CN211677593U - Thiourea dioxide continuous dissolving device - Google Patents
Thiourea dioxide continuous dissolving device Download PDFInfo
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- CN211677593U CN211677593U CN201922458204.0U CN201922458204U CN211677593U CN 211677593 U CN211677593 U CN 211677593U CN 201922458204 U CN201922458204 U CN 201922458204U CN 211677593 U CN211677593 U CN 211677593U
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Abstract
The utility model belongs to the technical field of thiourea dioxide, concretely relates to thiourea dioxide continuous dissolving device. The thiourea dioxide continuous dissolving device comprises a feeding device, a dissolving device and a storage and distribution device; the feeding device is arranged above the dissolving device and comprises a material storage box for storing thiourea dioxide and a conveyor for conveying the thiourea dioxide; the dissolving device comprises a dissolving tank and a stirrer, wherein a stirring head of the stirrer extends into the dissolving tank, the dissolving tank is communicated with an alkali conveying pipeline and a water conveying pipeline, and the bottom of the dissolving tank is connected with a first material output pipeline; the storage and distribution device comprises a storage box, the tail end of the first material output pipeline is connected with an inlet of the storage box, and an outlet of the storage box is connected with a second material output pipeline. The utility model provides a thiourea dioxide solubility low, be heated easily when adding and wet the decomposition, block up the difficulty that corrodes the pipeline equipment, be difficult to add in succession.
Description
Technical Field
The utility model belongs to the technical field of thiourea dioxide, concretely relates to thiourea dioxide continuous dissolving device.
Background
Thiourea dioxide (CH)4N2O2S) is a substitute product of sodium hydrosulfite, has the characteristics of strong reducibility, good thermal stability, convenient storage and transportation and the like, and can be used as a reducing agent, a bleaching decolorizer, a plastic stabilizer, an organic solventThe synthetic antioxidant, the sensitizer of photosensitive materials and the like are widely applied in the industries of printing and dyeing, papermaking and the like, and have no hidden pollution trouble in the using process.
However, thiourea dioxide has low solubility, and is easily decomposed by heat, moisture and oxygen, and thus continuous addition is not easy to achieve.
In view of the above, it is important to design a continuous dissolving apparatus and process for thiourea dioxide.
SUMMERY OF THE UTILITY MODEL
In order to overcome the problems in the prior art, the utility model provides a thiourea dioxide continuous dissolving device and process. The dissolving device solves the problems that thiourea dioxide has low solubility, is easy to be heated, moistened and decomposed during adding, blocks and corrodes pipeline equipment and is difficult to be continuously added.
The utility model also provides an adopt above-mentioned device to dissolve thiourea dioxide technology.
In order to achieve the above purpose, the technical scheme of the utility model is as follows:
a thiourea dioxide continuous dissolving device comprises a feeding device, a dissolving device and a storage and distribution device;
the feeding device is arranged above the dissolving device and comprises a material storage box for storing thiourea dioxide and a conveyor for conveying the thiourea dioxide;
the dissolving device comprises a dissolving tank and a stirrer, wherein a stirring head of the stirrer extends into the dissolving tank, the dissolving tank is communicated with an alkali conveying pipeline and a water conveying pipeline, and the bottom of the dissolving tank is connected with a first material output pipeline;
the storage and distribution device comprises a storage box, the tail end of the first material output pipeline is connected with an inlet of the storage box, and an outlet of the storage box is connected with a second material output pipeline.
Preferably, the tail end of the second material output pipeline is provided with a plurality of branches, one branch is communicated with the dissolving tank through a return pipeline, and the rest branches are used for outputting products; the return line can prevent the valve or the pipeline from leaking due to overlarge pressure, and the return line flows back when the pressure of the conveying line exceeds a certain pressure.
Preferably, the vibrator is arranged on the outer wall of the storage box, and a material level meter is arranged in the storage box; the vibrator prevents thiourea dioxide from being too poor in damp fluidity, the storage box cannot be fed or materials are stored on the wall of the storage box, and the material level meter can prevent the material shortage in the storage box.
Preferably, a liquid level meter is arranged in the dissolving tank; preventing the liquid level in the dissolving tank from being too low and too high.
Preferably, the conveyor is a screw conveyor, and a shell of the screw conveyor is connected with a dry air conveying pipeline; the dry air can be introduced into the machine shell to prevent the thiourea dioxide from being accumulated and decomposed by moisture.
