CN210543478U

CN210543478U - Macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel

Info

Publication number: CN210543478U
Application number: CN201921020666.8U
Authority: CN
Inventors: 李小康; 李伟; 李向荣
Original assignee: Gannan Normal University
Current assignee: Gannan Normal University
Priority date: 2019-07-03
Filing date: 2019-07-03
Publication date: 2020-05-19
Anticipated expiration: 2029-07-03

Abstract

The utility model relates to an extraction element especially relates to a draw macroporous resin adsorption extraction element of hesperidin from navel orange peel. The technical problem to be solved is as follows: the macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel does not need frequent replacement of a container for collecting liquid, so that liquid is prevented from being spilled after the container is knocked down, and macroporous resin is convenient to replace. The technical scheme is as follows: a macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel comprises a base, a support rod, a charging barrel and the like; a supporting rod is arranged on the left of the outer top of the base. The utility model discloses a cooperation between four-way pipe and the discharging pipe can realize the fixed to the jar body, and it is internal to discharge the jar through the cross-pass through in the different time quantum through steerable navel orange peel juice of valve, clear water and eluant to can adsorb, elute flavonoid.

Description

Macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel

Technical Field

The utility model relates to an extraction element especially relates to a draw macroporous resin adsorption extraction element of hesperidin from navel orange peel.

Background

The macroporous adsorption resin is a macromolecular adsorption resin which does not contain exchange groups and has a macroporous structure, has a good macroporous network structure and a larger specific surface area, can selectively adsorb organic matters in an aqueous solution through physics, is a novel organic polymer adsorbent developed in the 60 th century, and has been widely applied to the fields of environmental protection, food, medicine and the like.

The macroporous adsorption resin takes styrene and propionate as monomers, added styrene as a cross-linking agent, and toluene and xylene as pore-foaming agents, which are cross-linked and polymerized with each other to form a porous skeleton structure. The resin is generally white spherical particles with the granularity of 20-60 meshes, is a cross-linked polymer containing ion exchange groups, has stable physicochemical properties, is insoluble in acid, alkali and organic solvents, and is not influenced by inorganic salts and strong ion low-molecular compounds. The resin adsorption works by means of Van der Waals attraction between it and adsorbed molecules (adsorbates) and physical adsorption through its huge specific surface, so that organic compounds can be separated by elution with a certain solvent according to their adsorption force and molecular weight to achieve different purposes of separation, purification, impurity removal, concentration, etc.

At present, when navel orange flavonoid compounds are extracted from navel orange peels in a laboratory, the navel orange flavonoid compounds are extracted by methods such as ultrasonic wave, soxhlet extraction, macroporous resin adsorption and the like, and the process of extracting the navel orange flavonoid compounds by the macroporous resin is relatively quick; but also has the following disadvantages; the container for collecting the liquid needs to be frequently replaced, and the container is easy to be knocked down in the replacement process, so that the liquid can be spilled; the macroporous resin is not easy to replace.

Therefore, aiming at the existing problems, the device does not need to frequently replace a container for collecting liquid in the process of extracting the flavonoid compounds from the navel oranges by using the macroporous resin, thereby avoiding the liquid from spilling out after the container is knocked down and being convenient for replacing the macroporous resin.

SUMMERY OF THE UTILITY MODEL

In order to overcome the problem that a container for collecting liquid needs to be frequently replaced, the container is easy to be knocked down in the replacement process, so that the liquid is spilled, and the macroporous resin is difficult to replace. The technical problem to be solved is as follows: the macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel does not need frequent replacement of a container for collecting liquid, so that liquid is prevented from being spilled after the container is knocked down, and macroporous resin is convenient to replace.

The technical scheme is as follows: the utility model provides a draw macroporous resin adsorption extraction element of hesperidin from navel orange peel, which comprises a base, branch, charging barrel, the four-way pipe, the valve, the jar body, the slide bar, discharging pipe and first spring, branch is installed to base top left outside, the embedded three charging barrel of installing in branch upper portion, three charging barrel bottom is equipped with the four-way pipe, the four-way pipe communicates with three charging barrel, all be equipped with the valve on the four-way pipe of every charging barrel bottom, open at the base middle part has the slide opening, the slidingtype is equipped with the slide bar in the slide opening, the discharging pipe is installed on the slide bar top, be connected with first spring between discharging pipe bottom and the base, first spring is around on the slide bar, be equipped with the detachable jar body between discharging pipe and the four-way pipe bottom, the internal appropriate amount macroporous resin that is.

Further, including holding and putting the device, hold and put the device including square hole bearing, square pole and plectane, the embedded square hole bearing of installing in base middle part, square hole bearing in-connection has square pole, and the plectane is installed to square pole bottom, and the plectane is located the base lower part, and the even spaced standing groove that has the place container of placing in plectane upper portion.

Further, including square hole handle cover, second spring and L type kelly, the cover has square hole handle cover on the square pole, is connected with the second spring between square hole handle cover and the square pole top, and the even interval of square hole handle cover lower part circumference installs L type kelly, and the even interval division in top has the card hole with L type kelly complex outside the base.

Compared with the prior art, the utility model has the advantages of it is following: the utility model discloses a cooperation between four-way pipe and the discharging pipe can realize the fixed to the jar body, through the steerable navel orange peel juice of valve, it is internal that clear water and eluant cross the jar of discharging through the cross in the time quantum of difference, thereby can adsorb flavonoid, the elution, place a plurality of containers in the standing groove of plectane, thereby can not need frequent change container, and then can avoid bumping the spill of the container back liquid, cooperation through L type kelly and card hole, thereby can fix the disc, the container on the disc just can not remove, the container can not remove when liquid flows into the container.

Drawings

Fig. 1 is a schematic view of the structure of the present invention.

In the above drawings: 1: base, 2: strut, 3: charging barrel, 4: four-way pipe, 5: valve, 6: a tank body, 7: slide hole, 8: slide bar, 9: discharge pipe, 10: first spring, 11: opening, 12: holding device, 121: square bore bearing, 122: square pole, 123: circular plate, 124: standing groove, 13: square hole handle sleeve, 14: second spring, 15: l-shaped clip lever, 16: and (6) clamping the hole.

Detailed Description

Although the present invention may be described with respect to particular applications or industries, those skilled in the art will recognize the broader applicability of the invention. Those of ordinary skill in the art will recognize other factors such as: terms such as above, below, upward, downward, and the like are used to describe the accompanying drawings and are not meant to limit the scope of the invention as defined by the appended claims. Such as: any numerical designation of first or second, and the like, is merely exemplary, and is not intended to limit the scope of the invention in any way.

Example 1

A macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel comprises a base 1, a support rod 2, charging barrels 3, four-way pipes 4, valves 5, tank bodies 6, sliding rods 8, a discharge pipe 9 and a first spring 10, wherein the support rod 2 is installed on the left of the outer top of the base 1, the base 1 is connected with the support rod 2 in a welding connection mode, the three charging barrels 3 are installed on the upper portion of the support rod 2 in an embedded mode, the four-way pipes 4 are arranged at the bottoms of the three charging barrels 3 and communicated with the three charging barrels 3, the four-way pipes 4 at the bottom of each charging barrel 3 are respectively provided with the valves 5, the middle of the base 1 is provided with a sliding hole 7, the sliding rods 8 are arranged in the sliding holes 7 in a sliding mode, the discharge pipe 9 is installed at the top end of each sliding rod 8, the first spring 10 is connected between the bottom of the discharge pipe 9 and the base 1, the first spring 10 is wound on the, the tank body 6 is filled with a proper amount of macroporous resin, the left side of the base 1 is provided with an opening 11, and the lower part of the discharge pipe 9 is positioned in the opening 11.

