CN210665229U - Detection equipment for vanadium content in ore - Google Patents

Detection equipment for vanadium content in ore Download PDF

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Publication number
CN210665229U
CN210665229U CN201921687696.4U CN201921687696U CN210665229U CN 210665229 U CN210665229 U CN 210665229U CN 201921687696 U CN201921687696 U CN 201921687696U CN 210665229 U CN210665229 U CN 210665229U
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CN
China
Prior art keywords
liquid storage
box body
storage bottle
hole
opening
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Expired - Fee Related
Application number
CN201921687696.4U
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Chinese (zh)
Inventor
袁光辉
张萍
耿敏
刘冲
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Ankang Hi Tech Hanergy Technology Co Ltd
Ankang University
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Ankang Hi Tech Hanergy Technology Co Ltd
Ankang University
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Priority to CN201921687696.4U priority Critical patent/CN210665229U/en
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Publication of CN210665229U publication Critical patent/CN210665229U/en
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Abstract

The utility model discloses a check out test set of vanadium content in ore belongs to analysis technical field. The apparatus comprises: a box body; the front side of the box body is provided with an opening and closing door, the bottom of the rear side is provided with a first through hole, the top of the box body is provided with a first feeding port, a second feeding port and a third feeding port, the top end of the box body is connected with a crushing device, and the bottom end of the box body is connected with a supporting table, a first liquid storage bottle and a spectrophotometer; the opening and closing door is provided with a switch button and a display screen, and a controller is arranged in the display screen; a first charging pipe is arranged below the second charging opening; a second feeding pipe is arranged below the third feeding port; a temperature control device is arranged inside the supporting table, and a second liquid storage bottle is arranged at the top of the supporting table. The utility model discloses well reducing mechanism smashes the ore, then handles in second stock solution bottle and first stock solution bottle, and spectrophotometer detects at last, and whole experimentation does not need the staff to carry out too much participation to the labour has been practiced thrift.

