CN210834362U - a gas sampler - Google Patents
a gas sampler Download PDFInfo
- Publication number
- CN210834362U CN210834362U CN201921625972.4U CN201921625972U CN210834362U CN 210834362 U CN210834362 U CN 210834362U CN 201921625972 U CN201921625972 U CN 201921625972U CN 210834362 U CN210834362 U CN 210834362U
- Authority
- CN
- China
- Prior art keywords
- bottle
- pipe
- gas
- bottle body
- stopper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000007788 liquid Substances 0.000 claims abstract description 66
- 238000010521 absorption reaction Methods 0.000 claims abstract description 65
- 241001411320 Eriogonum inflatum Species 0.000 claims abstract description 36
- 238000005273 aeration Methods 0.000 claims abstract description 24
- 238000003760 magnetic stirring Methods 0.000 claims abstract description 15
- 239000011521 glass Substances 0.000 claims abstract description 14
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 47
- 229920005372 Plexiglas® Polymers 0.000 claims description 47
- 239000004575 stone Substances 0.000 claims description 13
- 238000005086 pumping Methods 0.000 claims description 7
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 229910052593 corundum Inorganic materials 0.000 claims description 4
- 239000010431 corundum Substances 0.000 claims description 4
- 229910001651 emery Inorganic materials 0.000 claims description 4
- 239000011148 porous material Substances 0.000 claims description 4
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 4
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 4
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 3
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 3
- 238000005070 sampling Methods 0.000 abstract description 11
- 238000002474 experimental method Methods 0.000 abstract description 8
- 239000002253 acid Substances 0.000 abstract description 2
- 239000003513 alkali Substances 0.000 abstract description 2
- 230000007547 defect Effects 0.000 abstract description 2
- 239000007789 gas Substances 0.000 description 57
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 238000012544 monitoring process Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 210000003437 trachea Anatomy 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- VRZJGENLTNRAIG-UHFFFAOYSA-N 4-[4-(dimethylamino)phenyl]iminonaphthalen-1-one Chemical compound C1=CC(N(C)C)=CC=C1N=C1C2=CC=CC=C2C(=O)C=C1 VRZJGENLTNRAIG-UHFFFAOYSA-N 0.000 description 1
- 241001391944 Commicarpus scandens Species 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
Images
Landscapes
- Sampling And Sample Adjustment (AREA)
Abstract
Description
技术领域technical field
本实用新型属于气体采样器技术领域,具体涉及一种气体采样器。The utility model belongs to the technical field of gas samplers, in particular to a gas sampler.
背景技术Background technique
目前已有的气体采样器多选择玻璃材质的孟式洗瓶作为气体吸收液盛放容器,孟式洗瓶规格较为一致,无法定制,由于多采用玻璃材质,容易破碎,用于野外监测实验时,常常由于操作失误,造成玻璃破碎,导致实验失败。采样时,孟氏洗瓶的进气口和出气口通常需要用硅胶管与采样泵相连,实际操作中,常常因为硅胶管孔径大小不适,造成密封性不严。此外,孟氏洗瓶的曝气头较小,曝气面积有限,抽气采样时,气流快速通过曝气头,会形成巨大的气泡,气泡爆裂时,产生大量的水珠,随气流流失,降低了吸收效率,尤其是当实验需要,抽气速率较高时,气泡爆裂造成吸收液损失量非常大,给实验带入极大的误差;吸收液从瓶口倒出时,人工误差较大,对针对挥发性气体的研究不方便。At present, most of the existing gas samplers choose Meng-type washing bottles made of glass as the container for the gas absorption liquid. The specifications of Meng-type washing bottles are relatively consistent and cannot be customized. Because most of the glass materials are used, it is easy to break. It is used in field monitoring experiments. , Often due to operational errors, the glass is broken, resulting in the failure of the experiment. When sampling, the air inlet and outlet of the Montenegro washing bottle usually need to be connected to the sampling pump with a silicone tube. In actual operation, the sealing performance is often not tight due to the unsuitable aperture of the silicone tube. In addition, the aeration head of the Mengshi bottle is small, and the aeration area is limited. When the air is pumped and sampled, the air flow passes through the aeration head quickly, which will form huge air bubbles. The absorption efficiency is reduced, especially when the pumping rate is high when the experiment is required, the bubble burst causes a very large loss of the absorption liquid, which brings great errors to the experiment; when the absorption liquid is poured out of the bottle, the manual error is large. , it is inconvenient for research on volatile gases.