The operation process of the device is as follows: an operator firstly squeezes navel orange peel, then an appropriate amount of inorganic salt is added into the navel orange peel juice, the resin adsorption capacity can be increased, the operator fills an appropriate amount of navel orange peel juice into a charging barrel 3 at the left side, an appropriate amount of clear water is filled into a charging barrel 3 at the middle side, an appropriate amount of eluant is filled into a charging barrel 3 at the right side, the operator places a container for collecting waste liquid below a discharging pipe 9, the operator opens a valve 5 at the left side again, the navel orange peel juice can flow into a tank body 6 through a four-way pipe 4, flavonoid compounds in the navel orange peel juice can be adsorbed through macroporous resin in the tank body 6, the choice of the dripping speed of the navel orange peel juice is that the macroporous resin can be well contacted and adsorbed with the navel orange peel juice fully, after the navel orange peel juice completely flows out, the operator closes the valve 5 at the left side, the operator opens the valve 5 at the middle side, clear water can flow into the tank body 6 through the four-way pipe 4, so that residues among the macroporous resins can be washed, after washing is completed, an operator closes the valve 5 in the middle, the operator takes away the container for collecting waste liquid, the operator places the container for collecting flavonoids compounds below the discharge pipe 9, the operator opens the valve 5 on the right, eluent can flow into the tank body 6 through the four-way pipe 4, so that the flavonoids compounds adsorbed in the macroporous resins can be eluted, the elution flow rate is generally controlled to be 0.5-5mL/min, after the flavonoids compounds adsorbed in the macroporous resins are eluted, the operator closes the valve 5 on the right, the operator can take out the container for collecting the flavonoids compounds, the operator can carry out the next operation, when the macroporous resins in the tank body 6 need to be replaced, the operator firstly holds the tank body 6, the discharging pipe 9 is moved downwards, the sliding rod 8 can move downwards along with the downward movement, the first spring 10 is compressed along with the downward movement, after the discharging pipe 9 is separated from the tank body 6, an operator moves the tank body 6 downwards to separate the tank body 6 from the four-way pipe 4, the operator can take out the tank body 6, the operator loosens the discharging pipe 9 again, under the action of the first spring 10, the discharging pipe 9 can reset, the operator can replace the macroporous resin in the tank body 6, after the macroporous resin is replaced, the operator moves the discharging pipe 9 downwards and then clamps the upper part of the tank body 6 into the four-way pipe 4, the operator aligns the upper part of the discharging pipe 9 with the lower part of the tank body 6 again, the operator loosens the discharging pipe 9 again, under the action of the first spring 10, the discharging pipe 9 can move upwards, the discharging pipe 9 can be clamped into the lower part of the tank body 6.

Example 2

A macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel comprises a base 1, a support rod 2, charging barrels 3, four-way pipes 4, valves 5, tank bodies 6, sliding rods 8, a discharge pipe 9 and a first spring 10, wherein the support rod 2 is installed on the left of the outer top of the base 1, the three charging barrels 3 are installed on the upper portion of the support rod 2 in an embedded mode, the four-way pipes 4 are arranged at the bottoms of the three charging barrels 3 and communicated with the three charging barrels 3, the valves 5 are arranged on the four-way pipes 4 at the bottom of each charging barrel 3, a sliding hole 7 is formed in the middle of the base 1, the sliding rods 8 are arranged in the sliding hole 7 in a sliding mode, the discharge pipe 9 is installed at the top end of each sliding rod 8, the first spring 10 is connected between the bottom of the discharge pipe 9 and the base 1, the first spring 10 is wound on the sliding rods 8, the detachable tank body 6 is arranged between the, an opening 11 is arranged at the left of the base 1, and the lower part of the discharge pipe 9 is positioned in the opening 11.

Still including holding and putting device 12, hold and put device 12 including square hole bearing 121, square pole 122 and plectane 123, base 1 middle part is embedded installs square hole bearing 121, square hole bearing 121 in-connection has square pole 122, circular pole 123 is installed to square pole 122 bottom, square pole 122 is connected with plectane 123 through bolted connection's mode, plectane 123 is located base 1 lower part, the even spaced opening in plectane 123 upper portion has the standing groove 124 of placing the container.

