CN211753704U - Large-air-volume medium-concentration ethyl acetate recovery device - Google Patents
Large-air-volume medium-concentration ethyl acetate recovery device Download PDFInfo
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- CN211753704U CN211753704U CN201922304471.2U CN201922304471U CN211753704U CN 211753704 U CN211753704 U CN 211753704U CN 201922304471 U CN201922304471 U CN 201922304471U CN 211753704 U CN211753704 U CN 211753704U
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- Prior art keywords
- molecular sieve
- ethyl acetate
- rotating wheel
- sieve tank
- desorption
- Prior art date
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- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 title claims abstract description 72
- 238000011084 recovery Methods 0.000 title claims abstract description 14
- 239000002808 molecular sieve Substances 0.000 claims abstract description 63
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 63
- 238000003795 desorption Methods 0.000 claims abstract description 23
- 239000007789 gas Substances 0.000 claims abstract description 20
- 239000002912 waste gas Substances 0.000 claims abstract description 20
- 238000001179 sorption measurement Methods 0.000 claims description 23
- 239000002904 solvent Substances 0.000 claims description 6
- 230000008929 regeneration Effects 0.000 abstract description 12
- 238000011069 regeneration method Methods 0.000 abstract description 12
- 238000000034 method Methods 0.000 abstract description 11
- 238000009833 condensation Methods 0.000 abstract description 6
- 230000005494 condensation Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000002131 composite material Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 239000002894 chemical waste Substances 0.000 description 1
- 239000000112 cooling gas Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000010815 organic waste Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
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- Treating Waste Gases (AREA)
Abstract
The utility model provides a big amount of wind medium concentration ethyl acetate recovery unit, carries out the second grade runner through carrying out big amount of wind medium concentration ethyl acetate and adsorbs, has guaranteed the discharge to reach standard of tail gas, carries out thermal desorption to the ethyl acetate that the runner adsorbed down simultaneously, accomplishes the circulation regeneration of runner. And the ethyl acetate brought out by the hot air of the primary runner enters a molecular sieve after heat exchange to complete the desorption of the moisture. The high-concentration low-moisture ethyl acetate gas is recovered by low-temperature condensation. The cryogenically cooled gas with low concentration and low moisture exchanges heat with hot airflow regenerated by the front-stage runner, and is heated by the heater to regenerate the molecular sieve. And (4) after the molecular sieve is regenerated, gas enters an inlet of the system for circular treatment. The secondary runner regeneration gas is also mixed with the molecular sieve regeneration gas and returned to the inlet, so that the load of the deep cooler is effectively reduced. The process has the advantages of high waste gas treatment efficiency up to more than 99%, stable condensation and recovery effect, relatively mild working conditions, high safety, no secondary pollution, purer recovered ethyl acetate and direct application in production.
Description
Technical Field
The utility model relates to a big amount of wind medium concentration ethyl acetate recovery unit belongs to organic waste gas's recovery processing field.
Background
The research and development processes of semiconductors and new materials are more and more, and the industrialization is continuously developed. The new material industry is basically formed in large scale and gathering development situation in 2020, the technical equipment restriction in the fields of metal materials, composite materials, advanced semiconductor materials and the like is broken through, and the industrialization and the application of more than 70 key new materials are realized in the fields of carbon fiber composite materials and the like. The ethyl acetate is used as a good solvent of the binding material, and the problem of waste gas treatment in the using process becomes more prominent.
Patent 201710424442.2 discloses an adsorption filtration method for treating ethyl acetate in chemical waste gas, wherein the residence time of the process is 1-2min, the air flow velocity is very low in an adsorption tower with a height of 0.9m, the treatment efficiency for ethyl acetate with large air volume is very low, the method combines the microbial decomposition, and the process regulation and control for the adsorption tower are relatively strict. The emission of ethyl acetate with medium concentration is difficult to reach the standard.
Patent 201820722586.6 adopts condensation to combine the adsorption equipment of active carbon, and the load that the device needs to the ethyl acetate waste gas of low concentration is higher, and the adsorption equipment after the condensation does not have corresponding regeneration system, can bring the useless problem of danger.
When the secondary rotating wheel is adsorbed to meet the standard emission of waste gas, the problem of low-temperature condensation and frosting is effectively solved by adding the molecular sieve dehydration system, and the influence of the external air intake of the system on the system load is effectively reduced by adopting the deep cooling gas as the renewable gas source of the molecular sieve. The secondary runner regenerated gas has low concentration and directly enters the air inlet system, so that the load of the cryogenic system is effectively reduced.
Disclosure of Invention
The purpose provides an adopt the device that second grade runner absorption combines the low temperature condensation to retrieve in order to overcome prior art not enough, and this scheme simple structure can satisfy the discharge to reach standard of waste gas, guarantees the effective recovery of solvent simultaneously.
