CN210752662U - Ethylene glycol antimony's reaction crystallization kettle device - Google Patents
Ethylene glycol antimony's reaction crystallization kettle device Download PDFInfo
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- CN210752662U CN210752662U CN201921508759.5U CN201921508759U CN210752662U CN 210752662 U CN210752662 U CN 210752662U CN 201921508759 U CN201921508759 U CN 201921508759U CN 210752662 U CN210752662 U CN 210752662U
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Abstract
The utility model discloses a ethylene glycol antimony's reaction crystallization cauldron device relates to the chemical industry technical field, specifically is an ethylene glycol antimony's reaction crystallization cauldron device, which comprises an outer shell, the inside of shell is provided with the endotheca, the top fixed mounting of shell has the upper cover, the top of upper cover is provided with the rotation motor, the fixed gear reducer that has cup jointed in pivot of rotating the motor, gear reducer's axis of rotation fixedly connected with montant, the side of montant is provided with rotates the seat, the fixed rotary rod that has cup jointed in inside of rotating the seat. This ethylene glycol antimony's reaction crystallization kettle device through set up rotary rod and horizontal puddler in the side of montant, stirs about and to the inside medium of endotheca respectively to avoided the medium because the inhomogeneous so that slow problem of reaction of mixing that the sediment leads to has shortened medium and has mixed and the time of reaction thereby improved the medium reaction efficiency among this crystallization kettle device.
Description
Technical Field
The utility model relates to the technical field of chemical industry, specifically a ethylene glycol antimony's reaction crystallization kettle device.
Background
The crystallization kettle is a crystallization device which needs chilled water or refrigerant water to be rapidly cooled in an interlayer after material mixing reaction, and the key links of the crystallization kettle are the size of the area of the interlayer, the structural form and the material outlet form of a stirrer, high-precision polishing in a tank body and the requirement of no dead angle in cleaning in the tank body so as to meet the use conditions of the process. The crystallization kettle is a mixing reaction device for domestic processes of material mixing, heating, cooling, stirring and the like in the industries of chemical industry, pharmacy, food and the like. Due to different processes and media, the materials are often inflammable, explosive, extremely toxic, and high in temperature and pressure. The stirring form, the rotating speed, the heating and cooling requirements of the equipment are different.
Puddler among traditional crystallization kettle can only be mostly rotatory on same water flat line along with the rotation of motor, this kind of stirring mode can only be better play the stirring to the medium on the same water flat line in the crystallization kettle about, can appear settling or the phenomenon of subsiding to some medium in the reaction, the top from crystallization kettle falls the below, the inhomogeneous phenomenon of mixing then can appear in the top in the crystallization kettle this moment then, thereby influence mix and the reaction between the medium, and some medium can the adhesion at crystallization kettle's inner wall after the reaction, cause material loss on the one hand also to influence the inside cleanness of crystallization kettle.
SUMMERY OF THE UTILITY MODEL
The utility model provides a to prior art not enough, the utility model provides a ethylene glycol antimony's reaction crystallization kettle device has solved the problem that proposes in the above-mentioned background art.
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes: a reaction crystallization kettle device of ethylene glycol antimony comprises a shell, wherein an inner sleeve is arranged inside the shell, an upper cover is fixedly arranged at the top of the shell, a rotating motor is arranged at the top of the upper cover, a rotating shaft of the rotating motor is fixedly sleeved with a gear reducer, a vertical rod is fixedly connected with a rotating shaft of the gear reducer, a rotating seat is arranged on the side surface of the vertical rod, a rotating rod is fixedly sleeved in the rotating seat, a longitudinal stirring rod is arranged on the outer wall of the rotating rod, a through groove is arranged on the side surface of the shell, a connecting rod is arranged in the through groove, two ends of the connecting rod are fixedly connected with scraping plates, the side edge of the scraper is connected with the inner wall of the inner sleeve in a sliding way, the middle part of the connecting rod is fixedly connected with a telescopic rod, the side of montant is provided with the horizontal puddler that is located the rotary rod below, the bottom fixedly connected with of montant prevents stifled bull stick.
Optionally, the inner wall of the outer shell is wave-shaped, a heat insulation layer is arranged between the inner wall and the outer wall of the outer shell, and cooling water is filled between the inner wall of the outer shell and the outer wall of the inner sleeve.
