SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide an extraction system that can draw automatically, this extraction system can be used to carry out the automation to pharmaceutical composition and draw.
To achieve the purpose, the utility model adopts the following technical proposal:
an extraction system comprising an extraction bottle, further comprising:
a water bath extraction process line comprising a water bath extraction device for water bath extraction;
an ultrasonic extraction process line comprising an ultrasonic extraction device for ultrasonic extraction;
a labeling mechanism for labeling the extraction bottle with an identification label; and
a screening mechanism configured to enable screening of the extraction bottles to corresponding extraction process lines according to the identification tags on the extraction bottles.
In one embodiment, the water bath extraction device comprises a water bath device, a condensation pipe, a fixing frame and a driving mechanism, wherein the fixing frame comprises a supporting frame and a mounting frame used for fixing the condensation pipe and the extraction bottle, the mounting frame is arranged on the supporting frame and connected with the driving mechanism, the driving mechanism is configured to be capable of driving the mounting frame to drive the condensation pipe and the extraction bottle to move left and right and up and down on the supporting frame, and the water bath device is arranged below the mounting frame.
In one embodiment, the support frame is provided with a transmission line for transmitting the extraction bottles, the water bath extraction device further comprises a first manipulator and a second manipulator for connecting the extraction bottles between the transmission line and the mounting frame, the first manipulator is arranged on the mounting frame, and the second manipulator is arranged on the support frame.
In one embodiment, the mounting frame is provided with a clamping mechanism for clamping and fixing the condenser pipe, the clamping mechanism comprises a clamping jaw and a clamping jaw tightness driving unit, the clamping jaw tightness driving unit is connected with the clamping jaw and can drive the clamping jaw to clamp the condenser pipe and loosen the condenser pipe.
In one embodiment, the water bath extraction device further comprises a detection sensor for detecting the combination condition of the condensation pipe and the extraction bottle.
In one embodiment, the water bath extraction device further comprises a condenser pipe cleaning mechanism, the condenser pipe cleaning mechanism comprises a first spray head capable of spraying cleaning agent to clean the condenser pipe and a liquid receiving disc used for collecting waste liquid generated by cleaning the condenser pipe, and the first spray head is mounted on the mounting frame.
In one embodiment, the condenser tube cleaning mechanism further comprises a second spray head mounted on the mounting frame, the second spray head being configured to spray gas to dry the condenser tube.
In one embodiment, the first spray head and/or the second spray head are/is rotatably arranged on the mounting frame; or,
the quantity of mounting bracket is a plurality of, and is a plurality of the mounting bracket sets up side by side on the support frame, every correspond on the mounting bracket and be equipped with first shower nozzle.
In one embodiment, the condenser tube cleaning mechanism further comprises a driving device connected with the liquid receiving disc and used for driving the liquid receiving disc to move.
In one embodiment, the extraction system further comprises a frame, and the water bath extraction process line and the ultrasonic extraction process line are both arranged on the frame;
still be equipped with in the frame:
the storage area is used for storing the standby extraction bottles;
the liquid injection plugging area is provided with a liquid injection plugging device, and the liquid injection plugging device is used for injecting an extraction solvent into the extraction bottle and plugging the extraction bottle after the extraction solvent is injected; and
and the standing waiting area is used for temporarily storing the extraction bottle after extraction is finished.
The utility model discloses following beneficial effect has at least:
the extraction system of the utility model has a plurality of extraction modes, and can simultaneously carry out a plurality of extraction processes; can control the operating condition of screening mechanism, labelling mechanism, supersound extraction element and water bath extraction element through the controller during the use, can label automatically, autofilter and automatic extraction, realize extracting process's automation and go on, convenient control and control are more accurate, fully liberate the manpower, and help improving work efficiency.
