CN211636519U - A novel reaction unit for methyl oleate production test - Google Patents
A novel reaction unit for methyl oleate production test Download PDFInfo
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- CN211636519U CN211636519U CN201922443269.8U CN201922443269U CN211636519U CN 211636519 U CN211636519 U CN 211636519U CN 201922443269 U CN201922443269 U CN 201922443269U CN 211636519 U CN211636519 U CN 211636519U
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Abstract
The utility model provides a novel reaction device for a production test of methyl oleate, which comprises a reaction box, a motor is fixed at the upper end of the reaction box, an output shaft of the motor penetrates through the upper end of the reaction box, extends into the reaction box and is fixedly connected with a middle shaft rod in the reaction box, the annular outer end of the middle shaft rod is fixed with a rotating piece, the upper end of the rotating piece is fixed with a driving component through a pull rope, the driving component is arranged at the top end inside the reaction box, the driving component comprises a guide plate fixed at the top end inside the reaction box and a hollow cylinder fixed at the annular outer end of the middle shaft lever, the deflector is established at the inside and hollow section of thick bamboo laminating of hollow section of thick bamboo on the inside top of reaction box, the lower extreme of deflector evenly is equipped with two at least guide arms, at least two the stay cord is all fixed to the guide arm lower extreme, the utility model discloses rational in infrastructure has improved the material and has mixed the effect, has improved reaction efficiency.
Description
Technical Field
The utility model relates to a novel reaction unit for methyl oleate production test belongs to methyl oleate production technical field.
Background
In the production test of methyl oleate, a reaction kettle needs to be stirred vigorously to realize good mass transfer and heat transfer among materials, and paddle stirring is generally adopted. The reation kettle of current methyl oleate production test usefulness, its inside stirring structure comprises simple paddle mostly, and the motor drives the paddle and can only carry out unidirectional rotation, can't carry out fine upper and lower mixture to the material, leads to mixing effect poor, causes reaction rate low.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a novel reaction unit for methyl oleate production test to solve the inside stirring structure of the reation kettle who provides among the above-mentioned background art methyl oleate production test usefulness and constitute by simple paddle mostly, the paddle can only carry out one-way rotation, can't carry out fine upper and lower mixture to the material, lead to mixing the effect poor, cause the problem that reaction rate is low, the utility model discloses it is rational in infrastructure, improved the material and mixed the effect, improved reaction efficiency.
In order to achieve the above purpose, the present invention is realized by the following technical solution: the utility model provides a novel reaction unit for methyl oleate production test, includes the reaction box, reaction box upper end fixed motor, the output shaft of motor pass the reaction box upper end and extend to the reaction box inside and with the inside axis pole fixed connection of reaction box, the annular outer end fixed rotation piece of axis pole, rotate the piece upper end and pass through the fixed subassembly that drives of stay cord and drive the unit mount on the inside top of reaction box, drive the subassembly including fixing the deflector on the inside top of reaction box and fixing the hollow cylinder in the annular outer end of axis pole, the deflector is established in the inside and hollow cylinder laminating of hollow cylinder on the inside top of reaction box, the lower extreme of deflector evenly is equipped with two at least guide arms, at least two the stay cord is all fixed to the guide arm lower extreme.
Further, the rotating part comprises at least two rotating rods arranged at equal intervals along the vertical direction, at least two rotating rods are connected with one end, close to the middle shaft rod, of each rotating rod through a rotating shaft, at least two connecting blocks are fixed at the annular side end of the middle shaft rod and are adjacent to each other, the rotating rods are fixedly connected through connecting ropes, the uppermost rotating rods are fixedly connected with the guide rod through pull ropes, and the lowermost rotating rods are fixedly provided with gravity blocks at the lower ends of the rotating rods.
Furthermore, an air outlet pipe is fixed at the left position of the upper end of the reaction box and is communicated with the inside of the reaction box.
Further, the charging tube is fixed at the right position of the upper end of the reaction box, and extends to the inside of the reaction box.
Furthermore, the lower end face of the guide plate is processed into an inclined plane with a high left and a low right, at least two guide rods are rotatably provided with round wheels at the upper ends, and the round wheels are attached to the lower end of the inclined plane.
