CN210814001U

CN210814001U - Distillation device for filtering chemical reagent

Info

Publication number: CN210814001U
Application number: CN201921547395.1U
Authority: CN
Inventors: 贤少赟; 靳跃双; 陈冬恩
Original assignee: Tianjin Yaotech Co ltd
Current assignee: Tianjin Yaotech Co ltd
Priority date: 2019-09-18
Filing date: 2019-09-18
Publication date: 2020-06-23
Anticipated expiration: 2029-09-18

Abstract

The utility model discloses a be used for filterable distillation plant of chemical reagent, including the distillation case, the equal fixedly connected with support in both sides of distillation case surface, the equal fixedly connected with collecting plate in both sides of distillation incasement wall top, two fixedly connected with active carbon adsorption layer between the collecting plate, the top fixedly connected with box of distillation case, the top of distillation case just is located the inside fixedly connected with rotation motor of box, the utility model relates to a distillation technical field. This a distillation plant for chemical reagent filters sets up the pivot through the inside of distillation case, and the cooperation of motor, first gear and second gear is being rotated in the cooperation, is utilizing dead lever and scraper blade for the scraper blade can rotate along the inner wall of distillation case, thereby will be attached to and remove scraping at the dirt of distillation case inner wall, and the dirt falls on detachable reagent adsorption plate, has avoided the trouble of manual cleaning, has practiced thrift staff's time.

Description

Distillation device for filtering chemical reagent

Technical Field

The utility model relates to a distillation technical field specifically is a be used for filterable distillation plant of chemical reagent.

Background

Distillation is a thermodynamic separation process that utilizes the difference in boiling points of components in a mixed liquid or liquid-solid system to vaporize lower boiling components and recondense to separate the entire component, a unit operation that combines the two unit operations of evaporation and condensation. Compared with other separation means, such as extraction, filtration crystallization and the like, the method has the advantage that other solvents except system components are not required, so that new impurities are not introduced. And when the chemical reagent is too much, distillation treatment can be adopted, so that the chemical reagent can be recycled.

The filterable distillation plant of current chemical reagent, the distillation case is at the in-process of distillation, and distillation area can leave a lot of dirt and adhere to the inner wall at the distillation case, and the staff is difficult to the sanitization, and staff's time is wasted, and most chemical reagent have solid catalyst's participation when the reaction, and the filterable distillation plant of present chemical reagent does not filter it, need carry out prefiltration, and the process is loaded down with trivial details, and work efficiency is lower.

SUMMERY OF THE UTILITY MODEL

Not enough to prior art, the utility model provides a be used for filterable distillation plant of chemical reagent has solved the attached dirt of distillation zone and has been difficult to the clean up, and the unable problem of separating of fixed granule in the reagent.

In order to achieve the above purpose, the utility model discloses a following technical scheme realizes: a distillation device for filtering chemical reagents comprises a distillation box, wherein two sides of the outer surface of the distillation box are fixedly connected with supports, two sides of the upper part of the inner wall of the distillation box are fixedly connected with collecting plates, an activated carbon adsorption layer is fixedly connected between the two collecting plates, the top of the distillation box is fixedly connected with a box body, the top of the distillation box is fixedly connected with a rotating motor which is positioned inside the box body, the output end of the rotating motor is fixedly connected with a first rotating gear through a connecting shaft, the top of the inner cavity of the box body is rotatably connected with a rotating shaft, the bottom of the rotating shaft sequentially penetrates through the distillation box and the activated carbon adsorption layer from top to bottom and extends to the bottom of the activated carbon adsorption layer, a second rotating gear is fixedly connected above the outer surface of the rotating shaft, one side of the second rotating gear is meshed with one side of the first rotating, the utility model discloses a box, including pivot surface, box inner wall, the below fixedly connected with dead lever of pivot surface, the left end fixedly connected with rotor plate of dead lever, the left side fixedly connected with scraper blade of rotor plate, box inner wall fixedly connected with reagent adsorption plate.

Preferably, the two sides of the inner wall of the distillation box are fixedly connected with collecting boxes through supporting rods, the front surfaces of the outer surfaces of the collecting boxes are communicated with feeding pipes, one ends of the feeding pipes penetrate through the distillation box and extend to the outside of the distillation box, and the right side of the support is fixedly connected with a cylinder.

Preferably, the output end fixedly connected with filter of cylinder, the right side of filter runs through distillation box and collecting box and runs through to the outside of collecting box from a left side to the right side in proper order.

Preferably, the upper parts of two sides of the outer surface of the distillation box are fixedly connected with water outlet pipes, and one ends of the water outlet pipes penetrate through the distillation box and extend into the distillation box.

Preferably, the top of the support is fixedly connected with a vacuum pump, the air exhaust end of the vacuum pump is communicated with the right side of the outer surface of the distillation box, and the top of the distillation box is communicated with a pressure gauge through a pipeline.

Preferably, the bottom of the distillation box is fixedly connected with an electromagnetic heating coil, and the top of the electromagnetic heating coil is fixedly connected with an electromagnetic heating block.

Advantageous effects

The utility model provides a be used for filterable distillation plant of chemical reagent. Compared with the prior art, the method has the following beneficial effects:

(1) the distillation device for filtering the chemical reagent is characterized in that collecting plates are fixedly connected to two sides above the inner wall of a distillation box, an activated carbon adsorption layer is fixedly connected between the two collecting plates, the top of the distillation box is fixedly connected with a box body, the top of the distillation box is fixedly connected with a rotating motor positioned in the box body, the output end of the rotating motor is fixedly connected with a first rotating gear through a connecting shaft, the top of the inner cavity of the box body is rotatably connected with a rotating shaft, the bottom end of the rotating shaft sequentially penetrates through the distillation box and the activated carbon adsorption layer from top to bottom and extends to the bottom of the activated carbon adsorption layer, a second rotating gear is fixedly connected to the upper part of the outer surface of the rotating shaft, one side of the second rotating gear is meshed with one side of the first rotating gear, a fixed rod is fixedly connected to the lower part of the outer surface of the rotating shaft, box inner wall fixedly connected with reagent adsorption plate sets up the pivot through the inside of distillation case, and the cooperation of motor, first gear and second gear is being rotated in the cooperation, is utilizing dead lever and scraper blade for the scraper blade can rotate along the inner wall of distillation case, thereby will be attached to and remove to strike off at the dirt of distillation case inner wall, and the dirt falls on detachable reagent adsorption plate, has avoided the trouble of manual cleaning, has practiced thrift staff's time.

(2) This a be used for filterable distillation plant of chemical reagent, through bracing piece fixedly connected with collecting box in the both sides of distillation box inner wall, the front intercommunication of collecting box surface has the inlet pipe, the one end of inlet pipe runs through the distillation box and extends to the outside of distillation box, the right side fixedly connected with cylinder of two supports, the output fixedly connected with filter of cylinder, the right side of filter runs through distillation box and collecting box in proper order and runs through to the outside of collecting box from a left side to the right side, bottom through the collection box sets up the filter, make the solid particle in the collecting box, stay in the collecting box, the motion of cooperation cylinder, prevent that the solid particle from blockking up the surface at the filter, this structure is comparatively simple, the effect is obvious, chemical reagent prefilter's step has been saved, whole work flow has been simplified.

Drawings

FIG. 1 is a front view of the internal structure of the present invention;

FIG. 2 is a front view of the external structure of the present invention;

FIG. 3 is a side view of the internal structure of the feeding pipe of the present invention;

fig. 4 is a front view of the internal structure of the rotating shaft of the present invention.

In the figure: 1-distillation box, 2-bracket, 3-collecting plate, 4-activated carbon adsorption layer, 5-box, 6-rotating motor, 7-first rotating gear, 8-rotating shaft, 9-second rotating gear, 10-fixed rod, 11-rotating plate, 12-scraper, 13-reagent adsorption plate, 14-collecting box, 15-feeding pipe, 16-cylinder, 17-filter plate, 18-water outlet pipe, 19-vacuum pump, 20-pressure gauge, 21-electromagnetic heating coil, 22-electromagnetic heating block.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-4, the present invention provides a technical solution: a distillation device for filtering chemical reagents comprises a distillation box 1, the bottom of the distillation box 1 is fixedly connected with an electromagnetic heating coil 21, the electromagnetic heating coil 21 is electrically connected with an external power supply, the distillation box is prior art and can transfer heat to an electromagnetic heating block 22, the top of the electromagnetic heating coil 21 is fixedly connected with the electromagnetic heating block 22, the electromagnetic heating block 22 can heat chemical reagents in the distillation box 1, the upper parts of two sides of the outer surface of the distillation box 1 are fixedly connected with water outlet pipes 18, one end of each water outlet pipe 18 penetrates through the distillation box 1 and extends to the inside of the distillation box 1, two sides of the inner wall of the distillation box 1 are fixedly connected with a collection box 14 through support rods, the front surface of the outer surface of the collection box 14 is communicated with a feed pipe 15, the feed pipe 15 is provided with a matched pipe cover, one end of each feed pipe 15 penetrates through the distillation box 1 and extends to the outside, the air cylinder 16 is positioned on the right side of the left support 2, the air cylinder 16 is electrically connected with an external power supply, the output end of the air cylinder 16 is fixedly connected with a filter plate 17, the right side of the filter plate 17 sequentially penetrates through the distillation box 1 and the collecting box 14 from left to right and penetrates outside the collecting box 14, the two sides of the outer surface of the distillation box 1 are both fixedly connected with the supports 2, the top of each support 2 is fixedly connected with a vacuum pump 19, the vacuum pumps 19 are electrically connected with the external power supply and can reduce the pressure in the distillation box 1, so that chemical reagents can reach a boiling point more quickly and increase the distillation speed, the air suction end of each vacuum pump 19 is communicated with the right side of the outer surface of the distillation box 1, the top of the distillation box 1 is communicated with a pressure gauge 20 through a pipeline, the collecting plates 3 are both sides above the inner wall of the distillation box 1 and are both fixedly connected with the, the top of the distillation box 1 is fixedly connected with a box body 5, the top of the distillation box 1 and the inside of the box body 5 are fixedly connected with a rotating motor 6, the rotating motor 6 is electrically connected with an external power supply, the output end of the rotating motor 6 is fixedly connected with a first rotating gear 7 through a connecting shaft, the connecting shaft is fixed with the output shaft of the rotating motor 6 through a coupler, the top of the inner cavity of the box body 5 is rotatably connected with a rotating shaft 8, the bottom end of the rotating shaft 8 sequentially penetrates through the distillation box 1 and the activated carbon adsorption layer 4 from top to bottom and extends to the bottom of the activated carbon adsorption layer 4, a second rotating gear 9 is fixedly connected above the outer surface of the rotating shaft 8, one side of the second rotating gear 9 is meshed with one side of the first rotating gear 7, a fixed rod 10 is fixedly connected below the outer surface of the rotating shaft 8, two fixed, the left side fixedly connected with scraper blade 12 of rotor plate 11, the inner wall of box 5 passes through fixing base fixedly connected with reagent adsorption plate 13, and reagent adsorption plate 13 can cooperate the fixing base to take off and be convenient for change.

