CN211215458U - Purification device is used in chemical reagent preparation - Google Patents
Purification device is used in chemical reagent preparation Download PDFInfo
- Publication number
- CN211215458U CN211215458U CN201922031180.0U CN201922031180U CN211215458U CN 211215458 U CN211215458 U CN 211215458U CN 201922031180 U CN201922031180 U CN 201922031180U CN 211215458 U CN211215458 U CN 211215458U
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- chemical reagent
- reagent preparation
- box
- arranged above
- filter screen
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- 239000003153 chemical reaction reagent Substances 0.000 title claims abstract description 35
- 238000000746 purification Methods 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000007788 liquid Substances 0.000 claims abstract description 35
- 238000001704 evaporation Methods 0.000 claims abstract description 25
- 238000010438 heat treatment Methods 0.000 claims abstract description 18
- 238000007789 sealing Methods 0.000 claims abstract description 18
- 239000000919 ceramic Substances 0.000 claims abstract description 17
- 238000002955 isolation Methods 0.000 claims abstract description 13
- 239000002699 waste material Substances 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 4
- 238000005192 partition Methods 0.000 claims 2
- 230000008020 evaporation Effects 0.000 abstract description 13
- 239000012535 impurity Substances 0.000 abstract description 6
- 241000883990 Flabellum Species 0.000 abstract description 4
- 238000009833 condensation Methods 0.000 description 9
- 230000005494 condensation Effects 0.000 description 9
- 238000000926 separation method Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000010977 unit operation Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a purification device is used in chemical reagent preparation, including box and ceramic heating evaporating plate, the below axis of box is provided with the motor, the top of pivot is provided with the bottom sealing washer, the top outside of rotary rod is provided with the flabellum, the right side of spout is provided with the filter box, the axis top of inlet is provided with well cavity pole, the top of division board is provided with the isolation sealing washer, the right side below of condenser pipe is provided with out the liquid valve, the right side of ejection of compact valve is provided with out the workbin, the top of filter screen is provided with the door closure, the right side of handle is provided with the hinge, ceramic heating evaporating plate is located the right side below of inlet. This purification device is used in chemical reagent preparation compares with purification device for current general chemical reagent preparation for reagent is heated evenly, accelerates the evaporation rate, increases work efficiency, and it is simple and convenient to handle impurity, and is convenient for wash out incasement portion, and the condensing rate is fast.
Description
Technical Field
The utility model relates to a chemical reagent purification technical field specifically is a purification device is used in chemical reagent preparation.
Background
The purification means that impurities in a mixture are separated to improve the purity of the mixture, and the purification is an important chemical method and plays an important role in chemical preparation, most of the existing purification devices adopt a distillation method for purification, and the distillation is a thermodynamic separation process, and a unit operation process of evaporating low-boiling components by utilizing different boiling points of components in a mixed liquid or liquid-solid system and then condensing to separate the whole components is a combination of two unit operations of evaporation and condensation.
The chemical reagent preparation purification device at the present stage, reagent are heated inhomogeneously, and evaporation rate is slow, has slowed down work efficiency, and inconvenient washing goes out incasement portion, and the condensing rate is slow, so can not be fine satisfy people's user demand, to above-mentioned condition, carry out technical innovation on current chemical reagent purification device basis.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a purification device is used in chemical reagent preparation to it is inhomogeneous that the reagent of general chemical reagent preparation purification device is heated to provide in solving above-mentioned background art, and evaporation rate is slow, has slowed down work efficiency, and inconvenient washing goes out incasement portion, and the condensing rate is slow, so can not be fine satisfy people's user demand problem.