实用新型内容Utility model content
解决的技术问题:针对现有技术中存在密封性差、曝气面积有限以及实验误差大等技术问题,本实用新型提供一种气体采样器,该采样器具有耐酸碱、坚固耐用、不易破碎、所用曝气头曝气均匀、吸收效率高以及实验精确等优点,弥补了孟氏吸气瓶的缺陷。Technical problems solved: In view of the technical problems of poor sealing, limited aeration area and large experimental errors in the prior art, the utility model provides a gas sampler, which has the characteristics of acid and alkali resistance, sturdiness and durability, and is not easily broken. The advantages of the aeration head used are uniform aeration, high absorption efficiency and accurate experiments, which make up for the defects of the Montenegro aspirating bottle.
技术方案:一种气体采样器,所述采样器包括第一吸收装置、第二吸收装置、吸收液、直通管和集气瓶,所述第一吸收装置包括进气管a、直角气动接头、出气管a、瓶塞a、有机玻璃瓶a、磁力搅拌装置和转子,所述有机玻璃瓶a包括瓶身a、真空抽气支管a、吸收液出口a和橡胶塞,所述瓶身a为底端密封、顶端开口且内部空腔的圆柱体,所述真空抽气支管a设于瓶身a顶部,所述吸收液出口a设于瓶身a底端边缘,所述橡胶塞分别密封真空抽气支管a和吸收液出口a,所述瓶塞a活动连接于瓶身a开口端,用于密封瓶身a;所述进气管a包括管身a和曝气头,所述管身a顶部为圆柱形细管,中部和底部为内径扩大至少2倍的圆柱形粗管,所述曝气头与管身a底端连接,管身a顶部穿过瓶塞a与直角气动接头的一端连接,管身a其余部分设于瓶身a内部,曝气头设于瓶身a底部且与瓶身a底壁不接触;所述出气管a底端进气口设于瓶身a顶部,顶端出气口穿过瓶塞a与另一个直角气动接头的一端连接;所述转子设于瓶身a底壁内表面,所述有机玻璃瓶a活动连接于磁力搅拌装置顶部;Technical solution: a gas sampler, the sampler includes a first absorption device, a second absorption device, an absorption liquid, a straight pipe and a gas collecting bottle, the first absorption device includes an air inlet pipe a, a right-angle pneumatic joint, an outlet Trachea a, bottle stopper a, plexiglass bottle a, magnetic stirring device and rotor, the plexiglass bottle a includes a bottle body a, a vacuum suction branch pipe a, an absorbing liquid outlet a and a rubber stopper, and the bottle body a is the bottom A cylinder with a sealed end, an open top and an internal cavity, the vacuum suction branch pipe a is set at the top of the bottle body a, the absorbing liquid outlet a is set at the bottom edge of the bottle body a, and the rubber stoppers are respectively sealed for vacuum pumping. Trachea a and the absorbing liquid outlet a, the bottle stopper a is movably connected to the open end of the bottle body a, used to seal the bottle body a; the air inlet pipe a includes a tube body a and an aeration head, and the top of the tube body a is It is a thin cylindrical tube, the middle and bottom are thick cylindrical tubes with the inner diameter expanded by at least 2 times, the aeration head is connected to the bottom end of the tube body a, and the top of the tube body a is connected to one end of the right-angle pneumatic joint through the bottle stopper a , the rest of the tube body a is arranged inside the bottle body a, the aeration head is arranged at the bottom of the bottle body a and does not contact the bottom wall of the bottle body a; The air outlet is connected to one end of another right-angle pneumatic joint through the bottle stopper a; the rotor is arranged on the inner surface of the bottom wall of the bottle body a, and the plexiglass bottle a is movably connected to the top of the magnetic stirring device;
所述第二吸收装置包括进气管b、出气管b、直角气动接头、瓶塞b和有机玻璃瓶b,所述有机玻璃瓶b包括瓶身b、真空抽气支管b、吸收液出口b和橡胶塞,所述瓶身b为底端密封、顶端开口且内部空腔的圆柱体,所述真空抽气支管b设于瓶身b顶部,所述吸收液出口b设于瓶身b底端边缘,所述橡胶塞分别密封真空抽气支管b和吸收液出口b,所述瓶塞b活动连接于瓶身b开口端,用于密封瓶身b;所述进气管b包括管身b和微孔短管,管身b为两端开口的内部中空圆柱形腔体,管身b顶部穿过瓶塞b与直角气动接头的一端连接,管身b其余部分设于瓶身b内部,所述微孔短管为底端密封、顶端开口且管壁开设微孔的内部空腔圆柱体,微孔短管的顶端与管身b底端无缝连接,微孔短管的底端靠近管身b底壁内表面;所述出气管b底端进气口设于瓶身b顶部,顶端出气口穿过瓶塞b与另一个直角气动接头的一端连接;The second absorption device includes an air inlet pipe b, an air outlet pipe b, a right-angle pneumatic joint, a bottle stopper b and a plexiglass bottle b. The plexiglass bottle b includes a bottle body b, a vacuum suction branch pipe b, an absorption liquid outlet b and Rubber stopper, the bottle body b is a cylinder with a sealed bottom end, an open top end and an internal cavity, the vacuum suction branch pipe b is set at the top of the bottle body b, and the absorption liquid outlet b is set at the bottom end of the bottle body b On the edge, the rubber