CN210261145U - Nanometer flaky yttrium oxide powder preparation equipment - Google Patents
Nanometer flaky yttrium oxide powder preparation equipment Download PDFInfo
- Publication number
- CN210261145U CN210261145U CN201920909816.4U CN201920909816U CN210261145U CN 210261145 U CN210261145 U CN 210261145U CN 201920909816 U CN201920909816 U CN 201920909816U CN 210261145 U CN210261145 U CN 210261145U
- Authority
- CN
- China
- Prior art keywords
- yttrium oxide
- supporting
- top cover
- oxide powder
- supporting shaft
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 239000000843 powder Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 52
- 230000000149 penetrating effect Effects 0.000 claims abstract description 4
- 238000010438 heat treatment Methods 0.000 claims description 15
- 238000007599 discharging Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- WABPQHHGFIMREM-UHFFFAOYSA-N lead(0) Chemical compound [Pb] WABPQHHGFIMREM-UHFFFAOYSA-N 0.000 claims 2
- 239000000376 reactant Substances 0.000 abstract description 11
- 238000006243 chemical reaction Methods 0.000 description 11
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 9
- 235000006408 oxalic acid Nutrition 0.000 description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 description 1
- 238000003916 acid precipitation Methods 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Images
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
The utility model discloses a nanometer flaky yttrium oxide powder preparation device, which comprises a bottom plate, wherein two support columns are symmetrically arranged on the bottom plate, a fixing frame is arranged on the top surfaces of the two support columns, the fixing frame is horizontally arranged, a mounting seat is fixed at the end part of the fixing frame, and a driving hydraulic cylinder which is vertically and downwards arranged is arranged in the mounting seat; the bottom of the driving hydraulic cylinder is provided with a stirring device, the stirring device comprises a supporting shaft, the supporting shaft is coaxially connected to the bottom of the driving hydraulic cylinder, a top cover is connected to the supporting shaft in a penetrating manner, the edge of the top cover is connected with a plurality of L-shaped connecting arms, and the other ends of the connecting arms are fixedly connected with the top of the supporting shaft; and a second annular seat is arranged at the bottom of the supporting shaft. The utility model discloses can fully stir between the reactant that draws yttrium oxide, make and can fully fuse between it, let yttrium oxide draw more thoroughly.
Description
Technical Field
The utility model relates to an yttrium oxide draws equipment technical field, especially relates to a nanometer slice yttrium oxide powder preparation facilities.
Background
The yttrium oxide powder is an important high-technology ceramic raw material and is one of rare earth oxides which are applied to fluorescent powder; at present, the industrial production of superfine yttrium oxide is mainly an oxalic acid precipitation method, and the main process thereof is to add a surfactant into an oxalic acid solution, adjust the pH value by ammonia water, then add the adjusted yttrium chloride solution into the oxalic acid solution, rapidly stir, control the pH value of a reaction solution by the ammonia water, then filter, wash, dry and calcine to obtain yttrium oxide powder.
The reaction kettle is used as a physical and chemical reaction container, is important equipment in the production process of superfine yttrium oxide, has more types, and provides equipment for preparing nano flaky yttrium oxide powder in order to enable reactants in the reaction kettle to be more fully fused.
