CN211513476U - Efficient rotary evaporator capable of rapidly separating out saccharide intermediate - Google Patents

Efficient rotary evaporator capable of rapidly separating out saccharide intermediate Download PDF

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Publication number
CN211513476U
CN211513476U CN201922425785.8U CN201922425785U CN211513476U CN 211513476 U CN211513476 U CN 211513476U CN 201922425785 U CN201922425785 U CN 201922425785U CN 211513476 U CN211513476 U CN 211513476U
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water tank
box
gear
cylinder
heat dissipation
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CN201922425785.8U
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徐博
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Nanjing Wester Pharmaceutical Technology Co ltd
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Nanjing Wester Pharmaceutical Technology Co ltd
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Abstract

The utility model discloses a high-efficiency rotary evaporator for rapidly separating out saccharide intermediates, which comprises an evaporation cylinder; the evaporation cylinder is arranged at the top of the base; the outer surface of the base is provided with a control panel; the top of the evaporation cylinder is provided with a driving box; a feeding mechanism and a heater are arranged on one side of the evaporation cylinder; a stirring device is arranged in the evaporation cylinder corresponding to the driving box; the bottom end in the evaporation cylinder is provided with a rotating disc; a driving mechanism is arranged in the base corresponding to the rotating disc; the outer circumference of the rotating disc is fixedly connected with a rotating cylinder; the stirring device extends into the rotary cylinder; the other side of the evaporation cylinder is communicated with a condensing box through a condensate pipe; and a condensing mechanism is arranged on the condensing box. The utility model discloses convenient to use is energy-conserving, and work efficiency is high.