Furthermore, a limiting plate is fixed at the annular outer end of the guide rod, and a spring is arranged between the limiting plate and the bottom end inside the hollow cylinder.
Furthermore, a vertically arranged round hole is formed in the guide plate, the middle shaft rod penetrates through the round hole, at least two through grooves are formed in the bottom end of the inner portion of the hollow cylinder, and at least two guide rods are movably mounted inside the at least two through grooves respectively.
Further, the fixed fluid tank of reaction box lower extreme just extends to the fluid incasement portion, fluid case upper end left position installation thermometer and thermometer extend to the fluid incasement portion, the heating pipe and the heating pipe of the fixed band control by temperature change in the inside bottom of fluid case are established at the reaction box downside.
Further, the fixed liquid feeding pipe in oil liquid case side upper portion position, the drain pipe of the first ooff valve of oil liquid case lower extreme fixed band, the discharging pipe of reaction box lower extreme fixed band second ooff valve, and the discharging pipe passes the oil liquid case and extends to the oil liquid case lower extreme.
The utility model has the advantages that: the utility model discloses a novel reaction unit for methyl oleate production test, 1, through the rotation of motor drive middle axostylus axostyle, thereby it rotates to drive two at least bull sticks of rotating an inside, the middle axostylus axostyle rotates simultaneously and drives hollow section of thick bamboo and guide arm rotation, the guide arm rotates along the inclined plane of deflector lower extreme, the cooperation is in the thrust of compression state's spring to limiting plate and guide arm, reciprocate when making the guide arm pivoted, thereby it reciprocates to drive the bull stick through the stay cord, make the bull stick pivoted in-process carry out the luffing motion simultaneously, the stirring mixed effect of material has been improved, reaction rate has been improved.
2. The heating pipe heats oil in the oil tank, and then the heated oil is used for heating the materials in the reaction tank in an oil bath, so that the reaction is convenient to carry out.
Drawings
Other features, objects and advantages of the invention will become more apparent upon reading of the detailed description of non-limiting embodiments with reference to the following drawings:
FIG. 1 is a schematic diagram of a novel reaction apparatus for a production test of methyl oleate;
FIG. 2 is a partial enlarged view of the part A of the novel reaction apparatus for the production test of methyl oleate;
fig. 3 is a schematic diagram of the guide plate in the novel reaction device for the production test of methyl oleate.
In the figure: 1-reaction box, 2-motor, 3-guide plate, 4-guide rod, 5-spring, 6-pull rope, 7-rotating piece, 8-middle shaft rod, 9-oil tank, 10-driving component, 11-discharging pipe, 12-charging pipe, 41-limiting plate, 42-round wheel, 51-hollow cylinder, 52-through groove, 71-rotating rod, 72-connecting block, 73-connecting rope, 91-discharging pipe and 92-charging pipe.
Detailed Description
In order to make the technical means, creation features, achievement purposes and functions of the present invention easy to understand, the present invention is further described below with reference to the following embodiments.
Referring to fig. 1-3, the present invention provides a technical solution: the utility model provides a novel reaction unit for methyl oleate production test, including reaction box 1 as the reaction carrier, 1 upper end fixed motor 2 of reaction box, motor 2's output shaft passes 1 upper end of reaction box and extends to 1 inside of reaction box and with 1 inside axis pole 8 fixed connection of reaction box, the fixed rotation piece 7 that rotates of 8 annular outer ends of well axostylus axostyle, it drives subassembly 10 and install on 1 inside top of reaction box through 6 fixed drive of stay cord to rotate 7 upper ends, axostylus axostyle 8 and rotation 7 rotate in the motor 2 drive, it drives subassembly 10 and drives bull stick 71 luffing motion through 6 drive stay cords simultaneously to rotate 7 rotations, make and rotate 7 limit luffing motion of rotation, thereby the mixed effect of material has been improved.
The rotating member 7 comprises at least two rotating rods 71 which are arranged at equal intervals along the vertical direction, one ends of the at least two rotating rods 71, which are close to the middle shaft rod 8, are respectively provided with a connecting block 72 through a rotating shaft, the at least two connecting blocks 72 are respectively fixed at the annular side end of the middle shaft rod 8, two adjacent rotating rods 71 are fixedly connected through a connecting rope 73, the rotating rod 71 at the uppermost side is fixedly connected with the guide rod 4 through a pull rope 6, a gravity block is fixed at the lower end of the rotating rod 71 at the lowermost side, the connecting rope 73 facilitates the traction of the at least two rotating rods 71 between each other, the connecting block 72 facilitates the connection of the rotating rods 71 and the middle shaft rod 8, and when the guide rod 4 is convenient for the gravity block to move downwards, the.
An air outlet pipe is fixed at the left position of the upper end of the reaction box 1 and is communicated with the inside of the reaction box 1, so that gas generated in the reaction process can be conveniently discharged.
The fixed filling tube 12 of reaction box 1 upper end right position and filling tube 12 extend to reaction box 1 inside, the interpolation of the reaction mass of being convenient for.
The terminal surface processing is the inclined plane of high right-hand low in the left side under deflector 3, and two at least guide arms 4 upper ends are all through pivot installation round wheel 42, and two at least round wheels 42 all laminate at the inclined plane lower extreme, and when guide arm 4 rotated, round wheel 42 rotated along the inclined plane, and cooperation spring 5 made guide arm 4 reciprocate at the pivoted in-process.
A limiting plate 41 is fixed at the annular outer end of the guide rod 4, a spring 5 is arranged between the limiting plate 41 and the bottom end inside the hollow cylinder 51, and the limiting plate 41 achieves the function of limiting the spring 5.
The inside round hole that is equipped with vertical setting of deflector 3, well axostylus axostyle 8 runs through the round hole, and two at least logical grooves 52 are seted up to the inside bottom of hollow cylinder 51, and two at least guide arms 4 are movable mounting respectively inside two at least logical grooves 52, and well axostylus axostyle 8 can rotate inside the round hole, and guide arm 4 can reciprocate inside logical groove 52.
Inside the fixed fluid case 9 of 1 lower extreme of reaction box and extending to fluid case 9, inside fluid case 9 upper end left part position installation thermometer and thermometer extended to fluid case 9, the heating pipe and the heating pipe of the inside bottom fixed band control by temperature change of fluid case 9 established at 1 downside of reaction box, the inside loading of fluid case 9 has fluid, heat fluid through the heating pipe, the realization carries out the oil bath heating to the material of reaction box 1 inside, the thermometer is convenient for detect the temperature of fluid.
9 side upper portion position of fluid case fixes liquid feeding pipe 92, the drain pipe 91 of the first ooff valve of the lower extreme fixed band of fluid case 9, discharging pipe 11 and the discharging pipe 11 of 1 lower extreme fixed band second ooff valve of reaction box pass fluid case 9, and extend to the 9 lower extremes of fluid case, the joining of fluid of being convenient for of liquid feeding pipe 92, the discharging pipe 91 fluid of being convenient for discharge, discharging pipe 11 is convenient for discharge the material after the reaction.
The working principle is as follows: personnel will react required material through filling tube 12 and add inside reaction box 1, then through the rotation of motor 2 drive in the axostylus axostyle 8, thereby drive two at least bull stick 71 rotations of rotating 7 inside, simultaneously well axostylus axostyle 8 rotates and drives hollow section of thick bamboo 51 and guide arm 4 and rotate, guide arm 4 rotates along the inclined plane of deflector 3 lower extreme, the cooperation is in compression state's spring 5 to limiting plate 41 and guide arm 4's thrust, reciprocate when making guide arm 4 pivoted, thereby it reciprocates to drive bull stick 71 through stay cord 6, make bull stick 71 pivoted in-process carry out the luffing motion simultaneously, the stirring mixed effect of material has been improved, reaction rate has been improved.