Optionally, the quantity of rotary rod is two, the surface of rotary rod is provided with two sets of vertical puddlers, and the quantity of every vertical puddler of group is three and evenly distributed in the side of vertical puddler, the rotary rod includes overcoat layer, interior loop bar and changes the pearl, the middle part activity of overcoat layer and interior loop bar has cup jointed changes the pearl, interior loop bar fixed connection is on rotating the seat.
Optionally, the scraper is shaped like a circular ring, and the connecting rod is perpendicular to the rotating rod.
Optionally, the surface of the upper cover is provided with an observer, the feed inlet is formed above the upper cover, the side faces of the outer shell are respectively provided with a position finder and a thermometer, one end of the position finder penetrates through the inner walls of the outer shell and the inner sleeve, and the outer walls of the two ends of the outer shell are respectively provided with a cooling water inlet and a cooling water outlet.
Optionally, the quantity of horizontal puddler is four and evenly distributed in the side of montant, the discharge gate has been seted up to the bottom of shell and endotheca, prevent stifled bull stick and be located discharge gate department, the surface of preventing stifled bull stick is provided with the flight.
The utility model provides a ethylene glycol antimony's reaction crystallization kettle device possesses following beneficial effect:
1. this ethylene glycol antimony's reaction crystallization kettle device through set up rotary rod and horizontal puddler in the side of montant, stirs about and to the inside medium of endotheca respectively to avoided the medium because the inhomogeneous so that slow problem of reaction of mixing that the sediment leads to has shortened medium and has mixed and the time of reaction thereby improved the medium reaction efficiency among this crystallization kettle device.
2. This ethylene glycol antimony's reaction crystallization kettle device, through set up on the montant with the equal mutually noninterfere's of rotary rod and horizontal puddler scraper blade, thereby strike off the medium on the endotheca inner wall totally when the ejection of compact, avoid the medium adhesion to cause the material loss and to the not good clear problem of inner chamber of endotheca at the inner wall of endotheca, thereby improved this reaction kettle device's practicality, and prevent stifled bull stick through the bottom setting at the montant, the jam condition of material export has greatly been reduced, guarantee the convenience that this crystallization kettle device used.
Drawings
FIG. 1 is a schematic structural view of the present invention;
fig. 2 is a cross-sectional view of the present invention;
fig. 3 is a side view of the rotating rod of the present invention.
In the figure: 1. a housing; 2. an inner sleeve; 3. a heat-insulating layer; 4. rotating the motor; 5. a gear reducer; 6. an upper cover; 7. an observer; 8. a feed inlet; 9. a vertical rod; 10. rotating the rod; 1001. an overcoat layer; 1002. an inner loop bar; 1003. rotating the beads; 11. a longitudinal stirring rod; 12. a transverse stirring rod; 13. an anti-blocking rotating rod; 14. a discharge port; 15. a cooling water inlet; 16. a cooling water outlet; 17. a position finder; 18. a squeegee; 19. a telescopic rod; 20. a connecting rod.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1 to 3, the present invention provides a technical solution: a reaction crystallization kettle device of ethylene glycol antimony comprises a shell 1, an inner sleeve 2 is arranged inside the shell 1, an upper cover 6 is fixedly installed at the top of the shell 1, a rotating motor 4 is arranged at the top of the upper cover 6, a gear reducer 5 is fixedly sleeved on a rotating shaft of the rotating motor 4, a vertical rod 9 is fixedly connected with the rotating shaft of the gear reducer 5, a rotating seat is arranged on the side surface of the vertical rod 9, a rotating rod 10 is fixedly sleeved inside the rotating seat, a longitudinal stirring rod 11 is arranged on the outer wall of the rotating rod 10, a through groove is formed in the side surface of the shell 1, a connecting rod 20 is arranged inside the through groove, scraping plates 18 are fixedly connected to the two ends of the connecting rod 20, the side edges of the scraping plates 18 are slidably connected with the inner wall of the inner sleeve 2, a telescopic rod 19 is fixedly connected to the middle of the connecting rod 20, the telescopic rod 19 can be, thereby can guarantee scraping off of medium on the inner wall of inner sleeve 2 by scraper blade 18, the side of montant 9 is provided with the horizontal puddler 12 that is located the rotary rod 10 below, and the bottom fixedly connected with of montant 9 prevents stifled bull stick 13, prevents stifled bull stick 13 and dredges discharge gate 14 department under the rotation of montant 9, makes the better outflow of medium.