Preferably, the storage and distribution device further comprises a distributor, the tail end of the second material output pipeline is connected with an inlet of the distributor, the distributor is provided with four outlets, one outlet is communicated with the dissolving tank through a return pipeline, and the other three outlets are respectively connected with the first branch, the second branch and the third branch; the first branch and the third branch can distribute the thiourea dioxide solution to various flow lines according to actual production needs.
Preferably, the first material output pipeline is connected with a cleaning pipeline; the cleaning pipeline can clean the dissolving tank by introducing cleaning water after the dissolving is finished.
Preferably, the alkali conveying pipeline, the water conveying pipeline, the first branch, the second branch and the third branch are provided with first valves; a delivery pump is arranged on the second material output pipeline; and second valves are arranged on the first material output pipeline and the cleaning pipeline.
Preferably, the device of the utility model also comprises an automatic control system, the automatic control system is electrically connected with the conveyer, the stirrer, the vibrator, the charge level indicator, the liquid level meter, the first valve and the delivery pump.
Specifically, the first valve is a flow valve.
Preferably, the length-diameter ratio of the screw conveyer is not more than 5: 1; the screw and the shell are made of 316L, Teflon or nylon; prevent the thiourea dioxide from being wetted and decomposed into methyl ether sulfinic acid to corrode.
Preferably, the dry air conveying pipeline is filled with dry air with the dew point less than or equal to 10 ℃.
A dissolving process using the dissolving device, when alkali is not added, the maximum adding amount of thiourea dioxide is 2 percent of the adding amount of water; when the addition of alkali is required, the maximum addition amount of thiourea dioxide is 2 times of the addition amount of alkali. For example: when the amount of the added alkali is 2% of the added amount of water, the maximum added amount of thiourea dioxide is 4% of the added amount of water.
In the utility model, in order to prevent thiourea dioxide from being affected with damp, closed box bodies are adopted, namely the storage box, the dissolving box and the storage box are closed, and at the moment, a material level indicator in the storage box passes through the top cover of the storage box and enters the storage box; the liquid level meter in the dissolving tank, the alkali and water conveying pipelines communicated with the dissolving tank, the shaft of the stirrer, the material outlet of the conveyor and the like all penetrate through the top cover of the tank body to enter the dissolving tank.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the device of the utility model adopts the design of a closed box body and dry air, and the like, thereby solving the difficulties that thiourea dioxide has low solubility, is easy to be heated, moistened and decomposed during adding, blocks up and corrodes pipeline equipment and is difficult to be added continuously;
2. the device of the utility model is simple, and the vibrator, the charge level indicator and the liquid level indicator are controlled by the automatic control system, so that the real-time monitoring and adjustment of the actual situation can be realized;
3. the length-diameter ratio of a screw of the screw conveyer is not more than 5: 1; the screw and the shell are made of 316L, Teflon or nylon, and dry air with the dew point less than or equal to 10 ℃ is introduced into the dry air conveying pipeline, so that thiourea dioxide can be prevented from being damped and decomposed into methyl ether sulfinic acid;
4. the spiral conveyer can better uniformly convey thiourea dioxide from the storage box, and has the functions of sealing, homogenizing and stirring.
Drawings
FIG. 1 is a schematic structural view of a thiourea dioxide continuous dissolving device according to the present invention;
in the figure: the device comprises a dissolving tank 1, a storage tank 2, a stirrer 3, a storage tank 4, a screw conveyer 5, a motor 6, a distributor 7, a vibrator 8, a liquid level meter 9, an alkali conveying pipeline 10, a water conveying pipeline 11, a level meter 12, a first material output pipeline 13, a cleaning pipeline 14, a first branch 15, a second branch 16, a third branch 17, a return pipeline 18, a conveying pump 19, a dry air conveying pipeline 20, a flow valve 21, a second valve 22 and a second material output pipeline 23.
Detailed Description
The present invention will be further described with reference to the following examples and drawings, but the present invention is not limited thereto.
In the description of the present invention, it should be noted that, for the orientation words, such as the terms "upper", "lower", "left", "right", "top", "bottom", etc., indicating the orientation and the positional relationship based on the orientation or the positional relationship shown in the drawings is only for convenience of description and simplification of the description, but not for indicating or implying that the indicated device or element must have a specific orientation, be constructed and operated in a specific orientation, and should not be interpreted as limiting the specific scope of the present invention.