stopper seals the vacuum suction branch pipe b and the absorbing liquid outlet b respectively, and the bottle stopper b is movably connected to the open end of the bottle body b for sealing the bottle body b; the air inlet pipe b includes the pipe body b and The microporous short tube, the tube body b is an internal hollow cylindrical cavity with openings at both ends, the top of the tube body b is connected to one end of the right-angle pneumatic joint through the bottle stopper b, and the rest of the tube body b is arranged inside the bottle body b, so the The microporous short tube is an internal cavity cylinder with a sealed bottom end, an open top end and a microporous tube wall, the top of the microporous short tube is seamlessly connected with the bottom end of the tube body b, and the bottom end of the microporous short tube is close to the tube The inner surface of the bottom wall of the body b; the air inlet at the bottom end of the air outlet pipe b is arranged on the top of the bottle body b, and the top air outlet passes through the bottle stopper b and is connected with one end of another right-angle pneumatic joint;
所述吸收液分别装填于有机玻璃瓶a和有机玻璃瓶b中下部,装填高度分别低于出气管a和出气管b的底端;The absorbing liquid is respectively filled in the lower part of the plexiglass bottle a and the plexiglass bottle b, and the filling height is respectively lower than the bottom end of the gas outlet pipe a and the gas outlet pipe b;
直通管为进气端带有圆球形凸起的圆柱形管,一个直通管进气端与出气管a相接的直角气动接头的另一端连接,出气端与进气管b相接的直角气动接头的另一端连接;一个直通管进气端与待测气体连接,出气端与进气管a相接的直角气动接头的另一端连接;另一个直通管进气端与出气管b相接的直角气动接头的另一端连接,出气端与集气瓶进气口连接。The straight-through pipe is a cylindrical pipe with a spherical protrusion at the intake end. The intake end of a straight-through pipe is connected to the other end of the right-angle pneumatic joint connected to the exhaust pipe a, and the right-angle pneumatic joint of the exhaust end is connected to the intake pipe b. The other end of the straight pipe is connected to the other end of the right-angle pneumatic joint; the intake end of one straight pipe is connected to the gas to be tested, and the gas outlet is connected to the other end of the right-angle pneumatic joint connected to the intake pipe a; the intake end of the other straight pipe is connected to the gas outlet pipe b. The other end of the joint is connected, and the gas outlet is connected with the air inlet of the gas collecting bottle.
作为优选,所述瓶塞a顶端直径大于瓶身a开口端直径,底端直径小于瓶身a开口端直径;所述瓶塞b顶端直径大于瓶身b开口端直径,底端直径小于瓶身b开口端直径。Preferably, the diameter of the top of the bottle stopper a is larger than the diameter of the open end of the bottle body a, and the diameter of the bottom end is smaller than the diameter of the open end of the bottle body a; the diameter of the top end of the bottle stopper b is larger than the diameter of the open end of the bottle body b, and the diameter of the bottom end is smaller than the diameter of the bottle body a. b Diameter of open end.
作为优选,所述进气管a、出气管a、直通管、进气管b和出气管b分别为聚四氟乙烯软管。Preferably, the air inlet pipe a, the air outlet pipe a, the straight pipe, the air inlet pipe b and the air outlet pipe b are respectively polytetrafluoroethylene hoses.
作为优选,所述瓶塞a和瓶塞b为硅胶塞。Preferably, the bottle stopper a and the bottle stopper b are silica gel stoppers.
作为优选,所述曝气头为气泡石,所述气泡石由白刚玉、碳化硅和金刚砂烧结而成,所述气泡石表面布满孔径为100 μm的气孔。Preferably, the aeration head is air stone, the air stone is sintered from white corundum, silicon carbide and emery, and the surface of the air stone is covered with pores with a diameter of 100 μm.
作为优选,所述有机玻璃瓶a和有机玻璃瓶b底端分别为楔形,吸收液出口a和吸收液出口b分别设于有机玻璃瓶a和有机玻璃瓶b底端最薄的边缘处。Preferably, the bottom ends of the plexiglass bottle a and the plexiglass bottle b are respectively wedge-shaped, and the absorbing liquid outlet a and the absorbing liquid outlet b are respectively located at the thinnest edges of the bottom ends of the plexiglass bottle a and the plexiglass bottle b.
