding cover, and the shielding cover is in threaded connection with the folded rotating frame.

Further preferably, the length of the outer end surface of the semicircular hollow shell is longer than that of the inner end surface.

Further preferably, the lower end surface of the semicircular hollow shell is not overlapped with the inner lower surface of the reaction tank.

Further preferably, each discharge duct is located above the shutter cover.

The utility model provides a rotation type methyl phenyl silicon retort, one kind is rotatory through the periphery, heats and stirs the reactant, makes its reaction good, is convenient for to the different position samples, is convenient for carry out the device of clearance to the inner wall.

Drawings

The present invention will be described in further detail with reference to the accompanying drawings and embodiments:

FIG. 1 is a schematic structural diagram of a rotary methyl phenyl silicon reaction tank;

FIG. 2 is a front sectional view of the rotary methyl phenyl silicon reaction tank;

FIG. 3 is a top sectional view of the rotary methyl phenyl silicon reaction tank, the semicircular hollow shell, the hollow pipe and the arc-shaped heating plate;

FIG. 4 is a cross-sectional side view of the semi-circular hollow shell, the hollow tube, the folded turret, the arc-shaped heating plate, the multi-pronged suction tube and the shielding cover of the rotary type methyl phenyl silicon reaction tank;

FIG. 5 is a top view of the driving device, the sealing cap, the feeding pipe and the shielding cap of the rotary methyl phenyl silicon reaction tank;

FIG. 6 is a partially enlarged view of the sealing cap, the sealing ring, the discharge pipe, the control valve and the shielding cap of the rotary methyl phenyl silicon reaction tank;

FIG. 7 is a schematic diagram of the electrical circuit connections in a rotary methylphenylsilicon reactor vessel of the present invention;

in the figure: 1. a reaction tank; 2. a semi-circular hollow shell; 3. a hollow pipe; 4. a folding turret; 5. a drive device; 6. a sealing cover; 7. an arc-shaped heating plate; 8. a feed conduit; 9. a discharge pipeline; 10. a multi-pronged suction tube; 11. a seal ring; 12. a discharge conduit; 13. a control valve; 14. and (6) shielding the cover.

Detailed Description

The invention will be further explained below with reference to specific embodiments, without limiting the invention.

As shown in fig. 1-7, the utility model provides a reaction tank with sufficient reaction, which comprises a reaction tank 1 and also comprises: the reaction tank comprises a semicircular hollow shell 2, a plurality of hollow pipelines 3, a folding rotating frame 4, a driving device 5, a sealing cover 6, an arc-shaped heating plate 7, a feeding pipeline 8 and a discharging pipeline 9, wherein the cross section of the reaction tank 1 is circular, the semicircular hollow shell 2 is positioned in the reaction tank 1, the outer end surface of the semicircular hollow shell is lapped on the inner wall of the reaction tank 1, the arc-shaped heating plate 7 is positioned on the upper surface of the reaction tank 1 and used for shielding the upper part of the reaction tank, the lower end surface of the folding rotating frame 4 is fixedly connected to the center of the upper surface of the semicircular hollow shell 2, the upper end of the folding rotating frame passes through the center of the upper surface of the sealing cover 6, the folding rotating frame 4 is of a hollow structure and communicated with the inside of the semicircular hollow shell 2, the hollow pipelines 3 are positioned at the center of the inner side surface of the semicircular hollow shell 2, the connection part of the folded rotating frame 4 and the sealing cover 6 is provided with a sealing bearing, the driving device 5 is positioned on the upper surface of the sealing cover 6 and is used for driving the folded rotating frame 4 to vertically rotate, the feeding pipeline 8 is positioned at one end of the upper surface of the sealing cover 6, the discharging pipeline 9 is positioned on the side surface of the lower end of the reaction tank 1 and is used for overall drainage, when the device is used, raw materials of organic silicon required to be reacted are added into the reaction tank 1, when reaction is carried out, the reaction is carried out due to the fact that a plurality of raw materials react together, and therefore appropriate stirring needs to be carried out on the interior of the reaction tank 1, wherein the stirring operation is carried out, the driving device 5 is electrically connected with an external power supply, and after the external power supply is connected, the rotation work is carried out, and the driving end is used for driving the folded rotating frame 4 to, the folding rotating frame 4 is driven to rotate at the center of the reaction tank 1 and is fixedly connected with the semicircular hollow shell 2, so that the semicircular hollow shell 2 is driven to rotate circumferentially inside the reaction tank 1, the internal reaction raw materials are continuously stirred in the rotating process, and the reaction scabs on the inner wall of the reaction tank 1 are effectively scraped and cleaned, wherein the driving device 5 only plays a role in driving and rotating and comprises a rotating motor, a driving gear sleeved on the driving end of the rotating motor and a driven gear sleeved on the folding rotating frame 4 and meshed with the driving gear, the driving gear is driven by the rotating motor, the driving gear drives the driven gear through meshing to drive the folding rotating frame 4 for fixing the driven gear to rotate, and the sealing cover 6 on the upper surface of the reaction tank 1 is convenient to open and install, The reaction is good due to the feeding and the shielding of the upper part, the edge of the sealing cover 6 is preferably provided with a sealing strip, the sealing is better convenient, the inner part of the semicircular hollow shell 2 is of a hollow structure, the inner part of the folded rotating frame 4 is of a hollow structure and is communicated with the inner part of the semicircular hollow shell 2, the hot liquid capable of promoting the reaction is conveniently poured into the upper end of the folded rotating frame 4, the reaction is conveniently carried out at a certain temperature, the reaction is good, the plurality of hollow pipelines 3 which are positioned in the semicircular hollow shell 2 and are communicated with the inner part of the semicircular hollow shell 2 are convenient for pouring the hot liquid, the hollow pipelines extend into the reaction raw materials and are uniformly heated, and the plurality of hollow pipelines 3 extend into the inner part more and are more uniformly heated and can also be properly stirred when the semi-circular hollow shell is rotated along with the semi-circular shell, the reactants in the reactor are quickly and uniformly stirred and can be conveniently stirred when rotating, wherein the arc-shaped heating plate 7 positioned in the semicircular hollow shell 2 is convenient for heating the liquid in the reactor, preferably, the arc-shaped heating plate is a waterproof heating plate, wherein a power line can be selected and extended out from the upper end of the folded rotating frame 4, the power line is waterproof, the liquid in the reactor can be selected from insulating liquid and the like, according to the actual situation, if the arc-shaped heating plate 7 is selected and internally provided with a storage battery for supplying power, the insulating liquid is not needed, otherwise, the sealing protection is needed, the feeding pipeline 8 positioned at one end of the upper surface of the sealing cover 6 is good for feeding, the discharging pipeline 9 positioned on the side surface of the lower end of the reaction tank 1 is convenient for integrally discharging, wherein, a control valve is required to be installed on the feeding pipeline 8 and the discharging pipeline 9, the flow-in or flow-out is convenient to control, wherein a conical funnel and the like can be sleeved at the upper end of the feeding pipeline 8 for facilitating the feeding.