In order to achieve the above object, the utility model provides a following technical scheme: a purifying device for preparing chemical reagents comprises a box body and a ceramic heating evaporation plate, wherein a motor is arranged on the central axis below the box body, a rotating shaft is arranged above the motor, a bottom sealing ring is arranged above the rotating shaft, a rotating rod is arranged on the inner side of the bottom sealing ring, fan blades are arranged outside the rotating rod, a sliding groove is formed in the right side of each fan blade, a filter box is arranged on the right side of the sliding groove, a liquid inlet is formed in the upper portion of the filter box, a hollow rod is arranged above the central axis of the liquid inlet, an isolation plate is arranged outside the hollow rod, an isolation sealing ring is arranged above the isolation plate, a condensation pipe is arranged above the right side of the isolation sealing ring, a liquid outlet valve is arranged below the right side of the condensation pipe, a discharge valve is arranged below the liquid outlet valve, a discharge box is arranged on the, and the inside top of ejection of compact case is provided with the filter screen, the top of filter screen is provided with the door closure, and door closure left side top is provided with the handle, the right side of handle is provided with the hinge, and the below of hinge is provided with the waste liquid valve, the ceramic heating evaporating plate is located the right side below of inlet, and the right side of ceramic heating evaporating plate is provided with the feed inlet.
Preferably, the box body and the motor are detachably connected, and the motor and the rotating rod are welded.
Preferably, the rotating rod forms a rotating structure through a rotating shaft, and the rotating rod is detachably connected with the fan blades.
Preferably, the box body is fixedly connected with the sliding groove, and the filter box forms a sliding structure through the sliding groove.
Preferably, the discharge box is detachably connected with the filter screen, and the filter screen is parallel to the door cover.
Preferably, the door cover and the handle are welded, and the door cover forms a rotating structure through a hinge.
Compared with the prior art, the beneficial effects of the utility model are as follows:
1. the utility model discloses a rotatory setting is constituteed to box, motor, pivot, bottom sealing washer, rotary rod, flabellum and ceramic heating evaporating plate, and ceramic heating evaporating plate heating work, rotary rod constitute revolution mechanic through the pivot, and the rotary rod drives the reagent in the flabellum stirring box body for the reagent is heated evenly, accelerates evaporation rate, increases work efficiency;
2. the utility model discloses a spout, filter cartridge, play workbin, filter screen, door closure, handle and hinge constitute the setting of filtering collection, during the feeding, prevent that impurity in the reagent from getting into the box, the filter cartridge can slide and take out, makes things convenient for the filter cartridge to wash, and after the purification is accomplished, the staff opens the door closure, takes out the filter screen from the draw-in groove of play workbin, and it is simple and convenient to handle impurity, and is convenient for wash the workbin inside;
3. the utility model discloses a setting of inlet, well cavity pole, division board, isolation sealing washer, condenser pipe and play liquid valve constitution condensation, reagent gas gets into the condensation zone through well cavity pole from the inlet, becomes liquid through the condenser pipe and falls on the division board, and isolation sealing washer prevents liquid downflow, and the condenser pipe crosses the box, and the condenser pipe both ends are sealed, and the condensation speed is fast.
Drawings
FIG. 1 is a schematic view of the interior of the present invention;
FIG. 2 is a schematic view of the side view of the inside of the present invention;
fig. 3 is a schematic view of the top view structure of the present invention.