作为优选,所述有机玻璃瓶a和有机玻璃瓶b外表面分别设有刻度。Preferably, the outer surfaces of the plexiglass bottle a and the plexiglass bottle b are respectively provided with scales.
作为优选,所述磁力搅拌装置为微型磁力搅拌器。Preferably, the magnetic stirring device is a miniature magnetic stirrer.
有益效果:1.本新型分别经过第一吸收装置和第二吸收装置进行待测气体的收集,待测气体经过第一吸收装置初步吸收后,经过第二吸收装置进一步吸收,能够减少因为溶解不充分造成的人工误差。Beneficial effects: 1. The new model collects the gas to be tested through the first absorption device and the second absorption device respectively. After the gas to be tested is initially absorbed by the first absorption device, it is further absorbed by the second absorption device, which can reduce the amount of gas to be measured. full of human error.
2.本新型不仅可以作为挥发性气体采样装置,还可以作为洗气装置。作为洗气装置时,通过集气瓶采集被洗涤后气体;作为挥发性气体采样装置时,从吸收液出口将吸收液倒出,通过检测吸收液进一步检测挥发性气体。2. The new model can be used not only as a volatile gas sampling device, but also as a gas washing device. When used as a gas scrubbing device, the cleaned gas is collected through a gas collecting bottle; when used as a volatile gas sampling device, the absorbing liquid is poured out from the absorbing liquid outlet, and the volatile gas is further detected by detecting the absorbing liquid.
3.本新型在有机玻璃瓶顶部设有真空抽气支管,进行气体采集时,先用真空泵从真空抽气支管抽取有机玻璃瓶上部的空气,在作为洗气装置时,能够避免有机玻璃瓶中空气对集气瓶中采集到的样品的影响。3. The new model is provided with a vacuum suction branch pipe on the top of the plexiglass bottle. When gas collection is performed, the air in the upper part of the plexiglass bottle is first extracted from the vacuum suction branch pipe with a vacuum pump. The effect of air on the sample collected in the gas collection bottle.
4.本新型所述吸收液出口设于瓶身底端边缘,并且有机玻璃瓶底端分别为楔形,吸收液出口设于有机玻璃瓶底端最薄的边缘处,倒出吸收液时,能够避免吸收液沾到瓶壁上导致吸收液减少,并且能够使吸收液更容易被倒干净。4. The absorbing liquid outlet of this new model is located at the bottom edge of the bottle body, and the bottom ends of the plexiglass bottle are respectively wedge-shaped, and the absorbing liquid outlet is located at the thinnest edge of the bottom end of the plexiglass bottle. Avoiding the absorption liquid from sticking to the bottle wall will reduce the absorption liquid and make the absorption liquid easier to be poured out.
5.本新型第一吸收装置内部设有曝气头,底部设有磁力搅拌装置,曝气头采用由白刚玉、碳化硅和金刚砂在1500℃的高温下烧结而成的气泡石,气泡石表面布满孔径为100μm的气孔,产生的气泡较为细腻,气泡越小,与吸收液的接触面积越大,提高了吸收效率,当气泡露出水面爆裂时,溅起的水珠力度小,不会随气流流失,结合搅拌能够使被采集气体更容易被吸收液吸收或采集。5. There is an aeration head inside the first absorption device of this new type, and a magnetic stirring device at the bottom. The aeration head is made of air stone sintered from white corundum, silicon carbide and emery at a high temperature of 1500 ° C. The surface of the air stone is Filled with pores with a diameter of 100 μm, the generated bubbles are more delicate. The smaller the bubbles, the larger the contact area with the absorbing liquid, which improves the absorption efficiency. The loss of airflow, combined with agitation, can make the collected gas more easily absorbed or collected by the absorbing liquid.
6. 本新型第二吸收装置进气管底端靠近管身b底壁内表面,气体通过微孔短管溅射到瓶身b底部,增大了与吸收液的接触面积,能够最大范围的吸收气体中的杂质。6. The bottom end of the air inlet pipe of the new second absorption device is close to the inner surface of the bottom wall of the tube body b, and the gas is sputtered to the bottom of the bottle body b through the microporous short tube, which increases the contact area with the absorbing liquid and can absorb the maximum range. impurities in the gas.
7.本新型有机玻璃瓶作为容器,坚固耐用;以四氟乙烯软管和直角气动接头作为进气通道和出气通道,连接紧密,提高了气密性;进气管为透明色,出气管为橘红色,增加了辨识度,避免连接管路时出错;减少了实验误差。7. The new plexiglass bottle is used as a container, which is sturdy and durable; the tetrafluoroethylene hose and the right-angle pneumatic joint are used as the air inlet and outlet channels, which are tightly connected and improve the air tightness; the air inlet pipe is transparent, and the air outlet pipe is orange The red color increases the recognition degree and avoids mistakes when connecting the pipeline; reduces the experimental error.
