CN211159651U

CN211159651U - Material lifting device of trifluoromethanesulfonic acid reaction kettle

Info

Publication number: CN211159651U
Application number: CN201921850633.6U
Authority: CN
Inventors: 陈红斌; 祝金玲; 黄素玉
Original assignee: Time Chemical Co Ltd
Current assignee: Time Chemical Co Ltd
Priority date: 2019-10-31
Filing date: 2019-10-31
Publication date: 2020-08-04
Anticipated expiration: 2029-10-31

Abstract

The utility model discloses a trifluromethanesulfonic acid reation kettle material lifting device, which comprises a bracket, the upper surface of support is provided with storage case and reation kettle respectively, just the storage case is located one side of reation kettle, the side surface of support is fixedly connected with the installation base, the upper surface of installation base is connected with the water pump base, the upper surface of water pump base is installed with the water pump, the one end of water pump is connected with the conveying hose, the one end of conveying hose is connected with the ejection of compact hard tube, the conveying hose is kept away from the one end of ejection of compact hard tube and is connected with the storage case, the ejection of compact hard tube passes the top of reation kettle and gets into the inside of reation kettle; the utility model discloses in, through ejection of compact hard tube and the sleeve pipe that sets up, the cooperation through helical gear A, helical gear B and screw thread drives the sleeve pipe and rotates and drive ejection of compact hard tube and reciprocate, adjusts the height of nozzle to make nozzle spun material can fully integrate into reation kettle, save the time of stirring, promote production efficiency.

Description

Material lifting device of trifluoromethanesulfonic acid reaction kettle

Technical Field

The utility model belongs to the technical field of trifluoromethanesulfonic acid reation kettle, concretely relates to trifluoromethanesulfonic acid reation kettle material hoisting device.

Background

Trifluoromethanesulfonic acid, also known as trifluoromethanesulfonic acid, a very strong organic acid of the formula CF₃SO₃H, easy to dissolve in water and low in toxicity. The super-strong acid has wide application, is one of the known super-strong acids, and is a universal synthesis tool. The corrosion-resistant and hygroscopic material has strong corrosivity and hygroscopicity, can be widely applied to industries such as medicines and chemical engineering, has small dosage, strong acidity and stable property, can replace traditional inorganic acid such as sulfuric acid and hydrochloric acid in many occasions, and plays a role in optimizing and improving the process. Triflic acid is one of the most strong organic acids and contact with the eye will cause severe eye burns, possibly blindness. Contact with the skin can cause severe chemical burns, and even with a small number of operations, it is necessary to equip them with appropriate protective equipment (such as goggles, acid and alkali resistant gloves, gas masks). The addition of triflic acid to a polar solvent gives an exotherm due to dissolution which is similar to the effect of dissolving sulphuric acid in water. However, dissolving it in a polar solvent is inherently more dangerous than dissolving sulfuric acid in water, and the strong exotherm can cause volatilization and even explosion of the solvent. Therefore, dissolving a large amount of trifluoromethanesulfonic acid in an organic solvent should be avoided. When this is indeed required, it is imperative to control the rate of addition and ensure adequate stirring, good ventilation and, possibly, cooling of the exchanger, as much as possible of the heat generated is removed. The existing trifluoromethanesulfonic acid can only enter the upper part of a reaction kettle in the manufacturing process, so that the materials cannot be fully fused, more time for stirring is needed, and the production efficiency is influenced.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a trifluoromethanesulfonic acid reation kettle material hoisting device to the trifluoromethanesulfonic acid that provides in solving above-mentioned background art can only get into reation kettle's upper portion at the preparation in-process material, makes the material can't obtain fully to merge, need spend more time stirring, never influences the production efficiency problem.

In order to achieve the above object, the utility model provides a following technical scheme: a trifluromethanesulfonic acid reation kettle material lifting device comprises a support, wherein the upper surface of the support is respectively provided with a storage box and a reaction kettle, the storage box is positioned on one side of the reaction kettle, the side surface of the support is fixedly connected with an installation base, the upper surface of the installation base is connected with a water pump base, the upper surface of the water pump base is provided with a water pump, one end of the water pump is connected with a material conveying hose, one end of the material conveying hose is connected with a material discharging hard pipe, one end of the material conveying hose, which is far away from the material discharging hard pipe, is connected with the storage box, the material discharging hard pipe penetrates through the top of the reaction kettle to enter the reaction kettle, the outer surface of the material discharging hard pipe is provided with threads, the outer surface of the material discharging hard pipe is sleeved with a sleeve, the inner wall of the sleeve is provided with thread grooves matched with the threads, and the sleeve and the material discharging, the utility model discloses a reactor, including a reaction kettle, sheathed tube lower extreme, sleeve pipe support, bearing, sleeve pipe support, bearing, casing.

Preferably, an I-shaped isolation column is installed inside the bottom end of the water pump base, a buffer ring is installed between the I-shaped isolation column and the installation base, and a cross screw is installed at the connection position of the water pump base and the I-shaped isolation column.