Disclosure of Invention
The utility model aims at solving the defects existing in the prior art and providing a nanometer flaky yttrium oxide powder preparation device.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
designing nano flaky yttrium oxide powder preparation equipment, which comprises a bottom plate, wherein two support columns are symmetrically arranged on the bottom plate, the top surfaces of the two support columns are provided with a fixed frame, the fixed frame is horizontally arranged, the end part of the fixed frame is fixedly provided with a mounting seat, and a driving hydraulic cylinder which is vertically arranged downwards is arranged in the mounting seat;
the bottom of the driving hydraulic cylinder is provided with a stirring device, the stirring device comprises a supporting shaft, the supporting shaft is coaxially connected to the bottom of the driving hydraulic cylinder, a top cover is connected to the supporting shaft in a penetrating manner, the edge of the top cover is connected with a plurality of L-shaped connecting arms, and the other ends of the connecting arms are fixedly connected with the top of the supporting shaft;
a second annular seat is installed at the bottom of the supporting shaft, a plurality of strip-shaped supporting plates which are arranged at equal intervals are connected to the edge of the side surface of the second annular seat, and heating pipes which are in a vertical state are installed at the other ends of the strip-shaped supporting plates;
a supporting pipe body is sleeved on the supporting shaft, the supporting pipe body is positioned above the second annular seat, the top surface of the supporting pipe body penetrates through the top cover and extends to the outer side, a motor is installed on the top cover, belt pulleys are coaxially installed on a rotating shaft of the motor and the top of the supporting pipe body, and the two belt pulleys are connected through a belt;
the bottom of the supporting pipe body is coaxially provided with a first annular seat, the side face of the first annular seat is connected with a plurality of first stirring blades, the first stirring blades are arranged along the side face of a second annular seat in a circumferential equidistant mode, the included angle between each first stirring blade and the top face of the second annular seat is A, A is more than or equal to 0 degrees and less than or equal to 45 degrees, the top face of the tail end of each first stirring blade is provided with a second stirring blade in a vertical state, the included angle between each second stirring blade and the side face of the second annular seat is B, B is more than or equal to 0 degrees and less than or equal to 45 degrees, and the first stirring blades and the second stirring blades are positioned in a space surrounded;
the lower part of the stirring device is provided with an inner barrel, the inner barrel is positioned inside the outer shell, at least three supporting legs are connected outside the outer shell, the supporting legs are installed on the bottom plate, wherein the bottom of the inner barrel is connected with a discharge channel, and the tail end of the discharge channel is connected with a guide pipe.
Preferably, the top cover is an arc-shaped cover, an annular ring extending outwards is arranged at the edge of the top cover, the annular ring corresponds to the top of the inner cylinder in position, and a rubber sealing ring is arranged between the annular ring and the top of the inner cylinder.
Preferably, the support shaft is connected with the support tube body through a sealed bearing.
Preferably, the conducting wire on the heating pipe penetrates out of the top cover, and the joint of the conducting wire and the top cover is sealed.
Preferably, a pressure relief valve is mounted on the top cover.
Preferably, a valve is installed in the discharge channel.
Preferably, an insulating layer is arranged between the outer shell and the inner barrel.
The utility model provides a nanometer slice yttrium oxide powder preparation equipment, beneficial effect lies in: when the device is used, the driving hydraulic cylinder is descended, so that the top cover covers the inner cylinder to seal, the heating pipe is started to perform reaction heating, and meanwhile, the motor is started to drive the stirring blades to rotate to stir reactants, so that the reaction is more thorough, and the heat of the reactants can be prevented from being excessively concentrated; the utility model discloses can fully stir between the reactant that draws yttrium oxide, make and can fully fuse between it, let yttrium oxide draw more thoroughly.
Drawings
The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention.
In the drawings:
fig. 1 is a schematic structural diagram of a nano flaky yttrium oxide powder preparation device provided by the utility model.
Fig. 2 is a schematic structural diagram of a stirring device of a nano flaky yttrium oxide powder preparation device provided by the utility model.
Labeled as in the figure: the device comprises a bottom plate 1, an outer shell 2, a heat preservation layer 3, an inner cylinder 4, a supporting pipe body 5, a motor 6, an annular ring 7, a top cover 8, a mounting seat 9, a driving hydraulic cylinder 10, a fixing frame 11, a connecting arm 12, a supporting column 13, a valve 14, a discharge channel 15, a guide pipe 16, a supporting leg 17, a supporting shaft 18, a second stirring blade 19, a first stirring blade 20, a heating pipe 21, a strip-shaped supporting plate 22, a first annular seat 23, a second annular seat 24, a belt disc 25 and a pressure release valve 26.
Detailed Description
To make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail below with reference to the following examples and drawings, and the exemplary embodiments and descriptions thereof of the present invention are only used for explaining the present invention, and are not intended as limitations of the present invention.
The structural features of the present invention will now be described in detail with reference to the accompanying drawings.
Referring to fig. 1-2, a nano flaky yttrium oxide powder preparation device comprises a bottom plate 1, wherein two support columns 13 are symmetrically arranged on the bottom plate 1, the top surfaces of the two support columns 13 are provided with a fixed frame 11, the fixed frame 11 is horizontally arranged, an installation seat 9 is fixed at the end part of the fixed frame 11, and a driving hydraulic cylinder 10 which is vertically arranged downwards is arranged in the installation seat 9;
a stirring device is arranged at the bottom of the driving hydraulic cylinder 10 and comprises a supporting shaft 18, the supporting shaft 18 is coaxially connected to the bottom of the driving hydraulic cylinder 10, a top cover 8 is connected to the supporting shaft 18 in a penetrating mode, a plurality of L-shaped connecting arms 12 are connected to the edge of the top cover 8, the other ends of the connecting arms 12 are fixedly connected with the top of the supporting shaft 18, the top cover 8 and the supporting shaft 18 are fixed together through the connecting arms 12, and when the driving hydraulic cylinder 10 stretches, the top cover 8 can be driven to move up and down;
a second annular seat 24 is installed at the bottom of the supporting shaft 18, a plurality of strip-shaped supporting plates 22 which are arranged at equal intervals are connected to the edge of the side surface of the second annular seat 24, heating pipes 21 which are in a vertical state are installed at the other ends of the strip-shaped supporting plates 22, the heating pipes 21 are used for heating, and the generated heat is used for heating the reaction;
the cover is equipped with support body 5 on back shaft 18, and support body 5 is located 24 tops of second annular seat to support body 5 top surface and run through top cap 8 and extend the outside, install motor 6 on the top cap 8, and in the pivot of motor 6 and the equal coaxial arrangement in top of support body 5 have belt pulley 25, connect through the belt between two belt pulleys 25, motor 6 can drive and support body 5 and rotate on back shaft 18
A first annular seat 23 is coaxially installed at the bottom of the supporting pipe body 5, a plurality of first stirring blades 20 are connected to the side surface of the first annular seat 23, the first stirring blades 20 are circumferentially arranged along the side surface of the second annular seat 24 at equal intervals, an included angle between each first stirring blade 20 and the top surface of the second annular seat 24 is A, A is not less than 0 degree and not more than 45 degree, a second stirring blade 19 in a vertical state is installed on the top surface of the tail end of each first stirring blade 20, an included angle between each second stirring blade 19 and the side surface of the second annular seat 24 is B, B is not less than 0 degree and not more than 45 degree, and the first stirring blades 20 and the second stirring blades 19 are both positioned in a space surrounded by the heating pipe 21; when the motor 6 drives the supporting pipe body 5 to rotate, the first stirring blade 20 and the second stirring blade 19 rotate along with the supporting pipe body, the first stirring blade 20 is horizontally arranged and can stir the reactant in the vertical direction, the second stirring blade 19 is enclosed into a cylinder, the direction of the stirred reactant is vertical to the stirring direction of the first stirring blade 20, so that the reactant is randomly rolled, and the reaction is more sufficient;
an inner barrel 4 is arranged below the stirring device, the inner barrel 4 is located inside the outer shell 2, at least three supporting legs 17 are connected to the outer side of the outer shell 2, the supporting legs 17 are installed on the bottom plate 1, wherein a discharging channel 15 is connected to the bottom of the inner barrel 4, and the tail end of the discharging channel 15 is connected with a guide pipe 16.
Specifically, the utility model discloses when using, let drive hydraulic cylinder 10 descend for 8 lids of top cap are on inner tube 4, seal, and draw yttrium oxide's reactant all put including in inner tube 4, open heating pipe 21 and be the reaction heating, it drives second stirring vane 19 to open motor 6 simultaneously, first stirring vane 20 rotates, stir the reactant, not only can let the reaction more thorough, can also prevent that the reactant heat is too concentrated, can draw the liquid of reaction completion to the preservation container through pipe 16 afterwards can.