It is noted that the terms first, second, third and the like in the description and in the claims of the present application are used for distinguishing between similar elements and not necessarily for describing a particular sequential or chronological order. It should be understood that the data so used may be interchanged under appropriate circumstances such that embodiments of the application described herein may be used. Furthermore, the terms "comprising" and "having," as well as any variations thereof, are intended to cover non-exclusive inclusions.
Example 1
As shown in fig. 1, the thiourea dioxide continuous dissolving device of the present invention comprises a feeding device, a dissolving device and a storage and distribution device; the feeding device is arranged above the dissolving device and comprises a material storage box 4 for storing thiourea dioxide and a spiral conveyor 5 for conveying the thiourea dioxide; the dissolving device comprises a dissolving tank 1 and a stirrer 3, a stirring head of the stirrer 3 extends into the dissolving tank 1, the dissolving tank 1 is communicated with an alkali conveying pipeline 10 and a water conveying pipeline 11, and the bottom of the dissolving tank 1 is connected with a first material output pipeline 13; the storage and distribution device comprises a storage box 2 and a distributor 7, the tail end of a first material output pipeline 13 is connected with an inlet of the storage box 2, an outlet of the storage box 2 is connected with a second material output pipeline 23, the tail end of the second material output pipeline 23 is connected with an inlet of the distributor 7, the distributor 7 is provided with four outlets, one of the four outlets is communicated with the dissolving box 1 through a return pipeline 18, and the other three outlets are respectively connected with a first branch 15, a second branch 16 and a third branch 17; the first material output pipeline 13 is connected with a cleaning pipeline 14.
Specifically, the storage tank 4 stores solid thiourea dioxide; the storage tank 2 stores the thiourea dioxide solution dissolved by the dissolving tank 1.
The vibrator 8 is arranged on the outer wall of the storage box 4, and a material level meter 12 is arranged in the storage box 4; a liquid level meter 9 is arranged in the dissolving tank 1.
A dry air conveying pipeline 20 is connected to the shell of the screw conveyor 5, and a motor 6 is arranged on the right side of the screw conveyor 5; the length-diameter ratio of a screw of the screw conveyer 5 is not more than 5: 1; the screw and the shell are made of 316L, Teflon or nylon. The dry air conveying pipeline is filled with dry air with the dew point less than or equal to 10 ℃.
The alkali conveying pipeline 10, the water conveying pipeline 11, the first branch 15, the second branch 16 and the third branch 17 are provided with flow valves 21; a delivery pump 19 is arranged on the second material output pipeline 23; the first material output pipeline 13 and the cleaning pipeline 14 are provided with a second valve 22.
The device of the utility model also comprises a PLC control system which is electrically connected with the screw conveyer 5, the stirrer 3, the vibrator 8, the charge level indicator 12, the liquid level indicator 9, the flow valve 21 and the delivery pump 19; the PLC control system and how to electrically connect with other components may be controlled by conventional techniques in the art, and will not be described herein again. Specifically, the power of the delivery pump 19 is adjusted according to the flow of the loop pipeline, and the power of the delivery pump 19 is automatically reduced when the flow is large; adjusting the speed of adding water, alkali and thiourea dioxide according to the liquid level of the dissolving tank 1; and determining the charging time according to the level of the material storage box 2.
A dissolving process using the dissolving device, when alkali is not added, the maximum adding amount of thiourea dioxide is 2 percent of the adding amount of water; when the amount of the added alkali is 2% of the added amount of water, the maximum added amount of thiourea dioxide is 4% of the added amount of water.
Whether or not to add alkali and the amount of alkali to be added depend on the subsequent process (subsequent process using thiourea dioxide solution). When the terylene needs to be cleaned, alkali is needed to be added (the adding amount can be 2 percent of the water amount); when the non-alkali-resistant wool blended fabric is cleaned, alkali can be not added or less added.
The dissolving process of the thiourea dioxide of the utility model is simply introduced as follows:
when in use, the flow valves 21, the screw conveyer 5 and the vibrator 8 on the alkali conveying pipeline 10 and the water conveying pipeline 11 are firstly opened, and the conveying pump 19 and the stirrer 3 are started; send into solid thiourea dioxide and dissolve in dissolving case 1, then stir a certain time and make it dissolve the back, send thiourea dioxide solution to bin 2 buffering through first material output pipeline 13, partly thiourea dioxide solution is sent into through return line 18 and is dissolved case 1 and not only can continue to participate in dissolving, also can prevent that pipeline pressure is too big, and the production line is carried as the product to the surplus. When the level gauge 12 detects a low level, the system gives an alarm to prompt for charging. When the work is stopped, dry air is introduced into the screw conveyor 5 through the dry air conveying pipeline 20, so that thiourea dioxide in the screw conveyor is prevented from being damped.