Description

Efficient rotary evaporator capable of rapidly separating out saccharide intermediate
Technical Field
The utility model relates to a sugar processing technology field specifically is a high-efficient rotary evaporator who precipitates sugar midbody fast.
Background
The sugar intermediate precipitation needs to use a rotary evaporator; the rotary evaporator comprises a distillation flask, a rotating device, a condensing device, an evaporation tube, a heating device and other components, the distillation flask is in a negative pressure state through a vacuum pump, the distillation flask is rotated and simultaneously placed in a water bath kettle for constant-temperature heating, and a solution in the distillation flask is rotated and heated under the negative pressure to heat a solvent in the distillation flask, so that the solvent forms a film, and the evaporation area is increased. The existing rotary evaporator has low working efficiency in the preparation of the intermediate of the saccharides, and the saccharides are easy to solidify in the processing.
Therefore, in view of the above situation, there is an urgent need to develop a high-efficiency rotary evaporator capable of rapidly precipitating a saccharide intermediate.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a high-efficient rotatory evaporimeter of sugar midbody is appeared fast to solve the problem that proposes in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme:
a high-efficiency rotary evaporator for rapidly separating out saccharide intermediate comprises an evaporation cylinder; the evaporation cylinder is arranged at the top of the base; the outer surface of the base is provided with a control panel; the top of the evaporation cylinder is provided with a driving box; a feeding mechanism and a heater are arranged on one side of the evaporation cylinder; a stirring device is arranged in the evaporation cylinder corresponding to the driving box; the bottom end in the evaporation cylinder is provided with a rotating disc; a driving mechanism is arranged in the base corresponding to the rotating disc; the outer circumference of the rotating disc is fixedly connected with a rotating cylinder; the stirring device extends into the rotary cylinder; the other side of the evaporation cylinder is communicated with a condensing box through a condensate pipe; and a condensing mechanism is arranged on the condensing box.
As a further aspect of the present invention: the feeding mechanism comprises a feeding hole, a measuring cylinder and an electromagnetic tube from top to bottom in sequence; an electromagnetic one-way valve is arranged in the electromagnetic pipe.
As a further aspect of the present invention: a driving motor is arranged in the driving box; the driving motor is connected with the driving gear through a coupler; both sides of the driving gear are rotatably connected with driven gears; the bottom end of the driven gear is connected with a stirring mechanism; the stirring mechanism comprises a first stirring paddle and a second stirring paddle.
As a further aspect of the present invention: the top end of the driven gear is connected with a heat dissipation mechanism; the heat dissipation mechanism comprises a first gear; the first gear is connected with the driven gear through a shaft; the first gear is meshed with the second gear; the second gear is connected with the rotating blade through a rotating shaft; the inner wall of the driving box is provided with a heat dissipation copper pipe; the inner wall of the driving box is provided with a heat dissipation cover corresponding to the heat dissipation copper pipe; and the heat dissipation cover is provided with an activated carbon net.
As a further aspect of the present invention: the condensing mechanism comprises a condensing pipe; one end of the condensing pipe is communicated with a second water tank; the other end of the condensation pipe is connected with a first water tank; the first water tank and the second water tank are both arranged on the outer surface of the condensing box; the first water tank and the second water tank are also communicated through a circulating water tank; a pressure water pump is arranged on the circulating water tank; a semiconductor refrigerator is arranged on the side surface of the second water tank; the semiconductor refrigerator comprises a cold end and a hot end; the cold junction passes through the fixture block joint in the inside of No. two water tanks.
As a further aspect of the present invention: the bottom end of the base is provided with a moving mechanism; the moving mechanism comprises a supporting column; at least four support columns are arranged; the bottom end of the supporting column is provided with a lifting box; a lifting mechanism is arranged inside the lifting box; the bottom end of the lifting mechanism is correspondingly provided with universal wheels.
Compared with the prior art, the beneficial effects of the utility model are that: the measuring cylinder is convenient for accurate addition, and the electromagnetic tube is arranged to prevent the device from air leakage; through the arrangement of the first stirring paddle, the rotor and the second stirring paddle, the raw materials can be fully stirred; through the arrangement of the heat dissipation mechanism, the heat dissipation copper pipe and the heat dissipation cover, the kinetic energy of the driving motor can be provided for the heat dissipation mechanism, so that heat dissipation can be realized, good operation of the driving motor can be kept, and the mechanical energy of the driving motor can be fully utilized; the arrangement of the condensation pipe, the second water tank, the semiconductor refrigerator and the circulating water tank can quickly condense evaporated gas, and the working efficiency is improved; through the arrangement of the lifting mechanism, the universal wheels can be collected into the lifting box, so that the work is not influenced, and the movement is convenient. To sum up, the utility model discloses convenient to use is energy-conserving, and work efficiency is high.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a schematic structural view of the enlarged part of the present invention.
Fig. 3 is a schematic structural diagram of a semiconductor refrigerator according to the present invention.