As an improvement of the technical solution, the upper surface of the sealing cover 6 is provided with a plurality of through holes, a plurality of forked suction pipes 10 are arranged in the plurality of through holes, the lower end surface of each fork in the forked suction pipes 10 respectively corresponds to the end surfaces of the plurality of hollow pipes 3 one by one, a sealing ring 11 for sealing between the multi-forked suction pipes 10 is arranged in each through hole, the upper end of each fork in the multi-forked suction pipes 10 is provided with a discharge pipe 12, each discharge pipe 12 is provided with a control valve 13, wherein in order to measure the reaction conditions at different heights, the multi-forked suction pipes 10 are manually pulled upwards, according to the condition shown in fig. 2, reactants at different positions are sucked in the plurality of pipes, then the pulling of the upper ends is stopped, the reactants at different positions can enter the upper ends of the multi-forked suction pipes 10, and some reactants can also enter in each discharge pipe 12, the control valve 13 on each discharge pipe 12 is then opened to discharge the sucked reactant, collected separately, and tested, wherein the multi-pronged suction pipe 10 is always placed at the other end inside the reaction tank 1 without affecting the rotation of the semicircular hollow shell 2, and wherein the control valve 13 is used only for controlling the outflow, including but not limited to a ball valve, etc.

As the improvement of the technical scheme, the end faces of the hollow pipelines 3 are uniformly positioned on the same vertical line and coincide with the vertical central axis of the reaction tank 1, and because each end face of the multi-fork suction pipe 10 is correspondingly arranged with the end face of the hollow pipeline 3, the end faces of the hollow pipelines 3 are positioned on the same vertical line, the hollow pipelines are convenient to face the central position and perform good sampling detection on different heights.

As an improvement of the technical scheme, the upper end face of the folded rotating frame 4 is sleeved with a shielding cover 14, the shielding cover 14 is in threaded connection with the folded rotating frame 4, wherein the upper end face of the folded rotating frame 4 needs to be fed with liquid, so that the upper end of the folded rotating frame is communicated, in order to ensure good sealing performance, the shielding cover 14 is sleeved on the folded rotating frame 4, the shielding cover 14 is connected with the upper end of the folded rotating frame 4 through threads and is convenient to seal through screwing, wherein the threaded connection is realized by processing internal threads on the inner side surface of the shielding cover 14, and processing external threads matched with the internal threads on the outer side surface of the upper end of the folded rotating frame 4, so that the sealing performance is good through screwing.

As an improvement of the technical scheme, the length of the outer end surface of the semicircular hollow shell 2 is longer than that of the inner end surface, and because the length of the outer end surface of the semicircular hollow shell 2 is longer than that of the inner end surface, as shown in fig. 3, the semicircular hollow shell forms an inclined angle, so that the inner wall surface of the reaction tank 1 can be scraped well, and the cleaning is convenient.