In the figure: 1. a box body; 2. a motor; 3. a rotating shaft; 4. a bottom layer seal ring; 5. rotating the rod; 6. a fan blade; 7. a chute; 8. a filter cartridge; 9. a liquid inlet; 10. a hollow shaft; 11. a separator plate; 12. isolating the sealing ring; 13. a condenser tube; 14. a liquid outlet valve; 15. a discharge valve; 16. a discharging box; 17. a filter screen; 18. a door cover; 19. a handle; 20. a hinge; 21. a waste liquid valve; 22. ceramic heating evaporation plates; 23. and (4) feeding a material inlet.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: a purifying device for preparing chemical reagents comprises a box body 1 and a ceramic heating evaporation plate 22, wherein a motor 2 is arranged on the central axis below the box body 1, a rotating shaft 3 is arranged above the motor 2, a bottom sealing ring 4 is arranged above the rotating shaft 3, a rotating rod 5 is arranged on the inner side of the bottom sealing ring 4, the box body 1 is detachably connected with the motor 2, the motor 2 is welded with the rotating rod 5, a fan blade 6 is arranged outside the upper part of the rotating rod 5, a sliding groove 7 is arranged on the right side of the fan blade 6, the rotating rod 5 forms a rotating structure through the rotating shaft 3, the rotating rod 5 is detachably connected with the fan blade 6, the box body 1 is used for arranging the motor 2, the rotating shaft 3, the bottom sealing ring 4, the rotating rod 5, the fan blade 6 and the ceramic heating evaporation plate 22 to form a rotating device, the ceramic heating evaporation plate 22 is heated, and the, the rotating rod 5 drives the fan blades 6 to stir the reagent in the box body 1, so that the reagent is heated uniformly, the evaporation speed is increased, and the working efficiency is increased;
a filter box 8 is arranged on the right side of the chute 7, a liquid inlet 9 is arranged above the filter box 8, the box body 1 is fixedly connected with the chute 7, the filter box 8 forms a sliding structure through the chute 7, a hollow rod 10 is arranged above the central axis of the liquid inlet 9, a separation plate 11 is arranged outside the hollow rod 10, an isolation seal ring 12 is arranged above the separation plate 11, a condenser pipe 13 is arranged above the right side of the isolation seal ring 12, a liquid outlet valve 14 is arranged below the right side of the condenser pipe 13, a discharge valve 15 is arranged below the liquid outlet valve 14, a condensation device is formed by the liquid inlet 9, the hollow rod 10, the separation plate 11, the isolation seal ring 12, the condenser pipe 13 and the liquid outlet valve 14, reagent gas enters a condensation area through the hollow rod 10 from the liquid inlet 9, liquid is changed into liquid through the condenser pipe 13 and falls on the separation plate 11, the isolation seal ring 12 prevents the liquid from flowing, the condenser pipe 13 traverses the box body 1, and two ends of the condenser pipe 13 are sealed, so that the condensing speed is high;
a discharge box 16 is arranged on the right side of the discharge valve 15, a filter screen 17 is arranged above the discharge box 16, a door cover 18 is arranged above the filter screen 17, a handle 19 is arranged above the left side of the door cover 18, the discharge box 16 is detachably connected with the filter screen 17, the filter screen 17 is parallel to the door cover 18, a hinge 20 is arranged on the right side of the handle 19, a waste liquid valve 21 is arranged below the hinge 20, the door cover 18 is welded with the handle 19, the door cover 18 forms a rotating structure through the hinge 20, a filter box 8, the discharge box 16, the filter screen 17, the door cover 18, the handle 19 and the hinge 20 form a filtering and collecting device, when feeding is performed, impurities in a reagent are prevented from entering the box body 1, the filter box 8 can be taken out in a sliding manner, the filter box 8 is convenient to clean, after purification is completed, a worker opens the door cover 18, the filter screen 17 is taken out from a clamping groove of the discharge box, handle impurity simple and conveniently, and be convenient for wash out inside the workbin 16, ceramic heating evaporating plate 22 is located the right side below of inlet 9, and ceramic heating evaporating plate 22's right side is provided with feed inlet 23.
