CN211097690U - Primary alcohol precipitation device for safflower concentrated solution - Google Patents

Primary alcohol precipitation device for safflower concentrated solution Download PDF

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Publication number
CN211097690U
CN211097690U CN201921374214.XU CN201921374214U CN211097690U CN 211097690 U CN211097690 U CN 211097690U CN 201921374214 U CN201921374214 U CN 201921374214U CN 211097690 U CN211097690 U CN 211097690U
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China
Prior art keywords
alcohol precipitation
valve
precipitation tank
safflower
wall
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CN201921374214.XU
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Chinese (zh)
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杨鹏军
林志展
刘俊
王若飞
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Jiangsu Utions Technology Co ltd
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Jiangsu Utions Technology Co ltd
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Abstract

The utility model relates to a safflower concentrate processing technology field, in particular to a safflower concentrate one-time alcohol precipitation device, which solves the problem of poor alcohol precipitation effect of safflower concentrate caused by the incapability of accurately controlling the temperature and the amount of added ethanol in the prior art, and comprises an alcohol precipitation tank with an operation panel, wherein the alcohol precipitation tank is internally provided with a stirring rod, and the outer wall of the alcohol precipitation tank is respectively provided with a frozen water outlet valve, a cleaning fluid inlet valve, a concentrate inlet valve, a supernatant outlet valve, a frozen water inlet valve, an emptying valve and a vacuum pumping valve, and the bottom of the alcohol precipitation tank is provided with a blow-off pipe, the inner wall of the alcohol precipitation tank is provided with a first temperature sensor, and an ethanol inlet seat is welded on one side of the upper wall of the alcohol precipitation tank, compared with the prior art, the utility model improves the effect of safflower concentrate, and greatly improves the production efficiency thereof, but also greatly reduces the production cost.