Detailed Description
In order to facilitate understanding of the present invention, the present invention will be described more fully hereinafter with reference to the accompanying drawings. Preferred embodiments of the present invention are shown in the drawings. The invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
It should be noted that when a portion is referred to as being "secured to" another portion, it can be directly on the other portion or there can be an intervening portion. When a portion is said to be "connected" to another portion, it may be directly connected to the other portion or intervening portions may be present. The terms "vertical," "horizontal," "left," "right," and the like as used herein are for illustrative purposes only and do not denote a unique embodiment.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
The embodiment discloses an extraction system, which can be applied to extraction processes in the fields of chemical engineering, pharmacy and the like, such as extraction of medicinal components (including but not limited to extraction of traditional Chinese medicine components).
Referring to fig. 1 to 9, the extraction system includes an extraction bottle 30, a water bath extraction process line, an ultrasonic extraction process line, a labeling mechanism, and a screening mechanism; wherein the water bath extraction process line comprises a water bath extraction device for water bath extraction; the ultrasonic extraction process line includes an ultrasonic extraction device 80 for ultrasonic extraction; the labeling mechanism is used for labeling the identification label on the extraction bottle 30; the sifting mechanism is configured to be able to sift the extraction bottles 30 to the corresponding extraction process line according to the identification tags on the extraction bottles 30.
Further, the extraction system further comprises a controller, wherein the controller is respectively electrically connected with the screening mechanism, the labeling mechanism, the ultrasonic extraction device 80 and the water bath extraction device and can control the working states of the screening mechanism, the labeling mechanism, the ultrasonic extraction device 80 and the water bath extraction device. Can control the operating condition of screening mechanism, labelling mechanism, supersound extraction element 80 and water bath extraction element through the controller during the use, can label automatically, autofilter and automatic extraction, realized that multiple mode of extraction draws and the automation of drawing technology goes on, convenient control and control are more accurate, fully liberate the manpower, and help improving work efficiency.
As shown in fig. 1, the extraction system further includes a rack 100, and both the water bath extraction process line and the ultrasonic extraction process line are disposed on the rack 100. Further, the rack 100 is further provided with a storage area 110, a liquid injection and plugging area 120 and a standing waiting area 130; wherein, the storage area 110 is used for storing the standby extraction bottles 30; the liquid injection plugging area 120 is used for injecting the extraction solvent into the extraction bottle 30 and plugging the extraction bottle 30 filled with the extraction solvent; the waiting area 130 that stews is used for keeping in and accomplishes the bottle 30 that draws after drawing, deposits district 110, annotates liquid and adds stopper district 120 and the overall arrangement mode of waiting area 130 that stews on frame 100 can set up according to the actual demand, the utility model discloses do not do the restriction to this to make things convenient for whole drawing going on of technology to be the main can.
Specifically, annotate liquid area 120 that plugs and be equipped with and annotate liquid device that plugs, annotate liquid device that plugs and include annotating liquid equipment and the equipment that plugs, pour into extraction solvent to extracting bottle 30 through annotating liquid equipment, annotate extraction solvent after annotating liquid equipment to extracting bottle 30 and to extracting bottle 30 through the equipment that plugs and plug, the bottleneck stopper that will extract bottle 30 promptly is lived to the bottle plug to prevent to extract the solvent loss in the bottle 30. Optionally, the liquid injection device and the plugging device are respectively connected with the controller, and can automatically add liquid and automatically plug under the control of the controller, so that automation is realized.
When the extraction system is in operation, the extraction bottles 30 stored in the storage area 110 are transported to the filling and plugging area 120, and the extraction solvent is filled and plugged in the filling and plugging area 120; conveying the extraction bottle 30 subjected to liquid injection and plugging to a labeling mechanism, and labeling the extraction bottle 30 by the labeling mechanism, wherein the labels comprise a water bath extraction label and an ultrasonic extraction label; then screening the extraction bottles 30 with the labels attached through a screening mechanism, wherein the extraction bottles 30 with the water bath extraction labels attached are screened and sent to a water bath extraction process line, and are subjected to water bath extraction by a water bath extraction device, while the extraction bottles 30 with the ultrasonic extraction labels attached are screened and sent to an ultrasonic extraction process line, and are subjected to ultrasonic extraction by an ultrasonic extraction device 80; the extraction bottle 30 after the completion of the water bath extraction and the extraction bottle 30 after the completion of the ultrasonic extraction are both sent to the standing waiting area 130 for temporary storage.