本新型所述气体采样器尤其适合野外条件下,抽气速率高的气体采样实验。The gas sampler of the new type is especially suitable for gas sampling experiments with high pumping rate under field conditions.
附图说明Description of drawings
图1 为本新型所述装置结构示意图;Fig. 1 is a schematic diagram of the structure of the device according to the new model;
图2为第一吸收装置结构示意图;2 is a schematic structural diagram of a first absorption device;
图3为第二吸收装置结构示意图;3 is a schematic structural diagram of a second absorption device;
图4为第二吸收装置进气管b结构示意图。FIG. 4 is a schematic structural diagram of the intake pipe b of the second absorption device.
图中各数字标号代表如下:1.进气管a;2.直角气动接头;3.出气管a;4.瓶塞a;5.有机玻璃瓶a;6.吸收液;7.曝气头;8.真空抽气支管a;9.吸收液出口a;10.磁力搅拌装置;11.转子;12.刻度;13.进气管b;14.出气管b;15.瓶塞b;16.有机玻璃瓶b;17.微孔短管;18.真空抽气支管b;19.吸收液出口b;20.集气瓶;21.直通管。The numbers in the figure represent the following: 1. Inlet pipe a; 2. Right-angle pneumatic joint; 3. Air outlet pipe a; 4. Bottle stopper a; 5. Plexiglass bottle a; 6. Absorbing liquid; 8. Vacuum pumping branch pipe a; 9. Absorbing liquid outlet a; 10. Magnetic stirring device; 11. Rotor; 12. Scale; 13. Inlet pipe b; 14. Outlet pipe b; 15. Bottle stopper b; Glass bottle b; 17. Microporous short tube; 18. Vacuum suction branch pipe b; 19. Absorption liquid outlet b; 20. Gas collecting bottle; 21. Straight pipe.
具体实施方式Detailed ways
下面结合附图和具体实施例对本新型作进一步描述。The present invention will be further described below in conjunction with the accompanying drawings and specific embodiments.
实施例1Example 1
一种气体采样器,参见图1,所述采样器包括第一吸收装置、第二吸收装置、吸收液、直通管21和集气瓶20。A gas sampler, see FIG. 1 , the sampler includes a first absorption device, a second absorption device, an absorption liquid, a
参见图2,所述第一吸收装置包括进气管a1、直角气动接头2、出气管a 3、瓶塞a 4、有机玻璃瓶a 5、磁力搅拌装置10和转子11,所述有机玻璃瓶a 5包括瓶身a、真空抽气支管a8、吸收液出口a 9和橡胶塞,所述瓶身a为底端密封、顶端开口且内部空腔的圆柱体,所述真空抽气支管a 8设于瓶身a顶部,所述吸收液出口a 9设于瓶身a底端边缘,所述橡胶塞分别密封真空抽气支管a 8和吸收液出口a 9,所述瓶塞a 4活动连接于瓶身a开口端,用于密封瓶身a;所述进气管a 1包括管身a和曝气头7,所述管身a顶部为圆柱形细管,中部和底部为内径扩大至少2倍的圆柱形粗管,所述曝气头7与管身a底端连接,管身a顶部穿过瓶塞a 4与直角气动接头的一端连接,管身a其余部分设于瓶身a内部,曝气头7设于瓶身a底部且与瓶身a底壁不接触;所述出气管a 3底端进气口设于瓶身a顶部,顶端出气口穿过瓶塞a 4与另一个直角气动接头的一端连接;所述转子11设于瓶身a底壁内表面,所述有机玻璃瓶a 5活动连接于磁力搅拌装置10顶部;Referring to FIG. 2 , the first absorption device includes an air inlet pipe a1, a right-angle pneumatic joint 2, an air outlet pipe a 3, a bottle stopper a 4, a plexiglass bottle a 5, a magnetic stirring device 10 and a rotor 11, the plexiglass bottle a 5 includes a bottle body a, a vacuum suction branch pipe a8, an absorbing liquid outlet a 9 and a rubber stopper, the bottle body a is a cylinder with a sealed bottom end, an open top end and an internal cavity, and the vacuum suction branch pipe a8 is provided with On the top of the bottle body a, the absorbing liquid outlet a 9 is arranged on the edge of the bottom end of the bottle body a, the rubber stopper seals the vacuum suction branch pipe a 8 and the absorbing liquid outlet a 9 respectively, and the