When the device works, firstly, chemical reagents are poured into the collection box 14 from the feeding pipe 15, then, the pipe cover is covered, then, the air cylinder 16, the electromagnetic heating coil 21 and the vacuum pump 19 are simultaneously started, the vacuum meter 20 is observed, the air cylinder 16 is closed when the internal pressure of the distillation box 1 is enough, the liquid part of the chemical reagents flows to the bottom of the inner wall of the distillation box 1 through the filter plate 17, solid particles are remained in the collection box 14, after the chemical reagents are evaporated, steam passes through the reagent adsorption plate 13 and the activated carbon adsorption layer 4, so that the steam reaches the top of the distillation box 1 to be cooled to form water injection, falls onto the recollection plate 3, then leads out the water flow through the water outlet pipe 18, then, the rotating motor 6 is started to drive the first rotating gear 7 to rotate, further drive the second rotating gear 9 to rotate, further drive the rotating shaft 8 to rotate, so that the fixed rod 10 drives the scraper 12 on one side, thereby scraping off the dirt and finally pulling off the reagent adsorption plate 13.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a distillation plant for chemical reagent filters, includes distillation case (1), the equal fixedly connected with support (2) in both sides of distillation case (1) surface, its characterized in that: the utility model discloses a distillation box, including distillation box (1), the equal fixedly connected with collecting plate (3) in both sides of inner wall top, two fixedly connected with activated carbon adsorption layer (4) between collecting plate (3), the top fixedly connected with box (5) of distillation box (1), the top of distillation box (1) just is located the inside fixedly connected with rotation motor (6) of box (5), the output of rotation motor (6) is through connecting axle fixedly connected with first rotation gear (7), the top of box (5) inner chamber is rotated and is connected with pivot (8), the bottom of pivot (8) from last to running through distillation box (1) and activated carbon adsorption layer (4) in proper order and extending to the bottom of activated carbon adsorption layer (4), the top fixedly connected with second rotating gear (9) of pivot (8) surface, one side of second rotating gear (9) meshes with one side of first rotating gear (7), below fixedly connected with dead lever (10) of pivot (8) surface, the left end fixedly connected with rotor plate (11) of dead lever (10), the left side fixedly connected with scraper blade (12) of rotor plate (11), fixing base fixedly connected with reagent adsorption plate (13) is passed through to the inner wall of box (5).

2. A distillation apparatus for chemical reagent filtration according to claim 1, wherein: the improved distillation box is characterized in that the two sides of the inner wall of the distillation box (1) are fixedly connected with collecting boxes (14) through supporting rods, the front surfaces of the outer surfaces of the collecting boxes (14) are communicated with feeding pipes (15), one ends of the feeding pipes (15) penetrate through the distillation box (1) and extend to the outside of the distillation box (1), and the right side of the support (2) is fixedly connected with a cylinder (16).

3. A distillation apparatus for chemical reagent filtration according to claim 2, wherein: the output end of the air cylinder (16) is fixedly connected with a filter plate (17), and the right side of the filter plate (17) sequentially penetrates through the distillation box (1) and the collecting box (14) from left to right and penetrates through the outside of the collecting box (14).

4. A distillation apparatus for chemical reagent filtration according to claim 1, wherein: the water-saving distillation box is characterized in that water outlet pipes (18) are fixedly connected to the upper portions of two sides of the outer surface of the distillation box (1), and one ends of the water outlet pipes (18) penetrate through the distillation box (1) and extend into the distillation box (1).

5. A distillation apparatus for chemical reagent filtration according to claim 1, wherein: the top fixedly connected with vacuum pump (19) of support (2), the end of bleeding of vacuum pump (19) communicates with the right side of distillation case (1) surface, the top of distillation case (1) is through pipeline intercommunication there is manometer (20).

6. A distillation apparatus for chemical reagent filtration according to claim 1, wherein: the bottom of the distillation box (1) is fixedly connected with an electromagnetic heating coil (21), and the top of the electromagnetic heating coil (21) is fixedly connected with an electromagnetic heating block (22).