In the figure: 1-driving box, 2-feeding mechanism, 3-evaporator, 4-stirring paddle, 5-stirring paddle, 6-heater, 7-rotor, 8-rotating disk, 9-condensate pipe, 10-condenser box, 11-water tank, 12-condenser pipe, 13-water tank, 14-semiconductor refrigerator, 15-circulating water pipe, 16-base, 17-control panel, 18-moving mechanism, 19-driving motor, 20-driving gear, 21-driven gear, 22-gear, 23-gear, 24-rotating blade, 25-radiating copper pipe, 26-radiating cover, 27-cold end, 28-fixture block, 29-hot end.
Detailed Description
The technical solution of the present patent will be described in further detail with reference to the following embodiments.
Reference will now be made in detail to embodiments of the present patent, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are exemplary only for the purpose of explaining the present patent and are not to be construed as limiting the present patent.
Example 1
Referring to fig. 1-3, in an embodiment of the present invention, a high efficiency rotary evaporator for rapidly separating out saccharide intermediates includes an evaporation cylinder 3; the evaporation cylinder 3 is arranged on the top of the base 16; the outer surface of the base 16 is provided with a control panel 17; the top of the evaporation cylinder 3 is provided with a driving box 1; a feeding mechanism 2 and a heater 6 are arranged on one side of the evaporation cylinder 3; a stirring device is arranged in the evaporation cylinder 3 corresponding to the driving box 1; the bottom end in the evaporation cylinder 3 is provided with a rotating disc 8; a driving mechanism is arranged in the base 16 corresponding to the rotating disc 8; the outer circumference of the rotating disc 8 is fixedly connected with a rotating cylinder; the stirring device extends into the rotary cylinder; the other side of the evaporation cylinder 3 is communicated with a condensation box 10 through a condensate pipe 9; and a condensing mechanism is arranged on the condensing box 10.
Further, the feeding mechanism 2 comprises a feeding hole, a measuring cylinder and an electromagnetic tube from top to bottom in sequence; an electromagnetic one-way valve is arranged in the electromagnetic pipe; the measuring cylinder is convenient and accurate in adding amount, and the electromagnetic tube is arranged to prevent air leakage of the device.
Further, a driving motor 19 is arranged inside the driving box 1; the driving motor 19 is connected with a driving gear 20 through a coupler; both sides of the driving gear 20 are rotatably connected with driven gears 21; the bottom end of the driven gear 21 is connected with a stirring mechanism; the stirring mechanism comprises a first stirring paddle 4 and a second stirring paddle 5; through the setting of stirring rake 4, rotor 7 and No. two stirring rakes 5, can be with the raw materials intensive mixing.
Further, the top end of the driven gear 21 is connected with a heat dissipation mechanism; the heat dissipation mechanism comprises a first gear 22; the first gear 22 is connected with the driven gear 21 through a shaft; the first gear 22 is in meshed connection with the second gear 23; the second gear 23 is connected with a rotating blade 24 through a rotating shaft; the inner wall of the driving box 1 is provided with a heat radiation copper pipe 25; the inner wall of the driving box 1 is provided with a heat dissipation cover 26 corresponding to the heat dissipation copper pipe 25; an active carbon net is arranged on the heat dissipation cover 26; through the arrangement of the heat dissipation mechanism, the heat dissipation copper pipe 25 and the heat dissipation cover 26, the kinetic energy of the driving motor 19 can be provided for the heat dissipation mechanism, so that heat dissipation can be realized, good operation of the driving motor 19 can be kept, and the mechanical energy of the driving motor 19 can be fully utilized.
Further, the condensing mechanism includes a condensing pipe 12; one end of the condensation pipe 12 is communicated with a second water tank 13; the other end of the condensation pipe 12 is connected with a first water tank 11; the first water tank 11 and the second water tank 13 are both arranged on the outer surface of the condensation box 10; the first water tank 11 and the second water tank 13 are also communicated through a circulating water tank 15; a pressure water pump is arranged on the circulating water tank 15; a semiconductor refrigerator 14 is arranged on the side surface of the second water tank 13; the semiconductor refrigerator 14 includes a cold end 27 and a hot end 29; the lower the temperature of the hot end 29, the lower the temperature of the cold end 27; the cold end 27 is clamped in the second water tank 13 through a clamping block 28; through the setting of condenser pipe 12, No. two water tank 13, semiconductor refrigerator 14 and circulating water tank 15, can promote work efficiency with the gaseous rapid condensation of evaporation.
Example 2
Referring to fig. 1, a moving mechanism 18 is installed at the bottom end of the base 16; the moving mechanism 18 includes a support column; at least four support columns are arranged; the bottom end of the supporting column is provided with a lifting box; a lifting mechanism is arranged inside the lifting box; universal wheels are correspondingly arranged at the bottom end of the lifting mechanism; through the arrangement of the lifting mechanism, the universal wheels can be collected into the lifting box, so that the work is not influenced, and the movement is convenient.
The utility model discloses a theory of operation is: the measuring cylinder is convenient for accurate addition, and the electromagnetic tube is arranged to prevent the device from air leakage; through the arrangement of the first stirring paddle 4, the rotor 7 and the second stirring paddle 5, the raw materials can be fully stirred; through the arrangement of the heat dissipation mechanism, the heat dissipation copper pipe 25 and the heat dissipation cover 26, the kinetic energy of the driving motor 19 can be provided for the heat dissipation mechanism, so that heat dissipation can be realized, good operation of the driving motor 19 can be kept, and the mechanical energy of the driving motor 19 can be fully utilized; the arrangement of the condensation pipe 12, the second water tank 13, the semiconductor refrigerator 14 and the circulating water tank 15 can quickly condense evaporated gas, and the working efficiency is improved; through the arrangement of the lifting mechanism, the universal wheels can be collected into the lifting box, so that the work is not influenced, and the movement is convenient. To sum up, the utility model discloses convenient to use is energy-conserving, and work efficiency is high.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (6)

1. A high-efficiency rotary evaporator for rapidly separating out saccharide intermediates comprises an evaporation cylinder (3); the device is characterized in that the evaporation cylinder (3) is arranged at the top of the base (16); a control panel (17) is arranged on the outer surface of the base (16); the top of the evaporation cylinder (3) is provided with a driving box (1); a feeding mechanism (2) and a heater (6) are arranged on one side of the evaporation cylinder (3); a stirring device is arranged in the evaporation cylinder (3) corresponding to the driving box (1); the bottom end in the evaporation cylinder (3) is provided with a rotating disc (8); a driving mechanism is arranged in the base (16) corresponding to the rotating disc (8); the outer circumference of the rotating disc (8) is fixedly connected with a rotating cylinder; the stirring device extends into the rotary cylinder; the other side of the evaporation cylinder (3) is communicated with a condensation box (10) through a condensate pipe (9); and a condensing mechanism is arranged on the condensing box (10).
2. The high-efficiency rotary evaporator for rapidly separating out saccharide intermediates according to claim 1, wherein the feeding mechanism (2) comprises a feeding hole, a measuring cylinder and a solenoid from top to bottom; an electromagnetic one-way valve is arranged in the electromagnetic pipe.
3. The high-efficiency rotary evaporator for rapidly precipitating intermediate sugars as claimed in claim 1, wherein a driving motor (19) is provided inside the driving box (1); the driving motor (19) is connected with a driving gear (20) through a coupler; both sides of the driving gear (20) are rotatably connected with driven gears (21); the bottom end of the driven gear (21) is connected with a stirring mechanism; the stirring mechanism comprises a first stirring paddle (4) and a second stirring paddle (5).
4. The high-efficiency rotary evaporator for rapidly precipitating a saccharide intermediate according to claim 3, wherein a heat dissipation mechanism is connected to the top end of the driven gear (21); the heat dissipation mechanism comprises a first gear (22); the first gear (22) is connected with the driven gear (21) through a shaft; the first gear (22) is in meshed connection with the second gear (23); the second gear (23) is connected with a rotating blade (24) through a rotating shaft; the inner wall of the driving box (1) is provided with a heat dissipation copper pipe (25); the inner wall of the driving box (1) is provided with a heat dissipation cover (26) corresponding to the heat dissipation copper pipe (25); and an active carbon net is arranged on the heat dissipation cover (26).
5. The high-efficiency rotary evaporator for rapid precipitation of sugar intermediates according to claim 1, wherein the condensing mechanism comprises a condensing tube (12); one end of the condensation pipe (12) is communicated with a second water tank (13); the other end of the condensation pipe (12) is connected with a first water tank (11); the first water tank (11) and the second water tank (13) are both arranged on the outer surface of the condensation box (10); the first water tank (11) is communicated with the second water tank (13) through a circulating water tank (15); a pressure water pump is arranged on the circulating water tank (15); a semiconductor refrigerator (14) is arranged on the side surface of the second water tank (13); the semiconductor refrigerator (14) comprises a cold end (27) and a hot end (29); the cold end (27) is clamped in the second water tank (13) through a clamping block (28).
6. The high-efficiency rotary evaporator for rapidly precipitating sugar intermediates according to claim 1, wherein the bottom end of the base (16) is provided with a moving mechanism (18); the moving mechanism (18) comprises a support column; at least four support columns are arranged; the bottom end of the supporting column is provided with a lifting box; a lifting mechanism is arranged inside the lifting box; the bottom end of the lifting mechanism is correspondingly provided with universal wheels.
CN201922425785.8U 2019-12-30 2019-12-30 Efficient rotary evaporator capable of rapidly separating out saccharide intermediate Active CN211513476U (en)

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Application Number Priority Date Filing Date Title
CN201922425785.8U CN211513476U (en) 2019-12-30 2019-12-30 Efficient rotary evaporator capable of rapidly separating out saccharide intermediate

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Application Number Priority Date Filing Date Title
CN201922425785.8U CN211513476U (en) 2019-12-30 2019-12-30 Efficient rotary evaporator capable of rapidly separating out saccharide intermediate

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110694295A (en) * 2019-10-11 2020-01-17 郑刚 Special extraction device and extraction method for chamomile extract

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110694295A (en) * 2019-10-11 2020-01-17 郑刚 Special extraction device and extraction method for chamomile extract

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