Furthermore, the top cover 8 is an arc-shaped cover, an annular ring 7 extending outwards is arranged on the edge of the top cover 8, the annular ring 7 corresponds to the top of the inner cylinder 4, and a rubber sealing ring is arranged between the annular ring 7 and the top of the inner cylinder 4, so that the sealing performance between the annular ring 7 and the inner cylinder 4 is better.
Further, the supporting shaft 18 is connected with the supporting tube body 5 through a sealed bearing.
Further, the wires on the heating pipe 21 penetrate out of the top cover 8, and the connection position of the wires and the top cover 8 is sealed.
Further, a pressure release valve 26 is installed on the top cover 8 to prevent the air pressure in the inner cylinder 4 from being too high, and the pressure release valve 26 is used for adjusting the air pressure balance in the inner cylinder 4.
Further, a valve 14 is installed in the discharging passage 15.
Further, a heat insulation layer 3 is arranged between the outer shell 2 and the inner cylinder 4, and the heat insulation layer 3 is made of asbestos.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (7)
1. A nanometer flaky yttrium oxide powder preparation device comprises a bottom plate (1) and is characterized in that two support columns (13) are symmetrically arranged on the bottom plate (1), fixed frames (11) are arranged on the top surfaces of the two support columns (13), the fixed frames (11) are horizontally arranged, a mounting seat (9) is fixed at the end part of each fixed frame (11), and a driving hydraulic cylinder (10) which is vertically and downwards arranged is arranged in each mounting seat (9);
a stirring device is arranged at the bottom of the driving hydraulic cylinder (10), the stirring device comprises a supporting shaft (18), the supporting shaft (18) is coaxially connected to the bottom of the driving hydraulic cylinder (10), a top cover (8) is connected to the supporting shaft (18) in a penetrating manner, the edge of the top cover (8) is connected with a plurality of L-shaped connecting arms (12), and the other ends of the connecting arms (12) are fixedly connected with the top of the supporting shaft (18);
a second annular seat (24) is installed at the bottom of the supporting shaft (18), the edge of the side surface of the second annular seat (24) is connected with a plurality of strip-shaped supporting plates (22) which are arranged at equal intervals, and heating pipes (21) in a vertical state are installed at the other ends of the strip-shaped supporting plates (22);
the supporting pipe body (5) is sleeved on the supporting shaft (18), the supporting pipe body (5) is located above the second annular seat (24), the top surface of the supporting pipe body (5) penetrates through the top cover (8) and extends to the outer side, the motor (6) is installed on the top cover (8), belt discs (25) are coaxially installed on a rotating shaft of the motor (6) and the top of the supporting pipe body (5), and the two belt discs (25) are connected through a belt;
a first annular seat (23) is coaxially installed at the bottom of the supporting pipe body (5), a plurality of first stirring blades (20) are connected to the side face of the first annular seat (23), the first stirring blades (20) are circumferentially arranged along the side face of the second annular seat (24) at equal intervals, an included angle between each first stirring blade (20) and the top face of the second annular seat (24) is A, A is larger than or equal to 0 degrees and smaller than or equal to 45 degrees, a second stirring blade (19) in a vertical state is installed on the top face of the tail end of each first stirring blade (20), an included angle between each second stirring blade (19) and the side face of the second annular seat (24) is B, B is larger than or equal to 0 degrees and smaller than or equal to 45 degrees, and the first stirring blades (20) and the second stirring blades (19) are both located inside a space surrounded by the;
the lower part of the stirring device is provided with an inner barrel (4), the inner barrel (4) is located inside the outer shell (2), the outer side of the outer shell (2) is at least connected with three supporting legs (17), the supporting legs (17) are installed on the bottom plate (1), wherein the bottom of the inner barrel (4) is connected with a discharge channel (15), and the tail end of the discharge channel (15) is connected with a guide pipe (16).