Description

Primary alcohol precipitation device for safflower concentrated solution
Technical Field
The utility model relates to a safflower concentrate processing technology field especially relates to a safflower concentrate once alcohol precipitation device.
Background
After the installation and debugging are completed, workers can carry out primary alcohol precipitation on the safflower concentrated solution through hot ethanol and cold ethanol according to the production process requirements so as to meet the primary alcohol precipitation production process requirements of the safflower concentrated solution.
The existing primary alcohol precipitation equipment for the safflower concentrated solution mainly adopts manual field control, and only adopts a quantitative ethanol adding mode to carry out alcohol precipitation, so that the temperature and the amount of added ethanol cannot be accurately controlled, the optimal alcohol precipitation effect of the safflower concentrated solution cannot be realized, and great influence is generated on production.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the problem that the alcohol precipitation effect of the safflower concentrated solution is poor because the temperature and the amount of adding ethanol can not be accurately controlled, and the proposed alcohol precipitation device of the safflower concentrated solution is once.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
a primary alcohol precipitation device for a safflower concentrated solution comprises an alcohol precipitation tank with an operation panel, wherein a stirring rod is arranged inside the alcohol precipitation tank, and the outer wall of the alcohol precipitation tank is respectively provided with a chilled water outlet valve, a cleaning fluid inlet valve, a concentrated solution inlet valve, a supernatant liquid outlet valve, a chilled water inlet valve, an emptying valve and a vacuum pumping valve, and the bottom of the alcohol precipitation tank is provided with a blow-off pipe, the inner wall of the alcohol precipitation tank is provided with a first temperature sensor, an ethanol inlet seat is welded on one side of the upper wall of the alcohol precipitation tank, the upper part of the ethanol inlet seat is connected with a liquid storage tank with a second temperature sensor through a connecting pipe, a liquid inlet flowmeter is arranged on the inner wall of the connecting pipe, the upper end of the liquid storage tank is connected with an ethanol inlet pipe, a temperature control chassis is arranged at the bottom end inside the liquid storage tank, an electromagnetic valve is arranged in the middle of the temperature control chassis, and a heating coil and a condensing coil of an annular structure are respectively arranged in the temperature control chassis.
Preferably, the chilled water liquid outlet valve is arranged above the chilled water liquid inlet valve, and the operating panel is arranged on the side wall of the alcohol precipitation tank through a screw.
Preferably, there is a stirring motor through bolt fixed mounting in the middle of the top of alcohol precipitation jar, and the top of puddler is connected fixedly through shaft coupling and stirring motor's output.
Preferably, the blow-off pipe and the alcohol precipitation tank are arranged integrally, and a blow-off valve is arranged on the side wall of the blow-off pipe.
Preferably, the second temperature sensor is embedded in the inner wall of the liquid storage tank, and the temperature control chassis is fixed to the inner wall of the liquid storage tank through welding.
Preferably, the total area of the region in which the heating coil is located is equal to the area of the region in which the condensing coil is located.
Compared with the prior art, the utility model discloses a set up temperature sensor in alcohol precipitation jar and monitor jar internal temperature to set up the feed liquor flowmeter at the ethanol feeding department and monitor the volume that the ethanol adds, thereby carry out accurate temperature control and volume's control to the ethanol that adds, improved the alcohol precipitation effect of safflower concentrate, promoted its production efficiency by a wide margin; in addition, in the ethanol adding process, the heating coil and the condensing coil are made into an annular structure and are arranged at the bottom of the liquid storage tank, so that an operator can conveniently adjust the cold and hot degrees when the ethanol is added, and compared with the method of respectively arranging the cold ethanol pipe and the hot ethanol pipe, the production cost is greatly reduced.
Drawings
Fig. 1 is a schematic structural view of a primary alcohol precipitation device for a safflower concentrate provided by the utility model;
fig. 2 is a schematic view of an ethanol feeding structure of a primary alcohol precipitation device for a safflower concentrate provided by the utility model;
fig. 3 is the structural schematic diagram of the temperature control chassis of the primary alcohol precipitation device for the safflower concentrated solution provided by the utility model.