As the improvement of the technical proposal, the lower end surface of the semicircular hollow shell 2 is not overlapped with the inner lower surface of the reaction tank 1, and the lower end of the semicircular hollow shell 2 is not overlapped with the inner lower surface of the reaction tank 1, so that a settling space is formed and the drainage of the lower end is convenient.

As an improvement of the technical scheme, each discharge pipeline 12 is positioned above the shielding cover 6, so that the discharge operation is convenient to carry out at the upper end, the internal reaction is not influenced, and the sampling is convenient.

In order to facilitate the discharge of the waste water, a support frame is sleeved at the lower end of the outer side of the reaction tank 1, and the reaction tank 1 is suspended in the air, so that the discharge pipeline 9 can be conveniently discharged downwards;

in order to facilitate the feeding of the feeding pipeline 8, a conical hopper or a pipeline connector can be sleeved on the feeding pipeline, so as to facilitate the connection with an external pipeline and facilitate the feeding;

all the cover is equipped with the heating circle in 3 outer ends of every hollow pipeline, is convenient for when rotating, heats, carries out good heating to inside reactant, because quantity is more, consequently heats evenly fast, because hollow pipeline 3 and semi-circular hollow shell 2 between have certain distance, the temperature reduces in the transmission easily, influence reaction goes on, wherein the heating circle is only used for heating, including but not limited to heating plate etc..

The embodiments of the present invention are written in a progressive manner, emphasizing the differences of the various embodiments, and similar parts can be referred to each other.

The embodiments of the present invention have been described in detail with reference to the drawings, but the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art.

Claims

1. The utility model provides a rotation type methyl phenyl silicon retort, includes retort (1), its characterized in that still including: the reaction tank comprises a semicircular hollow shell (2), a plurality of hollow pipelines (3), a folding rotating frame (4), a driving device (5), a sealing cover (6), an arc-shaped heating plate (7), a feeding pipeline (8) and a discharging pipeline (9), wherein the cross section of the reaction tank (1) is circular, the semicircular hollow shell (2) is positioned in the reaction tank (1), the outer end surface of the semicircular hollow shell is lapped on the inner wall of the reaction tank (1), the sealing cover (6) of the arc-shaped heating plate (7) is positioned on the upper surface of the reaction tank (1) and used for shielding the upper part of the reaction tank, the lower end surface of the folding rotating frame (4) is fixedly connected at the center of the upper surface of the semicircular hollow shell (2), the upper end of the folding rotating frame passes through the center of the upper surface of the sealing cover (6), the folding rotating frame (4) is of a hollow structure and is communicated with the interior, the novel reactor is characterized in that the hollow pipelines (3) are located at the center of the inner side surface of the semicircular hollow shell (2) and are uniform, the semicircular hollow shell (2) is communicated with the inside of the semicircular hollow shell, a sealing bearing is arranged at the joint of the folding rotating frame (4) and the sealing cover (6), the driving device (5) is located on the upper surface of the sealing cover (6) and is used for driving the folding rotating frame (4) to vertically rotate, the feeding pipeline (8) is located at one end of the upper surface of the sealing cover (6), and the discharging pipeline (9) is located on the side surface of the lower end of the reactor (1) and is used for overall drainage.

2. The rotary methyl phenyl silicon reaction tank as claimed in claim 1, wherein the upper surface of the sealing cover (6) is provided with a plurality of through holes, a multi-fork suction pipe (10) is arranged in the plurality of through holes, the lower end surface of each fork in the multi-fork suction pipe (10) is respectively corresponding to the end surfaces of the plurality of hollow pipelines (3), a sealing ring (11) used for sealing the multi-fork suction pipe (10) is arranged in each through hole, the upper end of each fork in the multi-fork suction pipe (10) is provided with a discharge pipeline (12), and each discharge pipeline (12) is provided with a control valve (13).

3. A rotary methylphenylsilicon reactor according to claim 2, wherein the end surfaces of the hollow pipes (3) are uniformly located on the same vertical line and coincide with the vertical central axis of the reactor (1).

4. The rotary methyl phenyl silicon reaction tank as claimed in claim 1, wherein a shielding cover (14) is sleeved on the upper end face of the folded rotating frame (4), and the shielding cover (14) is in threaded connection with the folded rotating frame (4).

5. A rotary methylphenylsilicon reaction tank according to claim 1, wherein the semi-circular hollow shell (2) has an outer end surface longer than an inner end surface.

6. A rotary methylphenylsilicon reaction tank according to claim 1, characterized in that the lower end surface of the semi-circular hollow shell (2) is not overlapped with the inner lower surface of the reaction tank (1).

7. A rotary methylphenylsilicon reaction tank according to claim 2 wherein each discharge conduit (12) is located above the sealing lid (6).