The inner wall of the outer shell 1 is wavy, the heat insulation layer 3 is arranged between the inner wall and the outer wall of the outer shell 1, cooling water is filled between the inner wall of the outer shell 1 and the outer wall of the inner sleeve 2, the inner wall of the outer shell 1 is wavy, and the wavy side faces are beneficial to increasing the area and increasing the volume of the cold water in a jacket formed by the outer shell 1 and the inner sleeve 2 at the same height, so that the cold water speed of a medium in the inner sleeve 2 is increased, and the cooling efficiency of the medium is improved.
Wherein, the quantity of rotary rod 10 is two, the surface of rotary rod 10 is provided with two sets of vertical puddlers 11, the quantity of every vertical puddler 11 of group is three and evenly distributed in the side of vertical puddler 11, rotary rod 10 includes overcoat layer 1001, interior loop bar 1002 with change pearl 1003, overcoat layer 1001 has cup jointed with the middle part activity of interior loop bar 1002 and has changeed pearl 1003, interior loop bar 1002 fixed connection is on rotating the seat, inclination is 120 degrees between the vertical puddler 11 of every group, the rotation of changeing pearl 1003 has guaranteed that vertical puddler 11 can rotate when the pressure of receiving the medium, thereby it overturns from top to bottom to drive the medium, reach the purpose of stirring the medium from top to bottom, it subsides to place the medium.
The scraper 18 is shaped like a circular ring, the connecting rod 20 is perpendicular to the rotating rod 10, the connecting rod 20 and the rotating rod 10 are respectively located on the side faces of the vertical rod 9, and the connecting rod 20 cannot touch the rotating rod 10 when moving downwards, so that the scraper 18 is guaranteed to move downwards to scrape media on the inner wall of the inner sleeve 2 completely.
Wherein, the surface of upper cover 6 is provided with viewer 7, upper cover 6 has seted up feed inlet 8 in the top, the side of shell 1 is provided with position finder 17 and thermometer respectively, the inner wall of shell 1 and endotheca 2 is run through to one end of position finder 17, the outer wall at shell 1 both ends is provided with cooling water inlet 15 and cooling water outlet 16 respectively, viewer 7 is used for observing the reaction condition of medium in endotheca 2, feed inlet 8 is used for sending the medium into the inner chamber of endotheca 2, the thermometer measures the temperature, position finder 17 utilizes the liquid level height of medium in endotheca 2 of U type pipe characteristic measurement.
Wherein, the quantity of horizontal puddler 12 is four and evenly distributed in the side of montant 9, and discharge gate 14 has been seted up to the bottom of shell 1 and endotheca 2, prevents stifled bull stick 13 and is located discharge gate 14 department, prevents stifled bull stick 13's surface and is provided with the flight, and the flight is the state of decurrent rotation under the rotation of montant 9 to drive the medium and flow to discharge gate 14 department, avoid discharge gate 14 department to block up.
In conclusion, when the ethylene glycol antimony reaction crystallization kettle device is used, firstly, a medium is placed into an inner cavity of an inner sleeve 2 through a feed inlet 8, then the feed inlet 8 is sealed, a rotating motor 4 is started to drive a vertical rod 9 to rotate, the medium presses a longitudinal stirring rod 11 arranged on a rotating rod 10 due to the irregular movement of the medium in the inner sleeve 2, the longitudinal stirring rod 11 drives an outer sleeve layer 1001 to rotate around an inner sleeve rod 1002 to stir the medium up and down, secondly, cooling water is pumped into the inner cavity between an outer shell 1 and the inner sleeve 2 from a cooling water inlet 15 and flows out from a cooling water outlet 16, so that the medium in the inner sleeve 2 is cooled, the temperature of the medium in the inner cavity of the inner sleeve 2 can be observed through a thermometer, meanwhile, the liquid level height of liquid in the inner cavity of the inner sleeve 2 is observed according to a position finder 17, the reaction condition inside the inner sleeve 2 is observed through an observer, and finally, opening a valve on the discharge port 14, allowing the reacted medium to flow out of the inner sleeve 2, extending the telescopic rod 19 to push the connecting rod 20 to drive the scraper 18 to move downwards to scrape the medium on the inner wall of the inner sleeve 2, and driving the medium to flow to the discharge port 14 by the rotation of the auger on the surface of the anti-blocking rotating rod 13.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (6)
1. The utility model provides a ethylene glycol antimony's reaction crystallization kettle device, includes shell (1), its characterized in that: the inner sleeve (2) is arranged in the shell (1), an upper cover (6) is fixedly mounted at the top of the shell (1), a rotating motor (4) is arranged at the top of the upper cover (6), a gear reducer (5) is fixedly sleeved on a rotating shaft of the rotating motor (4), a vertical rod (9) is fixedly connected with a rotating shaft of the gear reducer (5), a rotating seat is arranged on the side surface of the vertical rod (9), a rotating rod (10) is fixedly sleeved in the rotating seat, a longitudinal stirring rod (11) is arranged on the outer wall of the rotating rod (10), a through groove is formed in the side surface of the shell (1), a connecting rod (20) is arranged in the through groove, scrapers (18) are fixedly connected to the two ends of the connecting rod (20), the side edges of the scrapers (18) are slidably connected with the inner wall of the inner sleeve (2), and a telescopic rod (19) is, the side of montant (9) is provided with horizontal puddler (12) that are located rotary rod (10) below, the bottom fixedly connected with of montant (9) prevents stifled bull stick (13).