2. The nano flaky yttrium oxide powder preparation equipment according to claim 1, wherein the top cover (8) is an arc-shaped cover, an annular ring (7) extending outwards is arranged on the edge of the top cover (8), the annular ring (7) corresponds to the top of the inner cylinder (4) in position, and a rubber sealing ring is arranged between the annular ring (7) and the top of the inner cylinder (4).
3. The apparatus for preparing nano flaky yttrium oxide powder according to claim 1, wherein the support shaft (18) is connected with the support tube body (5) through a sealed bearing.
4. The apparatus for preparing nano flaky yttrium oxide powder according to claim 1, wherein the lead wire on the heating tube (21) is penetrated out from the top cover (8), and the joint of the lead wire and the top cover (8) is sealed.
5. The apparatus for producing nano flaky yttrium oxide powder according to claim 1, wherein the top cap (8) is provided with a pressure relief valve (26).
6. The apparatus for producing nano flaky yttrium oxide powder according to claim 1, wherein a valve (14) is installed in the discharging passage (15).
7. The apparatus for preparing nano flaky yttrium oxide powder according to claim 1, wherein an insulating layer (3) is provided between the outer shell (2) and the inner cylinder (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920909816.4U CN210261145U (en) | 2019-06-18 | 2019-06-18 | Nanometer flaky yttrium oxide powder preparation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920909816.4U CN210261145U (en) | 2019-06-18 | 2019-06-18 | Nanometer flaky yttrium oxide powder preparation equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210261145U true CN210261145U (en) | 2020-04-07 |
Family
ID=70042984
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920909816.4U Expired - Fee Related CN210261145U (en) | 2019-06-18 | 2019-06-18 | Nanometer flaky yttrium oxide powder preparation equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210261145U (en) |
-
2019
- 2019-06-18 CN CN201920909816.4U patent/CN210261145U/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2015523195A (en) | Industrial microwave ultrasonic reactor | |
| CN210261145U (en) | Nanometer flaky yttrium oxide powder preparation equipment | |
| CN210357169U (en) | Chemical industry is with reation kettle that can improve reaction liquid reaction quality | |
| CN107930536A (en) | A kind of polyester resin polymerization reaction kettle | |
| CN115992038A (en) | Fermenting device for producing antibiotic-reducing feed active peptide and using method | |
| CN213467522U (en) | A raw material processing equipment for heparin sodium production preparation | |
| CN113717644B (en) | Preparation method and device of drier special for automatic dish-washing machine | |
| CN212915678U (en) | Reation kettle is used in preparation of PVC cross-linking agent | |
| CN211864622U (en) | Organic silicon resin colloid production facility | |
| CN214552736U (en) | Copper door coating preparation facilities | |
| CN205055860U (en) | Horizontal dissolving machine | |
| CN210906179U (en) | Enamel reaction kettle for producing water reducing agent | |
| CN209076679U (en) | A kind of allodihydrotestosterone production highly effective reaction kettle | |
| CN206510242U (en) | Centrifugal kneader body assembly | |
| CN204320299U (en) | Grease pressure still | |
| CN213231544U (en) | Nanometer flaky yttrium oxide powder preparation equipment | |
| CN111661852A (en) | Preparation device and process of zirconium silicate powder | |
| CN207307735U (en) | A kind of water-based industrial paint high speed dispersion tank | |
| CN205903894U (en) | Zinc stearate reactor | |
| CN206730591U (en) | Deaeration kettle is used in a kind of epoxy pouring sealant production | |
| CN111879122A (en) | Horizontal type ventilating stirring pressure roasting furnace | |
| CN205856978U (en) | A kind of asphalt modification integrated reactor | |
| CN215540905U (en) | Multistage stirring reation kettle | |
| CN106422942B (en) | Modified starch sill mixing equipment | |
| CN220460659U (en) | Reaction kettle for processing calcium molybdate |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200407 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |