CN210656157U - Quenching synthesizer for preparing insoluble sulfur - Google Patents

Abstract

The utility model discloses a quenching synthesizer for preparing insoluble sulfur, which comprises a synthesizer body, wherein an inlet pipe penetrates through the middle of the top of the synthesizer body, the inner wall of the inlet pipe is connected with a movable plate through a torsion spring, a liquid inlet pipe penetrates through the upper part of one side of the synthesizer body, the two sides inside the synthesizer body are connected with a treatment chamber through connecting pieces, a discharge port penetrates through the lower part of one side of the treatment chamber, the inner wall of the discharge port is connected with an electronic valve, a guide plate is connected with the lower part inside the treatment chamber, the quenching synthesizer for preparing insoluble sulfur is also provided with a heater, after quenching high-temperature sulfur, a user can start the heater to electrify a metal resistor inside the heater to emit heat to heat the sulfur and the quenching liquid, thereby promoting the evaporation of the quenching liquid and discharging the quenching liquid through an exhaust pipe, thereby reducing the preparation time of the sulfur and greatly improving the production efficiency of the sulfur.

Description

Quenching synthesizer for preparing insoluble sulfur

Technical Field

The utility model relates to the technical field of quenching synthesis of insoluble sulfur, in particular to a quenching synthesizer for preparing insoluble sulfur.

Background

Insoluble sulfur is elastic sulfur with a transparent and amorphous chain structure, which is obtained by heating sulfur powder to boiling (444.6 ℃) and quenching the sulfur powder in cold water, and most (65-95%) of the elastic sulfur is insoluble in carbon disulfide, so the elastic sulfur is called insoluble sulfur.

The existing quenching synthesizer for preparing insoluble sulfur is mostly used for directly spraying high-temperature sulfur into a container filled with circulating quenching liquid when quenching the high-temperature sulfur, but the method is difficult to uniformly cool the temperature of the sulfur when in use, and causes large consumption of the quenching medium, thereby causing waste of the quenching liquid, and the existing synthesizer is difficult to dry the sulfur in time after quenching the quenching liquid, thereby causing longer time for preparing the sulfur by the synthesizer, and greatly reducing the production efficiency of the sulfur.

Disclosure of Invention

An object of the utility model is to provide a quench synthesizer of preparation insolubility sulphur to the temperature that is difficult to make sulphur that proposes in solving above-mentioned background art carries out even cooling, and causes the quenching agent quantity great, leads to the quenching liquid extravagant, is difficult to timely carry out the drying to sulphur, thereby leads to the synthesizer to prepare the time of sulphur longer, has reduced the production efficiency's of sulphur problem greatly.

In order to achieve the above object, the utility model provides a following technical scheme:

a quenching synthesizer for preparing insoluble sulfur comprises a synthesizer body, wherein an inlet pipe penetrates through the middle of the top of the synthesizer body, the inner wall of the inlet pipe is connected with a movable plate through a torsion spring, a liquid inlet pipe penetrates through the upper portion of one side of the synthesizer body, both sides of the interior of the synthesizer body are connected with a treatment chamber through connecting pieces, a discharge port penetrates through the lower portion of one side of the treatment chamber, the inner wall of the discharge port is connected with an electronic valve, a guide plate is connected with the lower portion of the interior of the treatment chamber, both sides of the interior of the treatment chamber are connected with heaters, a motor is connected with the lower portion of the interior of the synthesizer body, the output end of the motor is connected with a stirring fan through a rotating shaft, supporting legs are connected to four corners of the bottom of the synthesizer body, a nitrogen chamber is connected to the other side of the, an air pump is connected to the middle of the top of the nitrogen chamber, an air inlet end of the air pump is connected with an air exhaust pipe, an air outlet end of the air pump is connected with an air delivery pipe, a pressurizing chamber is connected to the upper portion inside the synthesizer body, the bottom of the pressurizing chamber is connected with a first nozzle, and an exhaust pipe is connected to the upper portion of one side of the treatment chamber; the motor, the electronic valve, the heater and the stirring fan are all electrically connected with an external power supply and are provided with a controller.

Preferably, a plurality of activated carbon layers are arranged in the exhaust pipe, and the activated carbon layers are equidistantly distributed in the exhaust pipe.

Preferably, the two heaters are welded to both sides of the inside of the processing chamber, and the two heaters are symmetrically arranged with the center line of the length of the processing chamber as the center.

Preferably, one end of the liquid inlet pipe penetrates through the upper sides of the synthesizer body and the processing chamber in sequence and extends into the processing chamber, and one end of the liquid inlet pipe is connected with the second spray head.

Preferably, the stirring fan is sleeved on the outer surface of one end, far away from the motor, of the rotating shaft, and is made of stainless steel materials.

Preferably, the number of the torsion springs is two, and the two torsion springs are both made of manganese steel materials.

Preferably, the quenching liquid is a glycerol aqueous solution with the mass concentration of 15-30%.

Compared with the prior art, the beneficial effects of the utility model are that:

the quenching synthesizer for preparing insoluble sulfur is provided with a nitrogen chamber, an air pump, a pressurizing chamber, a stirring fan, a first spray nozzle and a second spray nozzle, wherein when a user quenches high-temperature sulfur, the air pump can extract nitrogen in the nitrogen chamber through an exhaust pipe and convey the nitrogen into the pressurizing chamber through a gas conveying pipe to protect and pressurize the high-temperature liquefied sulfur, so that the liquefied sulfur is atomized and sprayed out through the first spray nozzle, the second spray nozzle can spray out quenching liquid entering through a liquid inlet pipe, after the quenching liquid is sprayed out, a motor can drive the stirring fan to rotate through a rotating shaft to stir the quenching liquid and the high-temperature sulfur, so that the sulfur and the quenching liquid are in more sufficient contact, the temperature of the sulfur is uniformly cooled, the using amount of the quenching liquid is reduced, the waste of the quenching liquid is avoided, and a heater is also arranged, after the high-temperature sulfur is quenched, the user can start the heater, so that the metal resistor in the heater is electrified to generate heat to heat the sulfur and the quenching liquid, thereby promoting the evaporation of the quenching liquid and discharging the quenching liquid through the exhaust pipe, thereby reducing the preparation time of the sulfur and greatly improving the production efficiency of the sulfur.

Drawings

FIG. 1 is a schematic structural view of the present invention;

fig. 2 is an enlarged schematic view of a partial structure of the present invention a;

fig. 3 is a schematic view of a local structure of the motor of the present invention.

In the figure: 1. a synthesizer body; 2. a feed pipe; 3. a liquid inlet pipe; 4. a connecting member; 5. a processing chamber; 6. a discharge port; 7. an electronic valve; 8. a guide plate; 9. a motor; 10. a rotating shaft; 11. a stirring fan; 12. supporting legs; 13. a heater; 14. a nitrogen chamber; 15. an air inlet pipe; 16. an air exhaust pipe; 17. an air pump; 18. a gas delivery pipe; 19. a plenum chamber; 20. a first nozzle; 21. a second nozzle; 22. an exhaust pipe; 23. an activated carbon layer; 24. a torsion spring; 25. a movable plate.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

The utility model discloses in: the heater model is ZJ 20X-5.

Referring to fig. 1-3, the present invention provides a technical solution: a quenching synthesizer for preparing insoluble sulfur comprises a synthesizer body 1, a feeding pipe 2, a liquid inlet pipe 3, a connecting piece 4, a treatment chamber 5, a discharge port 6, an electronic valve 7, a guide plate 8, a motor 9, a rotating shaft 10, a stirring fan 11, supporting legs 12, a heater 13, a nitrogen chamber 14, an air inlet pipe 15, an air exhaust pipe 16, an air pump 17, an air pipe 18, a pressurizing chamber 19, a first spray nozzle 20, a second spray nozzle 21, an exhaust pipe 22, an activated carbon layer 23, a torsion spring 24 and a movable plate 25, wherein the feeding pipe 2 penetrates through the middle of the top of the synthesizer body 1, the movable plate 25 is connected to the inner wall of the feeding pipe 2 through the torsion spring 24, the torsion spring 24 is provided with two torsion springs 24, the two torsion springs 24 are made of manganese steel materials, the torsion spring 24 can conveniently open the movable plate 25 through contraction, the liquid inlet pipe 3 penetrates through the upper portion of, one end of the liquid inlet pipe 3 sequentially penetrates through one measuring part of the synthesizer body 1 and the treatment chamber 5 and extends into the treatment chamber 5, one end of the liquid inlet pipe 3 is connected with a second spray head 21, so that the second spray head 21 can atomize and spray quenching liquid entering through the liquid inlet pipe 3, two sides of the interior of the synthesizer body 1 are connected with the treatment chamber 5 through connecting pieces 4, a discharge hole 6 penetrates through the lower part of one side of the treatment chamber 5, the inner wall of the discharge hole 6 is connected with an electronic valve 7, a guide plate 8 is connected with the lower part of the interior of the treatment chamber 5, two sides of the interior of the treatment chamber 5 are connected with heaters 13, the two heaters 13 are welded on two sides of the interior of the treatment chamber 5, and the two heaters 13 are symmetrically arranged by taking the length center line of the treatment chamber 5 as the center, so that the heaters 13 can uniformly heat the sulfur and the quenching liquid in the treatment chamber 2, the inside below of synthesizer body 1 is connected with motor 9, the output of motor 9 is connected with stirring fan 11 through pivot 10, stirring fan 11 cup joints the one end surface of keeping away from motor 9 in pivot 10, just stirring fan 11 adopts stainless steel material to make and forms, avoids rusty corrosion because of the effect that receives water in stirring fan 11 long-time use, increases stirring fan 11's life, the bottom four corners of synthesizer body 1 all is connected with supporting legs 12, just the opposite side of synthesizer body 1 is connected with nitrogen chamber 14, one side of nitrogen chamber 14 runs through has intake pipe 15, and the top intermediate junction of nitrogen chamber 14 has air pump 17, the inlet end of air pump 17 is connected with exhaust tube 16, just the end of giving vent to anger of air pump 17 is connected with gas-supply pipe 18, the inside top of synthesizer body 1 is connected with pumping chamber 19, the bottom of plenum chamber 19 is connected with first shower nozzle 20, one side top of treatment chamber 5 is connected with blast pipe 22, the inside of blast pipe 22 is provided with a plurality of activated carbon layers 23, and is a plurality of activated carbon layers 23 equidistance distributes in the inside of blast pipe 22, and the activated carbon layer 23 of being convenient for adsorbs the purification to the gas that produces after the evaporation, avoids the direct discharge of poisonous and harmful gas.

The working principle is as follows: firstly, when a user uses the quenching synthesizer for preparing insoluble sulfur, the synthesizer body 1 is placed on the indoor horizontal ground through the supporting legs 12 and is connected with an external power supply, after the power supply is connected, the user can firstly fill nitrogen into the nitrogen chamber 14 through the air inlet pipe 15, then high-temperature sulfur is added through the inlet pipe 2, when the high-temperature sulfur enters the movable plate 25 through the inlet pipe 2, the torsion spring 24 can be compressed, so that the movable plate 25 is opened to enter the pressurizing chamber 19, the air pump 17 is started at the same time, the air pump 17 can pump the nitrogen in the nitrogen chamber 14 through the exhaust pipe 16 and convey the nitrogen to the pressurizing chamber 19 through the air conveying pipe 18, the high-temperature liquefied sulfur is protected and pressurized, so that the liquefied sulfur is atomized and sprayed out through the first spray nozzle 20, and the quenching liquid entering through the liquid inlet pipe 3 can be sprayed out through the second spray nozzle 21, after the quenching liquid is sprayed out, the motor 9 can drive the stirring fan 11 to rotate through the rotating shaft 10 to stir the quenching liquid and the high-temperature sulfur, after the sulfur is quenched, a user can start the heater 13 to electrify the metal resistor inside the heater 13 to generate heat to heat the sulfur and the quenching liquid, so that the evaporation of the quenching liquid is promoted, the quenching liquid is discharged through the exhaust pipe 22, when the gas is discharged, the gas can be adsorbed and filtered through the activated carbon layer, and finally, the user can open the electronic valve 7 to discharge the sulfur through the discharge hole 6.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. A quench synthesizer for the production of insoluble sulphur comprising a synthesizer body (1) characterized in that: a feed pipe (2) penetrates through the middle of the top of the synthesizer body (1), the inner wall of the feed pipe (2) is connected with a movable plate (25) through a torsion spring (24), a liquid inlet pipe (3) penetrates through the upper part of one side of the synthesizer body (1), and two sides inside the synthesizer body (1) are connected with a processing chamber (5) through a connecting piece (4), a discharge hole (6) penetrates through the lower part of one side of the treatment chamber (5), the inner wall of the discharge hole (6) is connected with an electronic valve (7), a guide plate (8) is connected with the lower part of the inner part of the treatment chamber (5), and both sides of the interior of the processing chamber (5) are connected with heaters (13), a motor (9) is connected to the lower part of the inner part of the synthesizer body (1), and the output end of the motor (9) is connected with a stirring fan (11) through a rotating shaft (10); supporting legs (12) are connected to four corners of the bottom of the synthesizer body (1), a nitrogen chamber (14) is connected to the other side of the synthesizer body (1), an air inlet pipe (15) penetrates through one side of the nitrogen chamber (14), an air pump (17) is connected to the middle of the top of the nitrogen chamber (14), an air inlet end of the air pump (17) is connected with an air exhaust pipe (16), and an air outlet end of the air pump (17) is connected with an air delivery pipe (18); the inside top of synthesizer body (1) is connected with pumping chamber (19), the bottom of pumping chamber (19) is connected with first shower nozzle (20), one side top of process chamber (5) is connected with blast pipe (22), the inside that feed liquor pipe (3) extended to process chamber (5) is provided with second shower nozzle (21), second shower nozzle (21) will be atomized and spout into process chamber (5) the inside through the quenching liquid that feed liquor pipe (3) got into.

2. The quench synthesizer of claim 1 for producing insoluble sulfur comprising: a plurality of activated carbon layers (23) are arranged in the exhaust pipe (22), and the activated carbon layers (23) are equidistantly distributed in the exhaust pipe (22).

3. The quench synthesizer of claim 1 for producing insoluble sulfur comprising: the two heaters (13) are welded on two sides of the interior of the processing chamber (5), and the two heaters (13) are symmetrically arranged by taking the length center line of the processing chamber (5) as the center.

4. The quench synthesizer of claim 1 for producing insoluble sulfur comprising: one end of the liquid inlet pipe (3) sequentially penetrates through the upper side of one side of the synthesizer body (1) and the processing chamber (5) and extends to the inside of the processing chamber (5), and one end of the liquid inlet pipe (3) is connected with a second spray head (21).

5. The quench synthesizer of claim 1 for producing insoluble sulfur comprising: the quenching liquid is a glycerol aqueous solution with the mass concentration of 15-30%.

6. The quench synthesizer of claim 1 for producing insoluble sulfur comprising: the stirring fan (11) is sleeved on the outer surface of one end, far away from the motor (9), of the rotating shaft (10), and the stirring fan (11) is made of stainless steel materials.

7. The quench synthesizer of claim 1 for producing insoluble sulfur comprising: the two torsion springs (24) are arranged, and the two torsion springs (24) are made of manganese steel materials.

Images