Preferably, the I-shaped isolation column and the buffer ring are rubber components, and the water pump base and the mounting base are fixed by inserting cross screws through the I-shaped isolation column and the buffer ring into the mounting base.

Preferably, the nozzle is installed to the bottom of ejection of compact hard tube, the upper surface of nozzle is connected with nozzle holder, ejection of compact hard tube and nozzle carry out the rotation through the bearing in the nozzle holder and are connected.

Preferably, the discharge hard pipe is hermetically connected with the sleeve, and the inner walls of the discharge hard pipe and the sleeve are coated with corrosion-resistant coatings.

Preferably, one end of the connecting rod penetrates through the inner wall of the reaction kettle and is rotatably connected through a bearing.

Compared with the prior art, the beneficial effects of the utility model are that:

1. the utility model discloses in, through ejection of compact hard tube and the sleeve pipe that sets up, the cooperation through helical gear A, helical gear B and screw thread drives the sleeve pipe and rotates and drive ejection of compact hard tube and reciprocate, adjusts the height of nozzle to make nozzle spun material can fully integrate into reation kettle, save the time of stirring, promote production efficiency.

2. The utility model discloses in, through "worker" type insulated column and the buffering ring that sets up for motor base can be unsettled, and the vibrations that produce when the motor rotates can not directly transmit for the support, plays the cushioning effect, makes the water pump can the steady operation.

Drawings

Fig. 1 is a schematic view of the structure of the present invention;

FIG. 2 is a schematic front sectional view of the present invention;

fig. 3 is the structural schematic diagram of the water pump base of the present invention.

In the figure: 1. a support; 2. a material storage box; 3. a reaction kettle; 4. installing a base; 5. a water pump base; 6. A water pump; 7. a delivery hose; 8. discharging the hard pipe; 9. a sleeve; 10. a bearing; 11. a cannula holder; 12. A bevel gear A; 13. a bevel gear B; 14. a connecting rod; 15. rotating the handle; 16. a thread; 17. a nozzle; 18. a cross screw; 19. i-shaped isolation columns; 20. and a buffer ring.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-3, the utility model provides a technical solution of a triflic acid reaction kettle material lifting device: a trifluromethanesulfonic acid reaction kettle material lifting device comprises a support 1, wherein a storage box 2 and a reaction kettle 3 are respectively arranged on the upper surface of the support 1, the storage box 2 is positioned on one side of the reaction kettle 3, an installation base 4 is fixedly connected to the side surface of the support 1, a water pump base 5 is connected to the upper surface of the installation base 4, a water pump 6 is installed on the upper surface of the water pump base 5, one end of the water pump 6 is connected with a material conveying hose 7, one end of the material conveying hose 7 is connected with a material discharging hard pipe 8, one end, far away from the material discharging hard pipe 8, of the material conveying hose 7 is connected with the storage box 2, the material discharging hard pipe 8 penetrates through the top of the reaction kettle 3 to enter the inside of the reaction kettle 3, a thread 16 is arranged on the outer surface of the material discharging hard pipe 8, a sleeve 9 is sleeved on the outer surface of the material discharging hard pipe 8, a thread groove matched with the thread 16 is arranged on the inner wall of, make ejection of compact hard tube 8 can reciprocate, the lower extreme of sleeve pipe 9 is provided with bearing 10, the external connection of bearing 10 has sleeve pipe support 11, the both ends of sleeve pipe support 11 and reation kettle 3's inner wall fixed connection, and bearing 10 is located sleeve pipe support 11's inside near intermediate position department, make sleeve pipe 9 can stable work, sleeve pipe 9 rotates through bearing 10 with sleeve pipe support 11 and is connected, sleeve pipe 9's upper end fixedly connected with helical gear A12, one side of helical gear A12 is connected with helical gear B13, and helical gear A12 is connected through tooth meshing with helical gear B13, make helical gear A12 helical gear B13 linkage, one side fixedly connected with connecting rod 14 of helical gear B13, the one end fixedly connected with rotation handle 15 of keeping away from helical gear B13 on connecting rod 14, can conveniently rotate helical gear B13.

Furthermore, an I-shaped isolation column 19 is installed inside the bottom end of the water pump base 5, a buffer ring 20 is installed between the I-shaped isolation column 19 and the installation base 4, and a cross screw 18 is installed at the connection position of the water pump base 5 and the I-shaped isolation column 19, so that the water pump 6 can be stable in operation.

Further, nozzle 17 is installed to ejection of compact hard tube 8's bottom, and nozzle 17's upper surface is connected with the nozzle holder, and ejection of compact hard tube 8 rotates through the bearing in the nozzle holder with nozzle 17 to be connected for nozzle 17 can not rotate, can steady operation.