In the figure: 1 alcohol precipitation jar, 11 first temperature sensor, 12 refrigerated water play liquid valves, 13 washing liquid feed valves, 14 concentrate feed liquor valves, 15 supernatant play liquid valves, 16 refrigerated water feed liquor valves, 17 blow off pipes, 18 blow off valves, 19 ethanol feed liquor seats, 2 ethanol feed liquor pipes, 3 liquid storage tanks, 31 second temperature sensor, 32 liquid inlet flow meter, 4 temperature control chassis, 41 heating coil, 42 condensing coil.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-3, a safflower concentrate primary alcohol precipitation device, including alcohol precipitation tank 1 with operation panel, there is a stirring motor fixed on the middle of the top of alcohol precipitation tank 1 through a bolt, the stirring motor is used to drive a stirring rod to stir the solution in alcohol precipitation tank 1, the top of the stirring rod is connected and fixed with the output end of the stirring motor through a shaft coupling, and the stirring rod is arranged in alcohol precipitation tank 1, and the outer wall of alcohol precipitation tank 1 is respectively provided with a chilled water outlet valve 12, a cleaning fluid inlet valve 13, a concentrate inlet valve 14, a supernatant outlet valve 15, a chilled water inlet valve 16, an emptying valve and a vacuum pumping valve, the chilled water outlet valve 12 is arranged above the chilled water inlet valve 16, the operation panel is arranged on the side wall of alcohol precipitation tank 1 through a screw, and the bottom of alcohol precipitation tank 1 is provided with a blow-off pipe 17, the blow-off pipe 17 is used for blow-off, the blow-off pipe 17 and the alcohol precipitation tank 1 are arranged integrally, a blow-off valve 18 is arranged on the side wall of the blow-off pipe 17, a first temperature sensor 11 (model Pt100) is arranged on the inner wall of the alcohol precipitation tank 1, the first temperature sensor 11 is used for monitoring the temperature in the alcohol precipitation tank 1, an ethanol liquid inlet seat 19 is welded on one side of the upper wall of the alcohol precipitation tank 1, the upper part of the ethanol liquid inlet seat 19 is connected with a liquid storage tank 3 through a connecting pipe, the liquid storage tank 3 is used for conveniently heating and cooling the ethanol solution in the liquid storage tank 3, a second temperature sensor 31 (model Pt100) is embedded in the inner wall of the liquid storage tank 3, the second temperature sensor 31 is used for measuring the temperature of the ethanol in the liquid storage tank 3, a liquid inlet flow meter 32 (model SG-NZ-KD1) is arranged on the inner wall of the connecting pipe, an ethanol liquid inlet pipe 2 is connected to, the middle of control by temperature change chassis 4 is provided with the solenoid valve (model SJ2000), and the solenoid valve is used for controlling whether the ethanol falls down to control by temperature change chassis 4's inside still is provided with annular structure's heating coil 41 and condensing coil 42 respectively, and the total area in heating coil 41 place region equals the area in condensing coil 42 place region, and control by temperature change chassis 4 is used for heating or cooling the ethanol.
In this embodiment, the first alcohol precipitation step of the safflower concentrate is as follows:
1. starting a stirring motor to control a stirring rod to work, closing an emptying valve, starting a concentrated solution inlet valve 14, starting a vacuumizing valve, and starting to suck the safflower concentrated solution into the alcohol precipitation tank 1 in vacuum;
2. adding hot ethanol: inputting the alcohol adding amount, the alcohol adding time and the temperature of the required hot ethanol on an operation panel, starting an ethanol liquid inlet pipe 2 according to the set alcohol adding amount and the set alcohol adding time, enabling the ethanol to enter a liquid storage tank 3, starting a heating coil 41 to heat the ethanol, automatically stopping heating the heating coil 41 when the ethanol is heated to the set temperature, starting a solenoid valve to be opened, enabling the hot ethanol to fall into an alcohol precipitation tank 1 from an ethanol liquid inlet seat 19 along a connecting pipe, and closing the ethanol liquid inlet pipe 2 after a liquid inlet flow meter 32 displays that data reaches a set value along with the continuous addition of the hot ethanol;
3. adding cold ethanol: inputting the alcohol adding amount, the alcohol adding time and the temperature of the required cold ethanol on an operation panel, opening an ethanol liquid inlet pipe 2 according to the set alcohol adding amount and the set alcohol adding time, enabling the ethanol to enter a liquid storage tank 3, starting a condensing coil 42 to work, cooling the ethanol, automatically stopping cooling the condensing coil 42 when the temperature is reduced to the set temperature, starting and opening a solenoid valve, enabling the cold ethanol to fall into an alcohol precipitation tank 1 from an ethanol liquid inlet seat 19 along a connecting pipe, and closing the ethanol liquid inlet pipe 2 after a liquid inlet flow meter 32 displays that data reaches a set value along with the continuous addition of the cold ethanol;
4. mixing: stopping the stirring motor when the built-in timer in the operation panel reaches the set mixing time and the mixing is finished;
5. standing: opening a chilled water outlet valve 12 and a chilled water inlet valve 16, and closing the chilled water outlet valve 12 and the chilled water inlet valve 16 when the temperature detected by a first temperature sensor 11 in the alcohol precipitation tank 1 is reduced to a set standing temperature (wherein stirring is strictly prohibited during standing);
6. when the standing time reaches a set value, finishing the standing;
7. opening an emptying valve of the alcohol precipitation tank 1, opening a supernatant liquid outlet valve 15, and starting to discharge liquid;
8. after the liquid is discharged, closing the supernatant liquid outlet valve 15, opening the drain valve 18, and opening the drain pipe 17 to discharge the slag;
9. after the slag is discharged, closing the drain valve 18, opening the cleaning liquid inlet valve 13, adding a certain amount of cleaning liquid, starting the stirring motor to control stirring, and starting a cleaning program;
10. closing the cleaning solution inlet valve 13, after cleaning, closing the stirring motor, opening the blow-down valve 18 to open the blow-down pipe 17, and starting a blow-down procedure;
11. and after the blowdown is finished, closing the blowdown valve 18, and finishing the primary alcohol precipitation of the safflower concentrated solution.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims (6)