In one embodiment, the water bath extraction device comprises a water bath device 10, a condensation pipe 20, a fixing frame 40 and a driving mechanism, wherein the fixing frame 40 comprises a supporting frame 41 and a mounting frame 42 for fixing the condensation pipe 20 and the extraction bottle 30, the mounting frame 42 is arranged on the supporting frame 41 and is connected with the driving mechanism, the driving mechanism is configured to be capable of driving the mounting frame 42 to drive the condensation pipe 20 and the extraction bottle 30 to move left and right and up and down on the supporting frame 41, and the water bath device 10 is arranged below the mounting frame 42. Specifically, the driving mechanism is electrically connected with the controller and can drive the mounting rack 42 to drive the condensation tube 20 and the extraction bottle 30 to move left and right and up and down on the support frame 41 under the control of the controller; the water bath apparatus 10 is electrically connected to a controller, and the operation state of the water bath apparatus 10 can be controlled by the controller.
Specifically, the water bath device 10 includes an electric heater and a water bath, the electric heater may be electrically connected to the controller, the water in the water bath is heated by the electric heater, and the controller controls the temperature of the water in the water bath; the top of the water bath is provided with an opening for the extraction bottle 30 positioned above to enter the water bath for water bath. The mounting rack 42 is driven by the driving mechanism to drive the condensation tube 20 and the extraction bottle 30 to move left and right and up and down on the support rack 41, so that the extraction bottle 30 is aligned with the water bath opening of the water bath device 10, and the extraction bottle 30 smoothly enters the water bath for water bath.
The support frame 41 is a main support member of the entire apparatus for supporting and mounting various components, which are reasonably arranged on the support frame 41, making the entire structure compact. The mounting rack 42 is disposed on the supporting rack 41, and the mounting rack 42 can be driven by a driving mechanism electrically connected with the controller to move the condensation tube 20 and the extraction bottle 30 on the supporting rack 41 to move left and right and up and down to get close to or get away from the water bath apparatus 10.
As shown in fig. 3 and 4, a conveyor line for conveying the extraction bottles 30 is provided on the support frame 41, and the water bath extraction apparatus further includes a first robot 51 and a second robot 52 for transferring the extraction bottles 30 between the conveyor line and the mounting frame 42, wherein the first robot 51 is provided on the mounting frame 42, and the second robot 52 is provided on the support frame 41. Specifically, the first and second manipulators 51 and 52 may be electrically connected to the controller, respectively; the fixed frame 40 further comprises a truss 43, wherein the truss 43 is arranged on the supporting frame 41 and is perpendicular to the mounting frame 42; the truss 43 is provided with a plurality of second robots 52, and the second robot 52 transfers the extraction bottles 30 on the transfer line to the first robot 51 or transfers the extraction bottles 30 held by the first robot 51 to the transfer line.
The mounting bracket 42 is provided with a clamping mechanism for clamping and fixing the condenser tube 20, and as shown in fig. 4 and 5, the clamping mechanism includes a clamping jaw 53 and a clamping jaw tightness driving unit (not shown) connected to the clamping jaw 53, and the clamping jaw tightness driving unit is configured to drive the clamping jaw 53 to clamp and loosen the condenser tube 20. Specifically, the clamping jaw tightness driving unit can be electrically connected with the controller, and the clamping jaw tightness driving unit is controlled by the controller to drive the clamping jaw 53 to clamp the condenser tube 20 and loosen the condenser tube 20. Alternatively, the clamping jaw tightness driving unit may adopt an air cylinder, a hydraulic cylinder, a motor or the like which can directly or indirectly drive the clamping jaw 53 to clamp the condensation pipe 20 and loosen the condensation pipe 20.
Specifically, the quantity of clamping jaw 53 is at least one, specifically can set up according to the actual demand, the utility model discloses do not do too much restriction to this. In view of the fact that the condensation duct 20 is generally in the shape of a long cylinder, it is preferable to provide two or more holding jaws 53 in order to be able to fix the condensation duct 20 more firmly.
As shown in fig. 7 to 9, in some embodiments, the extraction device further comprises a condenser collar 60, wherein the condenser collar 60 is detachably mounted on the distillate outlet end of the condenser tube 20 and can be at least partially inserted into the mouth of the extraction flask 30. Specifically, the outer wall of the condenser collar 60 accommodates the extraction bottle 30 and the inner wall of the condenser collar 60 accommodates the condenser tube 20. When the condenser collar 60 is used to cover the condenser 20, the gap between the condenser 20 and the extraction bottle 30 due to different diameters can be eliminated, so that the condenser 20 can be adapted to the extraction bottle 30 with an enlarged mouth.
Specifically, as shown in fig. 9, the condensation tube sleeve ring 60 includes a channel 61 for the condensation tube 20 to penetrate through, at least two mounting holes 62 penetrating through the side wall are provided on the side wall of the condensation tube sleeve ring 60, the at least two mounting holes 62 are arranged at intervals and respectively communicate with the channel 61, and the condensation tube sleeve ring 60 is fixedly connected with the condensation tube 20 through a fastener penetrating through the mounting holes 62. The installation holes 62 and the fasteners can be used for preventing the relative movement between the condensation pipe lantern ring 60 and the condensation pipe 20, so that the fixed connection between the two is realized; still have easy dismounting, independent assortment's advantage simultaneously, same condenser pipe lantern ring 60 can use with the condenser pipe 20 cooperation of difference, perhaps same condenser pipe 20 can use with the condenser pipe lantern ring 60 cooperation of difference to convenience of customers selects according to particular case.
Preferably, the condenser tube collar 60 is a polytetrafluoroethylene collar and the fasteners are jackscrews. The condenser tube lantern ring 60 is made of polytetrafluoroethylene, and the possibility that the robot damages the condenser tube lantern ring 60 when assembling in the automatic production process can be reduced.
As shown in fig. 9, in the present embodiment, the number of the mounting holes 62 is three, and the three mounting holes 62 are uniformly distributed on the side wall of the condenser tube collar 60 along the circumferential direction of the collar, that is, an included angle between central axes of two adjacent mounting holes 62 is 120 °, so as to better realize the fastening connection between the condenser tube collar 60 and the condenser tube 20.
Further, water bath extraction element is still including being used for detecting condenser pipe 20 and the detection sensor who draws bottle 30 combination condition, detects condenser pipe 20 and the combination condition who draws bottle 30 through detecting the sensor, guarantees that condenser pipe 20 and draw bottle 30 combine to carry out the water bath again after well and draw the work to avoid the water bath to draw the steam leakage of in-process, influence and draw efficiency. Specifically, the detection sensor is electrically connected to the controller.
The water bath extraction apparatus further includes a condenser tube cleaning mechanism, as shown in fig. 2, 3, 4 and 6, which includes a first spray head 70 and a liquid receiving tray for collecting waste liquid generated by cleaning the condenser tube 20, wherein the first spray head 70 is mounted on the mounting bracket 42. Specifically, the first spray head 70 is electrically connected to the controller, and is capable of spraying a cleaning agent to clean the condensation duct 20 under the control of the controller. Above-mentioned condenser pipe wiper mechanism can wash condenser pipe 20 on mounting bracket 42 through the automatic blowout cleaner of controller control installation first shower nozzle 70 on mounting bracket 42 during the use, and the waste liquid that produces after wasing condenser pipe 20 is collected through connecing the liquid dish, has realized the self-cleaning to condenser pipe 20, fully liberates the manpower.
By configuring the mounting rack 42 to be capable of moving up and down relative to the supporting rack 41, the mounting rack 42 can bring the condensation pipes 20 thereon to move up and down to be close to or far away from the liquid receiving tray located below. When in cleaning, the condensing pipe 20 moves downwards to be close to the liquid receiving tray, so that waste liquid generated after the condensing pipe 20 is cleaned during liquid receiving can be prevented from splashing; after cleaning, the condensation pipe 20 is moved upwards to be far away from the liquid receiving plate, so that the liquid receiving plate is convenient to move away.
In one embodiment, the number of the mounting frames 42 is multiple, the mounting frames 42 are arranged on the supporting frame 41 side by side, and the first spray head 70 is correspondingly arranged on each mounting frame 42, so that the plurality of condensation pipes 20 can be cleaned simultaneously, that is, the condensation pipes 20 can be cleaned in batch.
Further, since the condenser tube 20 after cleaning is wet due to the cleaning agent (e.g., water) remaining in the condenser tube 20, in order to accelerate the drying of the condenser tube 20, the condenser tube cleaning mechanism further includes a second spray head (not shown) mounted on the mounting bracket 42, the second spray head being configured to spray gas to dry the condenser tube 20. Specifically, the second nozzle is electrically connected to the controller, and the controller can control the second nozzle to spray air to blow the condensation duct 20. Preferably, in order to accelerate the drying speed, the drying may be performed using a gas having a temperature higher than room temperature. When the number of the mounting brackets 42 is plural, each mounting bracket 42 is correspondingly provided with the second spray head, so that the drying of the plurality of condensation pipes 20 can be simultaneously performed, that is, the condensation pipes 20 are dried in batch.
Optionally, the first spray head 70 and/or the second spray head may be rotatably disposed on the mounting bracket 42. When the condenser tube 20 is cleaned, the first nozzle 70 may be rotated at an angle such that the cleaning agent outlet is adjacent to and aligned with the condenser tube 20, so as to spray the cleaning agent into the condenser tube 20 for cleaning. When it is necessary to dry the condensation duct 20, the second nozzle may be rotated at an angle such that its gas outlet is adjacent to and aligned with the condensation duct 20, so as to spray gas to dry the condensation duct 20. Specifically, the first nozzle 70 and the second nozzle are respectively connected to a driving device, and the driving device can be controlled by the controller to drive the first nozzle 70 and the second nozzle to rotate. Specifically, the driving device may be a motor, an air cylinder, or a hydraulic cylinder, which can directly or indirectly drive the first nozzle 70 and the second nozzle to rotate.
In the embodiment shown in fig. 2 and 6, the condensation pipe 20 is disposed in the middle of the mounting frame 42, the second spray head and the first spray head 70 are disposed on the top of the mounting frame 42, the cleaning agent sprayed from the first spray head 70 cleans the condensation pipe 20 from top to bottom, and the gas sprayed from the second spray head dries the condensation pipe 20 from top to bottom.
Preferably, the drip pan is movably provided on the fixing frame 40 so that the drip pan can be moved to one side for condensation, water bath, etc. using the condensation duct 20 when there is no need to wash the condensation duct 20. In order to further realize automation, the condenser pipe cleaning equipment further comprises a driving device which is connected with the liquid receiving disc and used for driving the liquid receiving disc to move. Specifically, the driving mechanism is electrically connected with the controller, and the driving device is controlled by the controller to drive the liquid receiving disc to move, so that the liquid receiving disc moves to the position below the condensation pipe 20 or moves away from the position below the condensation pipe 20, the condensation pipe 20 is automatically cleaned, and manpower is fully liberated. Specifically, the driving device may be a motor, an air cylinder, a hydraulic cylinder, or the like capable of directly or indirectly driving the liquid receiving tray to move.
In summary, the above extraction system has at least the following advantages: the extraction system has multiple extraction modes and can simultaneously carry out multiple extraction processes; can control the operating condition of screening mechanism, labelling mechanism, supersound extraction element 80 and water bath extraction element through the controller during the use, can label automatically, autofilter and automatic extraction, realized extracting process's automation and gone on, convenient control and control are more accurate, fully liberate the manpower, and help improving work efficiency. The user can preset the technological parameters according to the actual requirements, such as the extraction time, the water bath temperature, the addition amount of the extraction solvent and the like, so as to accurately control the whole extraction process.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only represent some embodiments of the present invention, and the description thereof is specific and detailed, but not to be construed as limiting the scope of the present invention. It should be noted that, for those skilled in the art, without departing from the spirit of the present invention, several variations and modifications can be made, which are within the scope of the present invention. Therefore, the protection scope of the present invention should be subject to the appended claims.