The basic principles and the main features of the invention and the advantages of the invention have been shown and described above, it will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, but that the invention may be embodied in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (9)
1. A novel reaction unit for methyl oleate production test, includes reaction box (1), its characterized in that: the motor (2) is fixed at the upper end of the reaction box (1), an output shaft of the motor (2) penetrates through the upper end of the reaction box (1), extends into the reaction box (1) and is fixedly connected with a middle shaft lever (8) in the reaction box (1), a rotating piece (7) is fixed at the annular outer end of the middle shaft lever (8), a driving assembly (10) is fixed at the upper end of the rotating piece (7) through a pull rope (6), and the driving assembly (10) is installed at the top end in the reaction box (1);
drive subassembly (10) including fixing deflector (3) on reaction box (1) inside top and fixing hollow section of thick bamboo (51) in well axostylus axostyle (8) annular outer end, deflector (3) are established in hollow section of thick bamboo (51) inside and hollow section of thick bamboo (51) laminating on reaction box (1) inside top, the lower extreme of deflector (3) evenly is equipped with two at least guide arms (4), at least two stay cord (6) are all fixed to guide arm (4) lower extreme.
2. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: the rotating piece (7) comprises at least two rotating rods (71) which are arranged along the equal distance of the vertical direction, at least two rotating rods (71) are connected with one end of a middle shaft rod (8) in a close mode through rotating shafts, at least two connecting blocks (72) are fixed on the annular side end of the middle shaft rod (8) and are adjacent to each other, the rotating rods (71) are fixedly connected through connecting ropes (73), the rotating rods (71) are uppermost and are fixedly connected with guide rods (4) through pull ropes (6), and the rotating rods (71) are arranged at the lowest side.
3. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: an air outlet pipe is fixed at the left part of the upper end of the reaction box (1) and is communicated with the inside of the reaction box (1).
4. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: reaction box (1) upper end right part position fixed feed pipe (12) and feed pipe (12) extend to inside reaction box (1).
5. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: the lower end face of the guide plate (3) is processed into an inclined plane with a high left and a low right, at least two guide rods (4) are rotatably provided with round wheels (42), and the round wheels (42) are attached to the lower end of the inclined plane.
6. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: a limiting plate (41) is fixed at the annular outer end of the guide rod (4), and a spring (5) is arranged between the limiting plate (41) and the bottom end inside the hollow cylinder (51).
7. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: the guide plate (3) is internally provided with a vertically arranged round hole, the middle shaft rod (8) penetrates through the round hole, the bottom end inside the hollow cylinder (51) is provided with at least two through grooves (52), and the at least two guide rods (4) are respectively and movably arranged inside the at least two through grooves (52).
8. The novel reaction device for the production test of methyl oleate according to claim 1, wherein: the fixed oil tank (9) of reaction box (1) lower extreme just extends to inside oil tank (9), inside oil tank (9) upper end left part position installation thermometer and thermometer extended to oil tank (9), the heating pipe and the heating pipe of the inside bottom fixed band temperature control of oil tank (9) are established at reaction box (1) downside.
9. The novel reaction device for the production test of methyl oleate according to claim 8, wherein: oil tank (9) side upper portion position fixing liquid feeding pipe (92), drain pipe (91) of the first ooff valve of oil tank (9) lower extreme fixed band, discharging pipe (11) of reaction box (1) lower extreme fixed band second ooff valve, and discharging pipe (11) pass oil tank (9) and extend to oil tank (9) lower extreme.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922443269.8U CN211636519U (en) | 2019-12-30 | 2019-12-30 | A novel reaction unit for methyl oleate production test |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922443269.8U CN211636519U (en) | 2019-12-30 | 2019-12-30 | A novel reaction unit for methyl oleate production test |
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| CN211636519U true CN211636519U (en) | 2020-10-09 |
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| CN201922443269.8U Active CN211636519U (en) | 2019-12-30 | 2019-12-30 | A novel reaction unit for methyl oleate production test |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113230991A (en) * | 2021-04-29 | 2021-08-10 | 付豪 | Modified organosilicon coating preparation equipment |
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2019
- 2019-12-30 CN CN201922443269.8U patent/CN211636519U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113230991A (en) * | 2021-04-29 | 2021-08-10 | 付豪 | Modified organosilicon coating preparation equipment |
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Address after: 215000 Donghai Road, Jiangsu Yangzi River International Chemical Industrial Park, Suzhou, Jiangsu Patentee after: Suzhou Fengbei Biotechnology Co.,Ltd. Address before: Room 346b, building a, emerging industry development center, Zhangjiagang Free Trade Zone, Suzhou, Jiangsu 215000 Patentee before: SUZHOU FENGBEI BIOTECH Co.,Ltd. |
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