1. A primary alcohol precipitation device for a safflower concentrated solution comprises an alcohol precipitation tank (1) with an operation panel, wherein a stirring rod is arranged inside the alcohol precipitation tank (1), the outer wall of the alcohol precipitation tank (1) is provided with a chilled water outlet valve (12), a cleaning solution inlet valve (13), a concentrated solution inlet valve (14), a supernatant liquid outlet valve (15), a chilled water inlet valve (16), an emptying valve and a vacuum pumping valve respectively, and the bottom of the alcohol precipitation tank (1) is provided with a blow-off pipe (17), and is characterized in that the inner wall of the alcohol precipitation tank (1) is provided with a first temperature sensor (11), an alcohol inlet seat (19) is welded on one side of the upper wall of the alcohol precipitation tank (1), the upper part of the alcohol inlet seat (19) is connected with a liquid storage tank (3) with a second temperature sensor (31) through a connecting pipe, the inner wall of the connecting pipe is provided with a liquid inlet flowmeter (32), and the upper end of the liquid storage tank (3), and a temperature control chassis (4) is installed at the bottom end of the interior of the liquid storage tank (3), an electromagnetic valve is arranged in the middle of the temperature control chassis (4), and a heating coil (41) and a condensing coil (42) which are of annular structures are respectively arranged in the temperature control chassis (4).
2. The primary alcohol precipitation device for the safflower concentrate as claimed in claim 1, wherein the chilled water outlet valve (12) is installed above the chilled water inlet valve (16), and the operation panel is installed on the side wall of the alcohol precipitation tank (1) through screws.
3. The primary alcohol precipitation device for the safflower concentrated solution according to claim 1, characterized in that a stirring motor is fixedly installed in the middle of the top of the alcohol precipitation tank (1) through a bolt, and the top of a stirring rod is fixedly connected with the output end of the stirring motor through a coupler.
4. The primary alcohol precipitation device of the safflower concentrate as claimed in claim 1, characterized in that the blow-off pipe (17) and the alcohol precipitation tank (1) are integrally arranged, and a blow-off valve (18) is arranged on the side wall of the blow-off pipe (17).
5. The primary alcohol precipitation device for the safflower concentrate as claimed in claim 1, wherein the second temperature sensor (31) is embedded in the inner wall of the liquid storage tank (3), and the temperature control chassis (4) is fixed with the inner wall of the liquid storage tank (3) by welding.
6. The primary alcohol precipitation device of safflower concentrate of claim 1, characterized in that, the total area of the area that heating coil (41) is located is equal to the area of the area that condensing coil (42) is located.
CN201921374214.XU 2019-08-23 2019-08-23 Primary alcohol precipitation device for safflower concentrated solution Active CN211097690U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921374214.XU CN211097690U (en) 2019-08-23 2019-08-23 Primary alcohol precipitation device for safflower concentrated solution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921374214.XU CN211097690U (en) 2019-08-23 2019-08-23 Primary alcohol precipitation device for safflower concentrated solution

Publications (1)

Publication Number Publication Date
CN211097690U true CN211097690U (en) 2020-07-28

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201921374214.XU Active CN211097690U (en) 2019-08-23 2019-08-23 Primary alcohol precipitation device for safflower concentrated solution

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CN (1) CN211097690U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113521801A (en) * 2021-07-30 2021-10-22 山东明仁福瑞达制药股份有限公司 Device for separating and purifying traditional Chinese medicine components in alcohol precipitation tank, method and application thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113521801A (en) * 2021-07-30 2021-10-22 山东明仁福瑞达制药股份有限公司 Device for separating and purifying traditional Chinese medicine components in alcohol precipitation tank, method and application thereof

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