Description

Detection equipment for vanadium content in ore
Technical Field
The utility model relates to an analysis technical field, in particular to check out test set of vanadium content in ore.
Background
Vanadium is silver white metal, melting point is 1890 deg.C, boiling point is 3380 deg.C, and density is 6.110g/cm3Niobium, tantalum, tungsten, molybdenum, and are also known as refractory metals, are ductile, hard, non-magnetic, not easily oxidized in air, soluble in hydrofluoric acid, nitric acid, and aqua regia, and not easily corroded, and are also quite stable in alkali, sulfuric acid, and hydrochloric acid. Vanadium is widely used in the industries of metallurgy, aerospace, chemical industry, batteries and the like in the forms of ferrovanadium, vanadium compounds and metal vanadium. In nature, vanadium rarely forms an independent mineral, mainly occurring in vanadium titano-magnetite, phosphate rock, uranium-bearing sandstone and siltstone, and in addition, a large amount of vanadium occurs in bauxite and carbonaceous materials such as petroleum and coal.
In the prior art, when vanadium in ore is detected, a laboratory technician is required to mix and react a sample and a reagent according to a certain sequence, and then a spectrophotometer is used for measuring an absorbance value, so that a large amount of samples are usually taken in order to obtain high accuracy. However, when the sample size is large, the testing process takes a lot of labor and time, and a large error is generated when different personnel operate.
SUMMERY OF THE UTILITY MODEL
In order to make the content of vanadium in the more accurate quick detection ore, the utility model provides a detection equipment of vanadium content in ore. The technical scheme is as follows:
the equipment for detecting the content of vanadium in ore comprises a box body; the front side of the box body is provided with an opening and closing door, the bottom of the rear side is provided with a first through hole, the top of the box body is provided with a first feeding port, a second feeding port and a third feeding port, the top end of the box body is connected with a crushing device, and the bottom end of the box body is connected with a supporting table, a first liquid storage bottle and a spectrophotometer; the opening and closing door is provided with a switch button and a display screen, and a controller is arranged in the display screen; a first feeding pipe is arranged below the second feeding port; a second feeding pipe is arranged below the third feeding port; a temperature control device is arranged inside the supporting table, and a second liquid storage bottle is arranged at the top of the supporting table; a second through hole is formed below the side wall of the first liquid storage bottle, the second through hole is connected with the first through hole through a liquid discharge pipe, and a first switch valve is arranged on the liquid discharge pipe; a telescopic pipette is arranged on the spectrophotometer;
the crushing device is connected below the first charging opening and comprises a crushing roller and a conveying belt from top to bottom, a feed opening is arranged below the right wall, and the feed opening is connected with a feed plate; a third through hole is formed below the side wall of the second liquid storage bottle, a discharge pipe is connected to the third through hole, and a second switch valve is arranged on the discharge pipe;
and the spectrophotometer, the switch button, the display screen, the temperature control device, the telescopic pipette, the crushing roller, the conveyer belt, the first switch valve and the second switch valve are all in communication connection with the controller.
Furthermore, a filter is arranged on the discharge pipe.
Further, first stock solution bottle with second stock solution bottle bottom is provided with first agitator and second agitator respectively, just first agitator with the second agitator all with the controller carries out communication connection.
Further, still be provided with first counter and second counter on discharging pipe and the flexible pipette respectively, just first counter with the second counter all with controller carries out communication connection.
Further, the telescopic pipette is movably connected with the spectrophotometer.
Further, a handle is arranged on the opening and closing door.
Further, the display screen is a touch display screen.
Furthermore, the material of the opening and closing door is transparent material.
Furthermore, an opening and closing cover is connected to the first feeding port.
Furthermore, the bottom of the box body is provided with universal wheels.
The utility model provides a technical scheme's beneficial effect is: the utility model discloses well reducing mechanism smashes the ore, then handles in second stock solution bottle and first stock solution bottle, and spectrophotometer detects at last, and whole experimentation does not need the staff to carry out too much participation to the labour has been practiced thrift. Secondly, each component is controlled to operate accurately through the display screen, so that detected data are more accurate.
Drawings
Fig. 1 is a schematic structural diagram of a device for detecting vanadium content in ore provided by the present invention.
Reference numerals: 1-a box body; 2, opening and closing the door; 3-a first via; 4-a first feed inlet; 5-a second feed inlet; 6-a third feed inlet; 7-a crushing device; 8, supporting the table; 9-a first liquid storage bottle; 10-a spectrophotometer; 11-a switch button; 12-a display screen; 13-a controller; 14-a first feed tube; 15-a second feed tube; 16-a temperature control device; 17-a second liquid storage bottle; 18-a second through-hole; 19-a drain pipe; 20-a first on-off valve; 21-a telescopic pipette; 22-a crushing roller; 23-a conveyor belt; 24-a feed opening; 25-blanking plate; 26-a third via; 27-a discharge pipe; 28-a second on-off valve; 29-a filter; 30-a first stirrer; 31-a second stirrer; 32-a first meter; 33-a second meter; 34-a handle; 35-opening and closing the cover; 36-universal wheel.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer, embodiments of the present invention will be described in further detail below with reference to the accompanying drawings.
It will be understood that when an element is referred to as being "connected" to another element, it can be directly connected to the other element or intervening elements may also be present. The use of the terms "upper", "lower", "left", "right" and the like in the present invention is for illustrative purposes only.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