Aiming at the technical difficulties, the device mainly solves the problems from the following technical methods:
the large-air-volume medium-concentration ethyl acetate recovery device comprises a primary rotating wheel and a secondary rotating wheel, wherein the primary rotating wheel is connected with the secondary rotating wheel, a primary rotating wheel heater and a secondary rotating wheel heater are respectively arranged on the outer sides of the primary rotating wheel and are respectively connected with a precooler, waste gas is introduced into the primary rotating wheel by a main fan, the other ends of the primary rotating wheel and the secondary rotating wheel heater are connected with a heat exchanger, the heat exchanger is connected with a molecular sieve tank A and a molecular sieve tank B through an air inlet pipeline, an adsorption air inlet valve A and an adsorption air inlet valve B for controlling flow are arranged on the air inlet pipeline, exhaust pipelines are respectively arranged at the bottoms of the molecular sieve tank A and the molecular sieve tank B and are connected with a deep cooler, one end of the deep cooler is connected with the heat exchanger for further heat exchange, the other end of the deep cooler is connected with a solvent tank for storage, and an adsorption exhaust valve A and an adsorption exhaust valve B for controlling flow are .
Preferably, the method comprises the following steps: the heat exchanger is connected to a molecular sieve heater, the molecular sieve heater is connected to a desorption exhaust pipe, a molecular sieve tank A desorption exhaust valve and a molecular sieve tank B desorption exhaust valve which are used for indicating a molecular sieve tank B to a molecular sieve tank A on two sides and a molecular sieve tank A top which are used for indicating the molecular sieve tank B are respectively arranged on the desorption exhaust pipe, and a molecular sieve tank A desorption air inlet valve and a molecular sieve tank B desorption air inlet valve are also arranged on the molecular sieve tank A and the molecular sieve tank A top.
Preferably, the method comprises the following steps: one end of the secondary rotating wheel is connected to an external discharge port, and the other end of the secondary rotating wheel is connected to an exhaust gas inlet through a pipeline to further treat exhaust gas.
The invention has the characteristics of simple structure, convenient operation, good adsorption effect and the like.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Detailed Description
The invention will now be described in detail with reference to the accompanying drawings, in which: as shown in figure 1, the large-air-volume medium-concentration ethyl acetate recovery device comprises a primary rotating wheel 3 and a secondary rotating wheel 4, wherein the primary rotating wheel 3 and the secondary rotating wheel 4 are connected with each other, a primary rotating wheel heater 5 and a secondary rotating wheel heater 6 are respectively arranged on the outer sides of the primary rotating wheel 3, one end of the primary rotating wheel 3 is connected with a precooler 1, the precooler 1 transfers waste gas into the primary rotating wheel 3 by a main fan 2, the other end of the precooler 1 is connected with a heat exchanger 7, the heat exchanger 7 is connected with a molecular sieve tank A8 and a molecular sieve tank B9 through air inlet pipelines, an adsorption air inlet valve A13 and an adsorption air inlet valve B7 for controlling flow are arranged on the air inlet pipelines, the bottoms of the molecular sieve tank A8 and the molecular sieve tank B9 are respectively provided with exhaust pipelines, the exhaust pipelines are connected to a deep cooler 10, one end of the deep cooler 10 is connected to the heat exchanger for, and the exhaust pipeline is also provided with a molecular sieve tank A adsorption exhaust valve 17 and a molecular sieve tank B adsorption exhaust valve 18 for controlling flow.
Preferably, the method comprises the following steps: the heat exchanger 7 is connected to a molecular sieve heater 12, the molecular sieve heater 12 is connected to a desorption exhaust pipe, a molecular sieve tank A desorption exhaust valve 16 and a molecular sieve tank B desorption exhaust valve 20 which are used for exhausting molecular sieve tanks A8 and B9 on two sides and respectively arranged on the desorption exhaust pipe, and a molecular sieve tank A desorption air inlet valve 15 and a molecular sieve tank B desorption air inlet valve 19 are further arranged at the tops of the molecular sieve tank A8 and the molecular sieve tank A which is used for indicating the molecular sieve tank B9. One end of the secondary runner 4 is connected to an external discharge port, and the other end thereof is connected to an exhaust gas inlet through a pipeline for further processing exhaust gas.
The device comprises the following concrete implementation method:
the ethyl acetate recovery device of the invention comprises: the system comprises a precooler, a main fan, a primary rotating wheel, a secondary rotating wheel, a primary rotating wheel heater, a secondary rotating wheel heater, a heat exchanger, a molecular sieve tank A, a molecular sieve tank B, a deep cooler, a solvent tank and a molecular sieve heater.
Precooling ethyl acetate: mixing the waste gas with medium concentration from the workshop with the molecular sieve regeneration waste gas and the secondary runner regeneration waste gas, and cooling to 30-40 ℃ through heat exchange of a precooler;
secondary adsorption of the rotating wheel: the cooled waste gas enters a treatment area of a 3-stage rotating wheel, enters a treatment area of a 4-stage rotating wheel after primary adsorption, and is discharged after adsorption is completed;
regeneration of the runner: the system air inlet is processed through reposition of redundant personnel, and an air current is used for the regeneration of runner, and the regeneration gas carries out the primary heating of regeneration gas through runner desorption district, accomplishes the cooling of runner simultaneously. Heating the once heated regeneration waste gas to 180-;
molecular sieve dehydration of the waste gas: the high-concentration waste gas regenerated by the primary runner is reduced to the optimal temperature of 10-20 ℃ adsorbed by the molecular sieve adsorber through the heat exchanger, and the water content of the waste gas is very low after the waste gas is adsorbed by the bed layer;
condensing and recycling waste gas: the water content of the waste gas after being adsorbed by the molecular sieve is extremely low, and ethyl acetate in the waste gas is subjected to phase change after being condensed by a deep freezer to obtain an ethyl acetate solvent.