Further, the discharge hard pipe 8 is hermetically connected with the sleeve 9, and the inner walls of the discharge hard pipe 8 and the sleeve 9 are coated with corrosion-resistant coatings, so that the material cannot leak, and the discharge hard pipe 8 and the sleeve 9 are protected from corrosion.

Further, one end of the connecting rod 14 penetrates through the inner wall of the reaction kettle 3 and is rotatably connected through a bearing, so that the connecting rod 14 can be stable when rotating.

Furthermore, the I-shaped isolation column 19 and the buffering ring 20 are rubber components, and the water pump base 5 and the mounting base 4 are embedded into the mounting base 4 through the I-shaped isolation column 19 and the buffering ring 20 through the cross screw 18 for fixing, so that the water pump base 5 and the mounting base 4 are fixed together, the water pump 6 plays a role in damping during working, and the stability during working is improved.

The utility model discloses a theory of operation and use flow: the utility model discloses after the installation, through starting water pump 6, it passes through conveying hose 7 and ejection of compact hard tube 8 to drive the material, enter into reation kettle 3's inside, through rotating rotatory handle 15, it rotates to drive connecting rod 14, then make bevel gear B13 that links together rotate, through the insection, make bevel gear A12 linkage, make the sleeve 9 that links together simultaneously rotate, when sleeve 9 rotates, through the screw thread 16 that sets up, make ejection of compact hard tube 8 rise or descend, thereby make the nozzle 17 of connecting in ejection of compact hard tube 8 bottom can adjust the height, make the material can fully enter into reation kettle 3's inside, make the material fully fuse, never promote production efficiency.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a trifluoromethanesulfonic acid reation kettle material hoisting device, includes support (1), its characterized in that: the upper surface of the support (1) is respectively provided with a storage box (2) and a reaction kettle (3), the storage box (2) is positioned on one side of the reaction kettle (3), the side surface of the support (1) is fixedly connected with an installation base (4), the upper surface of the installation base (4) is connected with a water pump base (5), the upper surface of the water pump base (5) is provided with a water pump (6), one end of the water pump (6) is connected with a material conveying hose (7), one end of the material conveying hose (7) is connected with a material discharging hard pipe (8), one end of the material conveying hose (7) far away from the material discharging hard pipe (8) is connected with the storage box (2), the material discharging hard pipe (8) penetrates through the top of the reaction kettle (3) to enter the inside of the reaction kettle (3), the outer surface of the material discharging hard pipe (8) is provided with threads (16), and the outer surface of the material discharging hard pipe (8) is sleeved with, the inner wall of the sleeve (9) is provided with a thread groove matched with the thread (16), the sleeve (9) and the discharge hard tube (8) are rotationally connected with the thread (16) through the thread groove formed in the inner wall of the sleeve (9), the lower end of the sleeve (9) is provided with a bearing (10), the outer part of the bearing (10) is connected with a sleeve support (11), two ends of the sleeve support (11) are fixedly connected with the inner wall of the reaction kettle (3), the bearing (10) is positioned inside the sleeve support (11) and close to the middle position, the sleeve (9) is rotationally connected with the sleeve support (11) through the bearing (10), the upper end of the sleeve (9) is fixedly connected with a helical gear A (12), one side of the helical gear A (12) is connected with a helical gear B (13), and the helical gear A (12) is meshed with the helical gear B (13), one side fixedly connected with connecting rod (14) of helical gear B (13), the one end fixedly connected with rotation handle (15) of keeping away from helical gear B (13) on connecting rod (14).

2. The triflic acid reaction kettle material lifting device of claim 1, which is characterized in that: an I-shaped isolation column (19) is installed inside the bottom end of the water pump base (5), a buffer ring (20) is installed between the I-shaped isolation column (19) and the installation base (4), and a cross screw (18) is installed at the connection position of the water pump base (5) and the I-shaped isolation column (19).

3. The triflic acid reaction kettle material lifting device as claimed in claim 2, which is characterized in that: the I-shaped isolation column (19) and the buffer ring (20) are rubber components, and the water pump base (5) and the mounting base (4) are fixed by penetrating the I-shaped isolation column (19) and the buffer ring (20) into the mounting base (4) through cross screws (18).

4. The triflic acid reaction kettle material lifting device of claim 1, which is characterized in that: nozzle (17) are installed to the bottom of ejection of compact hard tube (8), the upper surface connection of nozzle (17) has nozzle holder, ejection of compact hard tube (8) rotate with nozzle (17) through the bearing in the nozzle holder and are connected.

5. The triflic acid reaction kettle material lifting device of claim 1, which is characterized in that: the discharging hard tube (8) is connected with the sleeve (9) in a sealing mode, and corrosion-resistant coatings are coated on the inner walls of the discharging hard tube (8) and the sleeve (9).

6. The triflic acid reaction kettle material lifting device of claim 1, which is characterized in that: one end of the connecting rod (14) penetrates through the inner wall of the reaction kettle (3) and is rotatably connected through a bearing.