Still including square hole handle cover 13, second spring 14 and L type kelly 15, the cover has square hole handle cover 13 on the square pole 122, is connected with second spring 14 between square hole handle cover 13 and the square pole 122 top, and the even interval of square hole handle cover 13 lower part circumference installs L type kelly 15, and the even interval of base 1 outer top is opened have with L type kelly 15 complex card hole 16.

The operation process of the device is as follows: the operator can place the container in standing groove 124, and when needs changed the container, the operator can rotate plectane 123 to can drive the container rotation on the plectane 123, so need not frequent operation alright quick more change the container of unloading pipe below, so just saved the time, and be difficult for unrestrained the flourishing liquid in the container, after the operation was accomplished, the operator took out the container on plectane 123 can.

The operator upwards stimulates square hole handle cover 13, square hole handle cover 13 can drive L type kelly 15 and up move, second spring 14 is tensile along with it, and then can make L type kelly 15 break away from card hole 16, so, the operator alright drive plectane 123 and container rotation through square hole handle cover 13's rotation, thereby the container of removable discharging pipe 9 below, after the change finishes, the operator loosens square hole handle cover 13, under the effect of second spring 14, square hole handle cover 13 and L type kelly 15 move down, L type kelly 15 alright block in the card hole 16, thereby can fix the disc, the container on the disc just can not move, the container can not move when liquid flows into the container, can avoid liquid to spill.

The above description is only an example of the present invention, and is not intended to limit the present invention. All equivalent substitutions made within the principle of the present invention should be included within the protection scope of the present invention. Details of the present invention not described in detail belong to the prior art known to those skilled in the art.

Claims

1. A macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel comprises a base (1), a support rod (2), charging barrels (3) and four-way pipes (4), wherein the support rod (2) is installed on the left of the outer top of the base (1), three charging barrels (3) are installed on the upper portion of the support rod (2) in an embedded mode, the four-way pipes (4) are arranged at the bottoms of the three charging barrels (3), the four-way pipes (4) are communicated with the three charging barrels (3), the device is characterized by further comprising valves (5), a tank body (6), sliding rods (8), a discharging pipe (9) and a first spring (10), each four-way pipe (4) at the bottom of each charging barrel (3) is provided with a valve (5), the middle of the base (1) is provided with a sliding hole (7), each sliding rod (8) is arranged in each sliding hole (7), the top end of each sliding rod (8) is provided with a discharging pipe (9), and an elastic piece is, the elastic part is wound on the sliding rod (8), a detachable tank body (6) is arranged between the discharge pipe (9) and the bottom end of the four-way pipe (4), a proper amount of macroporous resin is arranged in the tank body (6), an opening (11) is formed in the left side of the base (1), and the lower part of the discharge pipe (9) is positioned in the opening (11).

2. The macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel according to claim 1, characterized by further comprising a bearing device (12), wherein the bearing device (12) comprises a square hole bearing (121), a square rod (122) and a circular plate (123), the square hole bearing (121) is installed in the middle of the base (1) in an embedded manner, the square hole bearing (121) is connected with the square rod (122) in the square hole bearing (121), the circular plate (123) is installed at the bottom end of the square rod (122), the circular plate (123) is located at the lower part of the base (1), and placing grooves (124) for placing containers are formed in the upper part of the circular plate (123) at uniform intervals.

3. The macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel according to claim 2, further comprising a square hole handle sleeve (13), a second spring (14) and an L-shaped clamp rod (15), wherein the square hole handle sleeve (13) is sleeved on the square rod (122), the second spring (14) is connected between the square hole handle sleeve (13) and the top end of the square rod (122), the L-shaped clamp rods (15) are installed on the lower portion of the square hole handle sleeve (13) at uniform intervals in the circumferential direction, and clamp holes (16) matched with the L-shaped clamp rods (15) are formed in the outer top of the base (1) at uniform intervals.

4. The macroporous resin adsorption extraction device for extracting hesperidin from navel orange peel as claimed in claim 3, wherein the elastic member is a spring.