Regeneration of the molecular sieve: after the gas which is not condensed by the deep cooler is heated by the heat exchanger for one time, the temperature is raised by the molecular sieve heater to reach the specified desorption temperature, the molecular sieve bed layer is reversely blown, and the adsorbed water is desorbed. The regenerated water is cooled and condensed by a precooler and then discharged out of the system, and then the drying adsorption tank is used for circularly absorbing the water. And meanwhile, the normal operation of the adsorption and desorption system is ensured by switching the 9 molecular sieve tank B.
Claims (3)
1. A large-air-volume medium-concentration ethyl acetate recovery device comprises a primary rotating wheel (3) and a secondary rotating wheel (4), wherein the primary rotating wheel (3) and the secondary rotating wheel (4) are connected with each other, and a primary rotating wheel heater (5) and a secondary rotating wheel heater (6) are respectively arranged on the outer sides of the primary rotating wheel and the secondary rotating wheel, the large-air-volume medium-concentration ethyl acetate recovery device is characterized in that one end of the primary rotating wheel (3) is connected with a precooler (1), waste gas is introduced into the primary rotating wheel (3) by a main fan (2) in the precooler (1), the other end of the primary rotating wheel is connected with a heat exchanger (7), the heat exchanger (7) is connected with a molecular sieve tank A (8) and a molecular sieve tank B (9) through an air inlet pipeline, an adsorption air inlet valve A (13) and an adsorption air inlet valve B (17) for controlling flow are arranged on the air inlet pipeline, the discharge pipeline is connected to a deep cooler (10), one end of the deep cooler (10) is connected to a heat exchanger (7) for further heat exchange, the other end of the deep cooler is connected with a solvent tank (11) for storage, and a molecular sieve tank A adsorption exhaust valve (14) and a molecular sieve tank B adsorption exhaust valve (18) for controlling flow are further arranged on the exhaust pipeline.
2. The large-air-volume medium-concentration ethyl acetate recovery device according to claim 1, wherein the heat exchanger (7) is connected to a molecular sieve heater (12), the molecular sieve heater (12) is connected to a desorption exhaust pipe, a molecular sieve tank A desorption exhaust valve (16) and a molecular sieve tank B desorption exhaust valve (20) which are used for exhausting molecular sieve tank A (8) and molecular sieve tank B (9) to two sides are respectively arranged on the desorption exhaust pipe, a pipeline connected to an exhaust gas inlet is further arranged at the top of the molecular sieve tank A (8) and the molecular sieve tank A which is used for indicating the molecular sieve tank B (9), and a sieve tank A desorption intake valve (15) and a molecular sieve tank B desorption intake valve (19) are respectively arranged on the molecular pipeline.
3. A high air flow medium concentration ethyl acetate recovery device according to claim 1, characterised in that one end of the secondary rotor (4) is connected to an external discharge port and the other end is connected to an exhaust gas inlet via a pipe for further treatment of the exhaust gas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922304471.2U CN211753704U (en) | 2019-12-20 | 2019-12-20 | Large-air-volume medium-concentration ethyl acetate recovery device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922304471.2U CN211753704U (en) | 2019-12-20 | 2019-12-20 | Large-air-volume medium-concentration ethyl acetate recovery device |
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| Publication Number | Publication Date |
|---|---|
| CN211753704U true CN211753704U (en) | 2020-10-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201922304471.2U Active CN211753704U (en) | 2019-12-20 | 2019-12-20 | Large-air-volume medium-concentration ethyl acetate recovery device |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110975522A (en) * | 2019-12-20 | 2020-04-10 | 杭州捷瑞空气处理设备有限公司 | Large-air-volume medium-concentration ethyl acetate recovery device and recovery method thereof |
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2019
- 2019-12-20 CN CN201922304471.2U patent/CN211753704U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110975522A (en) * | 2019-12-20 | 2020-04-10 | 杭州捷瑞空气处理设备有限公司 | Large-air-volume medium-concentration ethyl acetate recovery device and recovery method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 311305 No. 2088, Keji Avenue, Qingshan Industrial Zone, Lin'an City, Hangzhou City, Zhejiang Province Patentee after: Hangzhou Jierui Intelligent Equipment Co.,Ltd. Address before: 311305 No. 2088, Keji Avenue, Qingshan Industrial Zone, Lin'an City, Hangzhou City, Zhejiang Province Patentee before: HANGZHOU DRY AIR TREATMENT EQUIPMENT Co.,Ltd. |
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| CP01 | Change in the name or title of a patent holder |