Fig. 1 is a schematic structural diagram of a device for detecting vanadium content in ore provided by the present invention. Referring to fig. 1, the apparatus includes a case 1; the front side of the box body 1 is provided with an opening and closing door 2, the bottom of the rear side is provided with a first through hole 3, the top of the box body is provided with a first feeding hole 4, a second feeding hole 5 and a third feeding hole 6, the top end of the box body is connected with a crushing device 7, and the bottom end of the box body is connected with a support table 8, a first liquid storage bottle 9 and a spectrophotometer 10; the opening and closing door 2 is provided with a switch button 11 and a display screen 12, and a controller 13 is arranged inside the display screen 12; a first feeding pipe 14 is arranged below the second feeding port 5; a second feeding pipe 15 is arranged below the third feeding port 6; a temperature control device 16 is arranged in the support table 8, and a second liquid storage bottle 17 is arranged at the top of the support table; a second through hole 18 is formed below the side wall of the first liquid storage bottle 9, the second through hole 18 is connected with the first through hole 3 through a liquid discharge pipe 19, and a first switch valve 20 is arranged on the liquid discharge pipe 19; the spectrophotometer 10 is provided with a telescopic pipette 21;
the crushing device 7 is connected below the first charging hole 4 and comprises a crushing roller 22 and a conveyer belt 23 from top to bottom, a feed opening 24 is arranged below the right wall, and the feed opening 24 is connected with a feed plate 25; a third through hole 26 is formed below the side wall of the second liquid storage bottle 17, a discharge pipe 27 is connected to the third through hole 26, and a second switch valve 28 is arranged on the discharge pipe 27; and the spectrophotometer 10, the switch button 11, the display screen 12, the temperature control device 16, the telescopic pipette 21, the crushing roller 22, the conveyer belt 23, the first switch valve 20 and the second switch valve 28 are all in communication connection with the controller 13.
Wherein, the ore to be detected is added from the first charging hole 4, crushed by the crushing roller 22 and dropped onto the conveyer belt 23, and then dropped into the second liquid storage bottle 17 through the feed opening 24 and the feed plate 25; the second feed opening 5 is used for adding required chemical reagents, and the chemical reagents enter the second liquid storage bottle 17 through the first feed pipe 14 to dissolve ores added into the second liquid storage bottle 17; the second switch valve 28 is opened, and the dissolved solution in the second liquid storage bottle 17 enters the discharge pipe 27 through the third through hole 26 and then flows into the first liquid storage bottle 9; the third feed inlet 6 is used for adding required deionized water or chemical reagents, and then enters the first liquid storage bottle 9 through the second feed pipe 15 to dilute the solution dissolved in the first liquid storage bottle 9; the spectrophotometer 10 is used for detecting the diluted solution sucked from the first liquid storage bottle 9 by the telescopic pipette 21; the switch button 11 is used to turn the device on and off; the support table 8 is used for supporting a second liquid storage bottle 17; the display screen 12 is used for displaying the detection data; the controller 13 is used for controlling the spectrophotometer 10, the switch button 11, the display screen 12, the temperature control device 16, the telescopic pipette 21, the crushing roller 22, the conveyer belt 23, the first switch valve 20 and the second switch valve 28 to work; the temperature control device 16 is used for heating or refrigerating the second liquid storage bottle 17; when the first switch valve 20 is opened, the solution in the first liquid storage bottle 9 enters the liquid discharge pipe 19 through the second through hole 18 and then is discharged out of the box body 1 through the first through hole 3.
The crushing device 7 is fixedly connected with the top of the box body 1, and the support table 8, the first liquid storage bottle 9 and the spectrophotometer 10 are fixedly connected with the bottom of the box body 1; the second liquid storage bottle 17 is placed at the top of the supporting table 8 and is not connected with the supporting table 8, so that the second liquid storage bottle 17 is cleaned after detection is finished. Wherein, the fixed connection can be bolt connection or bonding.
It should be further noted that the front end of the blanking plate 25 is close to the left side of the second liquid storage bottle 17, and the orifice of the first feeding pipe 14 is close to the right side of the second liquid storage bottle 17; the orifice of the discharge pipe 27 is close to the left side of the first liquid storage bottle 9, and the orifice of the second feed pipe 15 is close to the rear side of the first liquid storage bottle 9, so that the telescopic pipette 21 can suck the solution in the first liquid storage bottle 9.
In addition, a communication connection is a connection method for transmitting information by using an electric signal. Converting a message from a source into an electrical signal, then encoding, modulating, amplifying or transmitting the electrical signal by a transmitting device, and converting a baseband signal into a form suitable for transmission in a transmission medium; and the information is transmitted through a transmission medium, and is subjected to inverse transformation at a receiving end through receiving end equipment to be recovered into information which is provided for a receiver. Such point-to-point communication is mostly bi-directional. Therefore, both ends where the communication partner is located are provided with the transmitting and receiving devices. I.e. two components that are communicatively connected may transmit signals to each other.
Furthermore, a filter 29 is disposed on the discharge pipe 27 to prevent the insoluble substances in the second liquid storage bottle 17 from entering the discharge pipe 27, thereby preventing the discharge pipe 27 and the discharge pipe 19 from being clogged.
Further, the first stirrer 30 and the second stirrer 31 are respectively arranged at the bottom of the first liquid storage bottle 9 and the bottom of the second liquid storage bottle 17, and the first stirrer 30 and the second stirrer 31 are both in communication connection with the controller 13. It should be noted that when the ore is dissolved in the second liquid storage bottle 17, the stirring of the second stirrer 31 can accelerate the dissolution of the ore, so that the time can be saved; when diluting the ore solution that dissolves in first stock solution bottle 9, first agitator 30 can make the more even of solution mixing to can make the data that detect more accurate.