2. The ethylene glycol antimony reaction crystallization kettle device according to claim 1, characterized in that: the inner wall of the outer shell (1) is wave-shaped, a heat insulation layer (3) is arranged between the inner wall and the outer wall of the outer shell (1), and cooling water is filled between the inner wall of the outer shell (1) and the outer wall of the inner sleeve (2).
3. The ethylene glycol antimony reaction crystallization kettle device according to claim 1, characterized in that: the quantity of rotary rod (10) is two, the surface of rotary rod (10) is provided with two sets of vertical puddler (11), and the quantity of every vertical puddler of group (11) is three and evenly distributed in the side of vertical puddler (11), rotary rod (10) are including overcoat layer (1001), interior loop bar (1002) and change pearl (1003), overcoat layer (1001) has cup jointed with the middle part activity of interior loop bar (1002) and has changeed pearl (1003), interior loop bar (1002) fixed connection is on rotating the seat.
4. The ethylene glycol antimony reaction crystallization kettle device according to claim 1, characterized in that: the scraper (18) is arranged in a ring shape, and the connecting rod (20) is perpendicular to the rotating rod (10).
5. The ethylene glycol antimony reaction crystallization kettle device according to claim 1, characterized in that: the surface of upper cover (6) is provided with viewer (7), feed inlet (8) have been seted up to the top of upper cover (6), the side of shell (1) is provided with position finder (17) and thermometer respectively, the inner wall of shell (1) and endotheca (2) is run through to the one end of position finder (17), the outer wall at shell (1) both ends is provided with cooling water inlet (15) and cooling water outlet (16) respectively.
6. The ethylene glycol antimony reaction crystallization kettle device according to claim 1, characterized in that: the quantity of horizontal puddler (12) is four and evenly distributed in the side of montant (9), discharge gate (14) have been seted up to the bottom of shell (1) and endotheca (2), prevent stifled bull stick (13) and be located discharge gate (14) department, the surface of preventing stifled bull stick (13) is provided with the flight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921508759.5U CN210752662U (en) | 2019-09-09 | 2019-09-09 | Ethylene glycol antimony's reaction crystallization kettle device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921508759.5U CN210752662U (en) | 2019-09-09 | 2019-09-09 | Ethylene glycol antimony's reaction crystallization kettle device |
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| Publication Number | Publication Date |
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| CN210752662U true CN210752662U (en) | 2020-06-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201921508759.5U Active CN210752662U (en) | 2019-09-09 | 2019-09-09 | Ethylene glycol antimony's reaction crystallization kettle device |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115007098A (en) * | 2022-05-27 | 2022-09-06 | 扬州宏远新材料股份有限公司 | Organic silicon oil anti-sticking reaction equipment convenient for discharging |
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2019
- 2019-09-09 CN CN201921508759.5U patent/CN210752662U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115007098A (en) * | 2022-05-27 | 2022-09-06 | 扬州宏远新材料股份有限公司 | Organic silicon oil anti-sticking reaction equipment convenient for discharging |
| CN115007098B (en) * | 2022-05-27 | 2023-09-19 | 扬州宏远新材料股份有限公司 | Organic silicone oil anti-sticking reaction equipment convenient to ejection of compact |
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