The working principle is as follows: when using this purification device for chemical reagent preparation, at first, the staff places the reagent from feed inlet 23, feed inlet 23 can be airtight, the reagent passes through filter cartridge 8 and gets into box 1, ceramic heating evaporation board 22 work, it makes flabellum 6 rotatory to open motor 2, let the reagent be heated evenly, rapid evaporation, gas reaches the condensation zone from inlet 9 and hollow rod 10, become liquid through condenser pipe 13 and fall on division board 11, keep apart sealing washer 12 and guarantee the seal of division board 11, reagent liquid is collected from liquid outlet valve 14, the smooth slope of bottom in the box 1, waste residue and waste liquid pass through discharge valve 15 and reach discharge box 16, on filter screen 17, be convenient for take out, waste liquid flows out from waste liquid valve 21.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a purification device is used in chemical reagent preparation, includes box (1) and ceramic heating evaporating plate (22), its characterized in that: the box body is characterized in that a motor (2) is arranged on the central axis below the box body (1), a rotating shaft (3) is arranged above the motor (2), a bottom sealing ring (4) is arranged above the rotating shaft (3), a rotating rod (5) is arranged on the inner side of the bottom sealing ring (4), a fan blade (6) is arranged outside the rotating rod (5), a sliding groove (7) is arranged on the right side of the fan blade (6), a filtering box (8) is arranged on the right side of the sliding groove (7), a liquid inlet (9) is arranged above the filtering box (8), a hollow rod (10) is arranged above the central axis of the liquid inlet (9), a partition plate (11) is arranged outside the hollow rod (10), an isolation sealing ring (12) is arranged above the partition plate (11), a condensing pipe (13) is arranged above the right side of the isolation sealing ring (12), a liquid outlet valve (14) is arranged below the right side of the condensing, and the below of going out liquid valve (14) is provided with ejection of compact valve (15), the right side of ejection of compact valve (15) is provided with ejection of compact case (16), and is provided with filter screen (17) above the inside of ejection of compact case (16), the top of filter screen (17) is provided with door closure (18), and door closure (18) left side top is provided with handle (19), the right side of handle (19) is provided with hinge (20), and the below of hinge (20) is provided with waste liquid valve (21), ceramic heating evaporating plate (22) are located the right side below of inlet (9), and the right side of ceramic heating evaporating plate (22) is provided with feed inlet (23).
2. The purifying apparatus for chemical reagent preparation according to claim 1, wherein: the box body (1) and the motor (2) are detachably connected, and the motor (2) and the rotating rod (5) are welded.
3. The purifying apparatus for chemical reagent preparation according to claim 1, wherein: the rotary rod (5) forms a rotary structure through the rotary shaft (3), and the rotary rod (5) is detachably connected with the fan blades (6).
4. The purifying apparatus for chemical reagent preparation according to claim 1, wherein: the box body (1) is fixedly connected with the sliding groove (7), and the filter box (8) forms a sliding structure through the sliding groove (7).
5. The purifying apparatus for chemical reagent preparation according to claim 1, wherein: go out between workbin (16) and filter screen (17) for dismantling the connection, and filter screen (17) and door closure (18) are parallel state.
6. The purifying apparatus for chemical reagent preparation according to claim 1, wherein: the door cover (18) and the handle (19) are welded, and the door cover (18) forms a rotating structure through a hinge (20).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922031180.0U CN211215458U (en) | 2019-11-22 | 2019-11-22 | Purification device is used in chemical reagent preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922031180.0U CN211215458U (en) | 2019-11-22 | 2019-11-22 | Purification device is used in chemical reagent preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN211215458U true CN211215458U (en) | 2020-08-11 |
Family
ID=71940688
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201922031180.0U Expired - Fee Related CN211215458U (en) | 2019-11-22 | 2019-11-22 | Purification device is used in chemical reagent preparation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN211215458U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116099224A (en) * | 2023-03-16 | 2023-05-12 | 安徽瑞柏新材料有限公司 | Ethyl acetate production is with recovery unit that can intelligent temperature regulation |
-
2019
- 2019-11-22 CN CN201922031180.0U patent/CN211215458U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116099224A (en) * | 2023-03-16 | 2023-05-12 | 安徽瑞柏新材料有限公司 | Ethyl acetate production is with recovery unit that can intelligent temperature regulation |
| CN116099224B (en) * | 2023-03-16 | 2023-08-01 | 安徽瑞柏新材料有限公司 | Ethyl acetate production is with recovery unit that can intelligent temperature regulation |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200811 |