Further, a first gauge 32 and a second gauge 33 are respectively disposed on the discharging pipe 27 and the telescopic pipette 21, and the first gauge 32 and the second gauge 33 are both in communication connection with the controller 13.
It should be noted that when the ore solution dissolved in the second liquid storage bottle 17 flows into the first liquid storage bottle 9, the volume of the flowing ore solution needs to be accurately determined, so that the content of vanadium in the ore can be calculated after the detection is completed; the cuvette (not shown in the figure) volume among the spectrophotometer 10 is less, when drawing the solution that needs to detect in flexible pipette 21 toward the cuvette (not shown in the figure), the volume that needs the control to draw prevents to draw too much for the solution overflows the cuvette (not shown in the figure), thereby avoids influencing testing result and damaging spectrophotometer 10.
Further, a telescopic pipette 21 is movably connected to the spectrophotometer 10. It should be noted that the telescopic pipette 21 can rotate left and right, and also can be extended up and down, left and right, so that the solution to be detected can be more conveniently sucked into a cuvette (not shown) in the spectrophotometer 10.
Further, the opening and closing door 2 is provided with a handle 34, so that the opening and closing door 2 can be opened and closed more conveniently.
Further, the display 12 is a touch display.
It should be noted that, the display screen 12 can display the setting control of the component included in the detection device for vanadium content in ore, when the worker needs to set the working parameter of a certain component, the setting control corresponding to the component on the display screen 12 can be clicked, the setting interface corresponding to the component can be displayed on the display screen 12 at this moment, and then the worker can set the component through the opening or closing control on the display screen 12. For example, if the worker needs to open the first stirrer 30, the worker only needs to click the control corresponding to the first stirrer 30 on the display screen 12, at this time, an interface for setting to open is displayed on the display screen 12, and the worker can click the open control to operate the first stirrer 30.
Furthermore, the material of the opening and closing door 2 is transparent material, so that the operation condition of each component in the box body 1 can be conveniently observed by a worker.
Further, the opening/closing cover 35 is connected to the first charging port 4, so that the ore can be prevented from being splashed out of the crushing apparatus 7 when the crushing drum 22 crushes the ore.
Further, the bottom of the case 1 is provided with universal wheels 36 so that the apparatus can be moved more conveniently.
Further, the bottoms of the first liquid storage bottle 9 and the second liquid storage bottle 17 can be further provided with a pH detector (not shown in the figure), so that the pH value of the solution in the first liquid storage bottle 9 and the second liquid storage bottle 17 can be detected in real time.
The utility model discloses a complete work flow can be: the staff presses shift knob 11 to start this equipment, the staff clicks crushing roller 22's setting control on display screen 12 after the start, can show crushing roller 22's setting interface on display screen 12 this moment, the staff clicks and opens the control, display screen 12 can send first working signal to controller 13 this moment, controller 13 sends second working signal to crushing roller 22 after receiving first working signal, crushing roller 22 begins to rotate after receiving the second working signal. After the rotation, the operator makes the conveyor belt 23 start to rotate through the display 12. Then, the staff opens the opening and closing cover 35, and a certain amount of ore is weighed and put on the crushing roller 22, and the crushing roller 22 crushes the ore, and the crushed ore falls into the conveyer belt 23, and through the rotation of conveyer belt 23 for the crushed ore enters into the second liquid storage bottle 17 through the blanking plate 25. Thereafter, the worker may add a certain amount of a desired chemical through the second feed opening 5 and then rotate the second agitator 31 through the display 12. If the solution in the second liquid storage bottle 17 needs to be heated, the operator can control the temperature control device 16 to heat the second liquid storage bottle 17 to the required temperature through the display screen 12.
After the above steps, the staff can observe whether the reaction is completed through the opening and closing door 2, and after the reaction is completed, the staff opens the second switch valve 28 through the display screen 12, so that a certain amount of solution after the reaction flows into the first liquid storage bottle 9, then a certain amount of deionized water or required chemical reagent is added through the third feed opening 6, and after the addition, the first stirrer 30 is opened through the display screen 12. After stirring and predetermineeing the time length, the staff can open spectrophotometer 10 through display screen 12, preheat spectrophotometer, set for the wavelength, then the staff can open the first cell (not shown in the figure) of shutter 2 in spectrophotometer 10 and add distilled water, afterwards, the staff absorbs a certain amount of solution from first stock solution bottle 9 through display screen 12 control flexible pipette 21, put into spectrophotometer 10's second cell (not shown in the figure), then transfer T to spectrophotometer 10 through display screen 12, then let spectrophotometer 10 carry out the absorbance value that detects the solution, after the detection is accomplished, spectrophotometer 10 sends data to controller 13, controller 13 receives the back and sends to display screen 12, display screen 12 receives and shows on the screen after the data. And recording the data by the staff.
It is worth explaining, the utility model discloses well reducing mechanism smashes the ore, then handles in second stock solution bottle and first stock solution bottle, and spectrophotometer detects at last, and whole experimentation does not need the staff to carry out too much participation to the labour has been practiced thrift. Secondly, each component is controlled to operate accurately through the display screen, so that detected data are more accurate.
The above description is only for the preferred embodiment of the present invention, and is not intended to limit the present invention, and any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention should be included within the protection scope of the present invention.

Claims (10)

1. The equipment for detecting the content of vanadium in ore is characterized by comprising a box body (1); the front side of the box body (1) is provided with an opening and closing door (2), the bottom of the rear side is provided with a first through hole (3), the top of the box body is provided with a first feeding hole (4), a second feeding hole (5) and a third feeding hole (6), the top end of the box body is connected with a crushing device (7), and the bottom end of the box body is connected with a supporting table (8), a first liquid storage bottle (9) and a spectrophotometer (10); the opening and closing door (2) is provided with a switch button (11) and a display screen (12), and a controller (13) is arranged inside the display screen (12); a first feeding pipe (14) is arranged below the second feeding port (5); a second feeding pipe (15) is arranged below the third feeding port (6); a temperature control device (16) is arranged in the support table (8), and a second liquid storage bottle (17) is arranged at the top of the support table; a second through hole (18) is formed below the side wall of the first liquid storage bottle (9), the second through hole (18) is connected with the first through hole (3) through a liquid discharge pipe (19), and a first switch valve (20) is arranged on the liquid discharge pipe (19); a telescopic pipette (21) is arranged on the spectrophotometer (10);
the crushing device (7) is connected below the first charging hole (4), and comprises a crushing roller (22) and a conveying belt (23) from top to bottom, a feed opening (24) is arranged below the right wall, and the feed opening (24) is connected with a feed plate (25); a third through hole (26) is formed below the side wall of the second liquid storage bottle (17), a discharge pipe (27) is connected to the third through hole (26), and a second switch valve (28) is arranged on the discharge pipe (27);
and the spectrophotometer (10), the switch button (11), the display screen (12), the temperature control device (16), the telescopic pipette (21), the crushing roller (22), the conveyer belt (23), the first switch valve (20) and the second switch valve (28) are in communication connection with the controller (13).
2. The apparatus for detecting the vanadium content in ores according to claim 1, wherein a filter (29) is further provided on the tapping pipe (27).
3. The device for detecting the vanadium content in the ore according to claim 1, wherein a first stirrer (30) and a second stirrer (31) are respectively arranged at the bottoms of the first liquid storage bottle (9) and the second liquid storage bottle (17), and the first stirrer (30) and the second stirrer (31) are in communication connection with the controller (13).
4. The apparatus for detecting vanadium content in ore according to claim 1, wherein a first meter (32) and a second meter (33) are respectively arranged on the discharge pipe (27) and the telescopic pipette (21), and the first meter (32) and the second meter (33) are both in communication connection with the controller (13).
5. The apparatus for detecting the vanadium content in ores according to claim 1, wherein the telescopic pipette (21) is movably connected to the spectrophotometer (10).
6. The equipment for detecting the content of vanadium in ore according to claim 1, characterized in that the opening and closing door (2) is provided with a handle (34).
7. The apparatus for detecting vanadium content in ore according to claim 1, wherein the display screen (12) is a touch display screen.
8. The equipment for detecting the content of vanadium in ore according to claim 1, characterized in that the material of the opening and closing door (2) is transparent.
9. The equipment for detecting the content of vanadium in ore according to claim 1, wherein an opening and closing cover (35) is connected to the first feeding port (4).
10. The apparatus for detecting vanadium content in ore according to claim 1, characterized in that the bottom of the box body (1) is provided with universal wheels (36).
CN201921687696.4U 2019-10-10 2019-10-10 Detection equipment for vanadium content in ore Expired - Fee Related CN210665229U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921687696.4U CN210665229U (en) 2019-10-10 2019-10-10 Detection equipment for vanadium content in ore

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921687696.4U CN210665229U (en) 2019-10-10 2019-10-10 Detection equipment for vanadium content in ore

Publications (1)

Publication Number Publication Date
CN210665229U true CN210665229U (en) 2020-06-02

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Application Number Title Priority Date Filing Date
CN201921687696.4U Expired - Fee Related CN210665229U (en) 2019-10-10 2019-10-10 Detection equipment for vanadium content in ore

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112098590A (en) * 2020-09-07 2020-12-18 央测(北京)检测技术研究院 Detection equipment for vanadium content in ore

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112098590A (en) * 2020-09-07 2020-12-18 央测(北京)检测技术研究院 Detection equipment for vanadium content in ore

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