The dissolving tank 1 sufficiently stirs the material introduced into the dissolving tank 1 by the stirrer 3 to disperse and dissolve the material. When the level gauge 9 detects a high level, the operation is stopped.
After the dissolving process is finished, cleaning water (cleaning agent can be added) is introduced into the dissolving tank 1 through the cleaning pipeline 14, then a second valve on the cleaning pipeline 14 is closed, a second valve on the material conveying pipeline 13 is opened, and the dissolving tank 1, the storage tank 2, the conveying pump 19, the distributor 7, the first branch, the third branch and the return pipeline 18 are cleaned; after the cleaning is finished, the second valve on the material conveying pipeline 13 is closed, the second valve on the cleaning pipeline 14 is opened, and the waste liquid after the cleaning is discharged.
Claims (8)
1. A thiourea dioxide continuous dissolving device is characterized by comprising a feeding device, a dissolving device and a storage and distribution device;
the feeding device is arranged above the dissolving device and comprises a material storage box for storing thiourea dioxide and a conveyor for conveying the thiourea dioxide;
the dissolving device comprises a dissolving tank and a stirrer, wherein a stirring head of the stirrer extends into the dissolving tank, the dissolving tank is communicated with an alkali conveying pipeline and a water conveying pipeline, and the bottom of the dissolving tank is connected with a first material output pipeline;
the storage and distribution device comprises a storage box, the tail end of the first material output pipeline is connected with an inlet of the storage box, and an outlet of the storage box is connected with a second material output pipeline.
2. The thiourea dioxide continuous dissolving apparatus of claim 1, wherein the second material output pipeline is provided with a plurality of branches at the end, one branch is communicated with the dissolving tank through the return pipeline, and the rest branches are used for product output.
3. The thiourea dioxide continuous dissolving apparatus of claim 1, wherein the vibrator is disposed on the outer wall of the storage tank, and a level gauge is disposed in the storage tank; and a liquid level meter is arranged in the dissolving tank.
4. The thiourea dioxide continuous dissolving apparatus of claim 1, wherein the conveyor is a screw conveyor, and a dry air conveying pipeline is connected to a casing of the screw conveyor.
5. The thiourea dioxide continuous dissolving apparatus of claim 1, wherein the storage and distribution means further comprises a distributor, the end of the second material output line is connected to an inlet of the distributor, the distributor has four outlets, one outlet is connected to the dissolving tank through a return line, and the other three outlets are connected to the first branch, the second branch and the third branch, respectively.
6. The thiourea dioxide continuous dissolving apparatus of claim 5, wherein the first material output line is connected with a cleaning line.
7. The thiourea dioxide continuous dissolving apparatus of claim 6, wherein the alkali conveying pipeline, the water conveying pipeline, the first branch, the second branch and the third branch are provided with a first valve; a delivery pump is arranged on the second material output pipeline; and second valves are arranged on the first material output pipeline and the cleaning pipeline.
8. The thiourea dioxide continuous dissolving apparatus of claim 4, wherein the screw length-diameter ratio of the screw conveyer is not more than 5: 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922458204.0U CN211677593U (en) | 2019-12-31 | 2019-12-31 | Thiourea dioxide continuous dissolving device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922458204.0U CN211677593U (en) | 2019-12-31 | 2019-12-31 | Thiourea dioxide continuous dissolving device |
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| CN211677593U true CN211677593U (en) | 2020-10-16 |
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| CN201922458204.0U Active CN211677593U (en) | 2019-12-31 | 2019-12-31 | Thiourea dioxide continuous dissolving device |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110935391A (en) * | 2019-12-31 | 2020-03-31 | 濮阳宏业环保新材料股份有限公司 | Sulfur dioxide urea continuous dissolving device and process |
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2019
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110935391A (en) * | 2019-12-31 | 2020-03-31 | 濮阳宏业环保新材料股份有限公司 | Sulfur dioxide urea continuous dissolving device and process |
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Address after: 457400 east of 600m Road north of the intersection of national highway 106 and Minsheng Road in Puyang industrial agglomeration area, Henan Province Patentee after: Puyang Shengkai environmental protection new material technology Co.,Ltd. Address before: 457400 north of Minsheng Road, Nanle County, Puyang City, Henan Province Patentee before: PUYANG HONGYE ENVIRONMENTAL PROTECTION NEW MATERIAL Co.,Ltd. |