bottle stopper a 4 is movably connected to the The open end of the bottle body a is used to seal the bottle body a; the air inlet pipe a 1 includes a pipe body a and an aeration head 7, the top of the pipe body a is a cylindrical thin tube, and the inner diameter is enlarged at least 2 times in the middle and bottom The cylindrical thick pipe, the aeration head 7 is connected with the bottom end of the pipe body a, the top of the pipe body a is connected with one end of the right-angle pneumatic joint through the bottle stopper a 4, and the rest of the pipe body a is located inside the bottle body a, The aeration head 7 is arranged at the bottom of the bottle body a and does not contact the bottom wall of the bottle body a; the bottom air inlet of the air outlet pipe a 3 is arranged on the top of the bottle body a, and the top air outlet passes through the bottle stopper a 4 and another One end of the right-angle pneumatic joint is connected; the rotor 11 is arranged on the inner surface of the bottom wall of the bottle body a, and the organic glass bottle a 5 is movably connected to the top of the magnetic stirring device 10;
参见图3和图4,所述第二吸收装置包括进气管b 13、出气管b 14、直角气动接头、瓶塞b 15和有机玻璃瓶b 16,所述有机玻璃瓶b 16包括瓶身b、真空抽气支管b 18、吸收液出口b 19和橡胶塞,所述瓶身b为底端密封、顶端开口且内部空腔的圆柱体,所述真空抽气支管b(18)设于瓶身b顶部,所述吸收液出口b 19设于瓶身b底端边缘,所述橡胶塞分别密封真空抽气支管b 18和吸收液出口b 19,所述瓶塞b 15活动连接于瓶身b开口端,用于密封瓶身b;所述进气管b 13包括管身b和微孔短管17,管身b为两端开口的内部中空圆柱形腔体,管身b顶部穿过瓶塞b 15与直角气动接头的一端连接,管身b其余部分设于瓶身b内部,所述微孔短管 17为底端密封、顶端开口且管壁开设微孔的内部空腔圆柱体,微孔短管17的顶端与管身b底端无缝连接,微孔短管17的底端靠近管身b底壁内表面;所述出气管b14底端进气口设于瓶身b顶部,顶端出气口穿过瓶塞b 15与另一个直角气动接头的一端连接;3 and 4, the second absorption device includes an air inlet pipe b 13, an air outlet pipe b 14, a right-angle pneumatic joint, a stopper b 15 and a plexiglass bottle b 16, the plexiglass bottle b 16 includes a bottle body b , the vacuum suction branch pipe b 18, the absorption liquid outlet b 19 and the rubber stopper, the bottle body b is a cylinder with a sealed bottom end, an open top end and an inner cavity, and the vacuum suction branch pipe b (18) is provided in the bottle On the top of the body b, the absorbing liquid outlet b 19 is arranged on the bottom edge of the bottle body b, the rubber stopper seals the vacuum suction branch pipe b 18 and the absorbing liquid outlet b 19 respectively, and the bottle stopper b 15 is movably connected to the bottle body b open end for sealing the bottle body b; the air inlet pipe b 13 includes a pipe body b and a microporous short pipe 17, the pipe body b is an inner hollow cylindrical cavity with open ends at both ends, and the top of the pipe body b passes through the bottle The plug b 15 is connected with one end of the right-angle pneumatic joint, and the rest of the tube body b is arranged inside the bottle body b. The top end of the microporous
所述吸收液分别装填于有机玻璃瓶a 5和有机玻璃瓶b 16中下部,装填高度分别低于出气管a 3和出气管b 14的底端;The absorbing liquid is filled in the lower part of the plexiglass bottle a 5 and the
直通管21为进气端带有圆球形凸起的圆柱形管,一个直通管进气端与出气管a 3相接的直角气动接头的另一端连接,出气端与进气管b 13相接的直角气动接头的另一端连接;一个直通管进气端与待测气体连接,出气端与进气管a 1相接的直角气动接头的另一端连接;另一个直通管进气端与出气管b 14相接的直角气动接头的另一端连接,出气端与集气瓶20进气口连接。The
所述气体采样器具体使用过程如下:分别向有机玻璃瓶a 5和有机玻璃瓶b 16中注入吸收液6,分别组装第一吸收装置和第二吸收装置,然后用一个直通管通过直角气动接头分别与出气管a 3和进气管b 13连接,再用一个直通管将集气瓶20通过直角气动接头与出气管b 14连接。然后分别用真空泵从真空抽气支管抽取有机玻璃瓶a 5和有机玻璃瓶b16上部的空气,然后用橡胶塞将真空抽气支管密封,打开磁力搅拌装置10。待测气体通过一个直通管进气端经过进气管a 1进入有机玻璃瓶a 5,气体通过曝气石7分散成小分子气体,加上转子11的搅拌作用,能够更充分地被吸收液洗涤,被洗涤后从瓶身a上部进入到出气管a 3,然后经过直通管的缓冲后经过进气管b 13进入有机玻璃瓶b 16,气体通过微孔短管溅射到瓶身b底部,增大了与吸收液6的接触面积,能够最大范围的吸收气体中的杂质,被吸收液洗涤后的气体从吸收液底部进入瓶身b的上部,然后经过出气管b 14和直通管进入集气瓶20,检测吸收液时,将吸收液出口a 9和吸收液出口b 19的橡胶塞取下,将吸收液倒出,能够最大程度的减少人为误差,最终完成气体的采集过程。The specific use process of the gas sampler is as follows: inject the
实施例2Example 2
同实施例1,区别在于,所述有机玻璃瓶a 5瓶身高度为25 cm,瓶底直径为5 cm。所述瓶塞a 4顶端直径大于瓶身a开口端直径,底端直径小于瓶身a开口端直径,瓶塞a 4的规格为50.8(小头直径)×62.7(大头直径)×25(高度)mm,材质为硅胶塞。进气管a 1顶部圆柱形细管直径为6 mm,中部和底部圆柱形粗管直径为12 mm,曝气头7为气泡石,所述气泡石由白刚玉、碳化硅和金刚砂在1500℃的高温下烧结而成,气泡石的直径为35 mm的球形体,气泡石表面布满孔径为100 μm的气孔,产生的气泡较为细腻,气泡越小,与吸收液的接触面积越大,提高了吸收效率,当气泡露出水面爆裂时,溅起的水珠力度小,不会随气流流失,减少了实验误差。曝气头7底端距离瓶身a底壁3 cm。Same as Example 1, the difference is that the height of the plexiglass bottle a 5 is 25 cm, and the diameter of the bottom of the bottle is 5 cm. The diameter of the top of the bottle stopper a 4 is larger than the diameter of the opening end of the bottle body a, and the diameter of the bottom end is smaller than the diameter of the opening end of the bottle body a. The size of the bottle stopper a 4 is 50.8 (small end diameter) × 62.7 (large end diameter) × 25 (height). ) mm, made of silicone plug. The diameter of the top cylindrical thin pipe of the intake pipe a 1 is 6 mm, the diameter of the middle and bottom cylindrical thick pipes is 12 mm, and the
有机玻璃瓶b 16瓶身高度为30 cm,瓶底直径为5 cm。所述瓶塞b 15顶端直径大于瓶身b开口端直径,底端直径小于瓶身b开口端直径,规格为50.8(小头直径)×62.7(大头直径)×25(高度)mm,材质为硅胶塞。进气管b 13管径为6 mm,微孔短管17的高度为1 cm。The
出气管a 3(出气管b 14)的进气端分别设于瓶身a(瓶身b)顶部并距离瓶塞a 4(瓶塞b 15)下表面2 cm处。进气管a 1(进气管b 13)的进气端穿出瓶身a(瓶身b)并高于瓶塞a4(瓶塞b 15)上表面4 cm。进气管a 1和进气管b 13分别为透明色,出气管a 3和出气管b 14分别为橘红色,以此增加辨识度,避免连接管路时出错。The air inlet ends of the air outlet pipe a 3 (the air outlet pipe b 14 ) are respectively arranged on the top of the bottle body a (bottle body b) and 2 cm away from the lower surface of the bottle stopper a 4 (the bottle stopper b 15 ). The air inlet end of the air inlet pipe a1 (the air inlet pipe b 13) passes through the bottle body a (bottle body b) and is 4 cm higher than the upper surface of the bottle stopper a4 (the bottle stopper b 15). The air intake pipe a1 and the air intake pipe b13 are respectively transparent, and the air outlet pipe a3 and the air outlet pipe b14 are respectively orange-red, so as to increase the recognition degree and avoid mistakes when connecting the pipes.
所述有机玻璃瓶a 5和有机玻璃瓶b 16底端分别为楔形,吸收液出口a 9和吸收液出口b 19分别设于有机玻璃瓶a 5和有机玻璃瓶b 16底端最薄的边缘处,倾倒吸收液时,能够最大程度的减少人为误差,使瓶中液体更容易被倒干净。所述有机玻璃瓶a 5和有机玻璃瓶b 16外表面分别设有刻度12,能够便于操作人员读取吸收液的体积。所述磁力搅拌装置10为微型磁力搅拌器,磁力搅拌装置10用于搅拌吸收液,使气体更充分地融入吸收液。The bottom ends of the organic glass bottle a 5 and the organic
所述进气管a 1、出气管a 3、直通管、进气管b 13和出气管b 14分别为聚四氟乙烯软管。直角气动接头2的内径为6 mm,每个直角气动接头分别与进气管的进气端和出气管的出气端连接,直角气动接头能与聚四氟乙烯软管快速连接,且紧密相连,提高了气密性。The air inlet pipe a 1 , the air outlet pipe a 3 , the straight pipe, the air
实施例3Example 3
采用实施例2的装置,以农田氨挥发采样为例,具体使用过程如下:Using the device of Example 2, taking farmland ammonia volatilization sampling as an example, the specific use process is as follows:
将氨挥发采样罩插入农田5 cm深处,利用PVC硬管将采样罩、实施例2制备的气体采样器与进气管a 1连接的直通管、抽气泵依次连接。本实施例中吸收液6为稀硫酸。开始监测前,首先将100 mL稀硫酸平均分成两份分别加入第一吸收装置和第二吸收装置。然后开启抽气泵抽气,抽气流量为20 L/min。选择8:00-10:00开展野外监测工作,抽气结束后将气体采样器中吸收液装入塑料瓶中,带回实验室,用靛酚蓝比色测定吸收液中NH4 +-N浓度。根据采样时间,采样罩面积测算农田氨挥发量。Insert the ammonia volatilization sampling hood into the farmland at a depth of 5 cm, and connect the sampling hood, the gas sampler prepared in Example 2 with the straight-through pipe connected to the air inlet pipe a1, and the suction pump in turn by using a PVC rigid pipe. In this embodiment, the absorbing
Claims (8)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921625972.4U CN210834362U (en) | 2019-09-27 | 2019-09-27 | a gas sampler |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921625972.4U CN210834362U (en) | 2019-09-27 | 2019-09-27 | a gas sampler |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210834362U true CN210834362U (en) | 2020-06-23 |
Family
ID=71252096
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201921625972.4U Expired - Fee Related CN210834362U (en) | 2019-09-27 | 2019-09-27 | a gas sampler |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210834362U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110592179A (en) * | 2019-09-16 | 2019-12-20 | 中国科学院微生物研究所 | Biological aerosol collecting method based on rotary liquid cavity |
| CN113340679A (en) * | 2021-06-03 | 2021-09-03 | 南开大学 | Sampling device and method for effectively collecting nano plastic in air |
-
2019
- 2019-09-27 CN CN201921625972.4U patent/CN210834362U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110592179A (en) * | 2019-09-16 | 2019-12-20 | 中国科学院微生物研究所 | Biological aerosol collecting method based on rotary liquid cavity |
| CN110592179B (en) * | 2019-09-16 | 2020-11-27 | 中国科学院微生物研究所 | A bioaerosol collection method based on a rotating liquid cavity |
| CN113340679A (en) * | 2021-06-03 | 2021-09-03 | 南开大学 | Sampling device and method for effectively collecting nano plastic in air |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107402145A (en) | A kind of air sampling container and the method for sampling | |
| CN106644605A (en) | Device and method for collecting bubble gas in geothermal water | |
| CN211235100U (en) | Sampler | |
| CN211825655U (en) | A kind of indoor air sampling analysis tube | |
| CN207866583U (en) | A kind of sample automatic acquisition device | |
| CN211856055U (en) | Mobile gas collection device | |
| CN211757274U (en) | Pipette ultrasonic cleaning device | |
| CN208443628U (en) | An on-site water sample filtering device | |
| CN216349779U (en) | Collecting assembly for cell sap samples | |
| CN206523331U (en) | The collection device of bubble gas in a kind of GEOTHERMAL WATER | |
| CN204008238U (en) | A kind of gas collector | |
| CN211448796U (en) | Pressure drop measuring device for experimental wood fiber ceramic filter | |
| CN209361958U (en) | An Improved Suction Filtration Device Capable of Automatic Sample Injection | |
| CN205608000U (en) | A test pen for immunology detects | |
| CN209286317U (en) | A kind of anti-pollution big volume BAL fluid collector | |
| CN218994745U (en) | Novel split type fecal sample quantitative collection device | |
| CN211885725U (en) | Closed solution filtering device | |
| CN2798077Y (en) | Sampling bottle for analyzing salt-spray fog concentration | |
| CN209606151U (en) | A kind of outdoor liquid asepsis sampler | |
| CN210787383U (en) | An ion exchange resin treatment device | |
| CN208188082U (en) | A kind of detection device based on micro-fluidic chip | |
| CN220912765U (en) | Plastic porous glass plate absorption tube | |
| CN221826551U (en) | Beverage sampling device | |
| CN217659944U (en) | Novel virus detection is with gathering device | |
| CN217490430U (en) | A circulating collection bottle for tangential flow ultrafiltration concentration |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200623 Termination date: 20210927 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |