CN210205954U - Novel continuous extraction and concentration device - Google Patents

Novel continuous extraction and concentration device Download PDF

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Publication number
CN210205954U
CN210205954U CN201920358433.2U CN201920358433U CN210205954U CN 210205954 U CN210205954 U CN 210205954U CN 201920358433 U CN201920358433 U CN 201920358433U CN 210205954 U CN210205954 U CN 210205954U
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concentration
extraction
outlet
feeding
inlet
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Yanling Pei
裴艳玲
Jianlei Guo
郭建磊
Jian Yang
杨健
Haipeng Yan
闫海朋
Haiqin Mo
墨海芹
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Hebei Xinminhe Pharmaceutical Technology Development Co Ltd
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Hebei Xinminhe Pharmaceutical Technology Development Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

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Abstract

The utility model discloses a novel draw enrichment in succession device, include solvent condensation storage chamber, vacuum solenoid valve, draw concentrated chamber, draw cup conveyer, on-line measuring system, refrigeration heat recovery system, touch-sensitive screen all-in-one, vacuum system, draw cup, extract storage jar and control system. The utility model discloses can realize traditional chinese medicine draw in succession, concentration and automatic quality detection, improve production efficiency, help realizing traditional chinese medicine automatic extraction, concentrated industrialization.

Description

Novel continuous extraction and concentration device
Technical Field
The utility model relates to a traditional chinese medicine draws concentrator field, concretely relates to novel draw concentration in succession device.
Background
China is the origin of traditional Chinese medicine, which has a long history in China and is a treasure of Chinese nationality. With the deepening of the understanding of people on traditional Chinese medicines and the recognization of western medicines, the thought of people slowly tends to return to nature. The traditional Chinese medicine is prepared from natural medicines, and the extraction and concentration technology of the traditional Chinese medicine is a very important process in the preparation process of the traditional Chinese medicine.
The extraction and concentration are important processes of the traditional Chinese medicine preparation process, and the quality of the medicine is directly influenced. The improvement of extraction and concentration technology and the improvement of equipment are key fields of transformation and upgrading of the traditional Chinese medicine manufacturing industry, and relate to the process of modernization and internationalization of the traditional Chinese medicine extraction and concentration technology.
The traditional Chinese medicine has various specificities, such as regionality of raw materials, complexity of component composition and the like, and the traditional Chinese medicine is laggard in domestic production process, low in production efficiency and lack of scientific and rigorous process parameters and clear quantitative indexes, so that the production quality of traditional Chinese medicine products is unstable, and the automation degree is not high.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a novel continuous traditional chinese medicine draws enrichment facility, can realize traditional chinese medicine draw in succession, concentration and automatic quality testing, improve production efficiency, help realizing traditional chinese medicine automatic extraction, concentrated industrialization.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
a novel continuous extraction and concentration device comprises a solvent condensation storage cavity, a vacuum electromagnetic valve, an extraction and concentration cavity, an extraction cup conveyor, an online detection system, a refrigeration and heat recovery system, a touch screen integrated machine, a vacuum system, an extraction cup, an extract storage tank and a control system; an extraction solvent outlet of the solvent condensation storage cavity is communicated with a solvent inlet of the vacuum electromagnetic valve; a solvent outlet of the vacuum electromagnetic valve is connected with a solvent inlet of the extraction concentration cavity; an extract outlet of the extraction concentration cavity is communicated with an extract inlet of the online detection system; an extract outlet of the online detection system is respectively communicated with an extract inlet of the extract storage tank and an extract reflux port of the extraction concentration cavity; a condensed water outlet and a condensed water return port of the refrigeration heat recovery system are respectively communicated with a condensed water inlet and a condensed water outlet of the solvent condensation storage cavity; the heating water outlet and the heating water return port of the refrigeration heat recovery system are respectively communicated with the heating water inlet and the heating water outlet of the extraction concentration cavity; an extraction cup inlet and an extraction cup outlet of the extraction cup conveyor respectively correspond to an extraction cup outlet and an extraction cup inlet of the extraction concentration cavity; the vacuum system is connected with the solvent condensation storage cavity; the control system is respectively in control connection with the solvent condensation storage cavity, the vacuum solenoid valve, the extraction concentration cavity, the extraction cup conveyor, the online detection system, the refrigeration heat recovery system, the vacuum system and the touch screen all-in-one machine.
Furthermore, the solvent condensation storage cavity comprises a solvent condensation storage cavity shell, a vortex condensation coil pipe, a condensed water inlet, a condensed water outlet, a solvent filling port, a vacuum port, an extraction solvent outlet and a vacuum pipeline; the condensed water inlet and the condensed water outlet are respectively communicated with the vortex condensing coil; the solvent filling port, the vacuum port, the extraction solvent outlet and the vacuum pipeline are respectively communicated with the solvent condensation storage cavity shell, and the vacuum port is communicated with the vacuum system; the vacuum pipeline is also communicated with the extraction concentration cavity.
Furthermore, the extraction concentration cavity comprises an extraction concentration cavity shell, an extraction motor, an extraction disc transmission part, an extraction disc, a feeding and discharging part, a feeding and discharging transmission part, a concentration motor, a concentration actuator transmission part, a concentration actuator, a speed measurement part, an extraction concentration cavity vacuum port, a solvent inlet, an extract outlet, an extract reflux port, a heating water inlet, a heating water outlet, a position sensor, a liquid level sensor, a vacuum pressure gauge and an ultrasonic generation system; the extraction motor, the concentration motor, the speed measurement part, the position sensor, the liquid level sensor, the vacuum pressure gauge and the ultrasonic generation system are all electrically connected to the control system; the extracting and concentrating cavity shell is provided with an extracting cup inlet and an extracting cup outlet which respectively correspond to the extracting cup outlet and the extracting cup inlet of the extracting cup conveyor; the concentration actuator is positioned in a concentration area of the extraction and concentration cavity shell, and the extraction disc is arranged in the extraction and concentration cavity shell and corresponds to the position of the concentration area;
the extracting motor is in transmission connection with the extracting disc through an extracting disc transmission part, the feeding and discharging transmission part is in transmission connection with the extracting disc transmission part, and the feeding and discharging transmission part is in transmission connection with the feeding and discharging part; the concentration motor is in transmission connection with the concentration actuator through a concentration actuator transmission part, and the speed measurement part is connected with the concentration actuator transmission part; the extraction concentration cavity vacuum port, the solvent inlet, the extract outlet, the extract reflux port, the heating water inlet, the heating water outlet and the vacuum pressure gauge are all communicated with the extraction concentration cavity shell, and the extraction concentration cavity vacuum port is also communicated with the solvent condensation storage cavity; the positions of the solvent inlet, the position sensor and the liquid level sensor respectively correspond to the positions of the extraction stations of the extraction disc; the ultrasonic generating system is connected with the extraction and concentration cavity shell;
the feeding and discharging part comprises at least two feeding and discharging wheels, each feeding and discharging wheel is provided with a receiving cavity, and an extraction cup feeding part is arranged in each receiving cavity; the receiving cavity of one of the material inlet and outlet wheels can correspond to an extraction cup inlet of the extraction concentration cavity shell and an extraction station of the extraction disc through rotation, and the receiving cavity of the other material inlet and outlet wheel can correspond to an extraction cup outlet of the extraction concentration cavity shell and an extraction station of the extraction disc through rotation; each feeding and discharging wheel is in transmission connection with the feeding and discharging transmission part; and the extraction station of the extraction disc is correspondingly provided with an extraction cup push-out component.
Furthermore, the extracting disc transmission part comprises an extracting disc large belt wheel, an extracting disc small belt wheel, an extracting disc synchronous belt and an extracting disc transmission shaft; the large extracting disc belt wheel is coaxially fixed on the extracting disc transmission shaft, the small extracting disc belt wheel is coaxially fixed on an output shaft of the extracting motor, and the extracting disc synchronous belt is respectively wound on the small extracting disc belt wheel and the large extracting disc belt wheel in a transmission manner; the extracting disc transmission shaft and the extracting disc are coaxially fixed.
Furthermore, the feeding and discharging transmission part comprises a large feeding and discharging belt wheel, a synchronous feeding and discharging belt, a small feeding and discharging belt wheel, a small feeding and discharging auxiliary belt wheel, a feeding and discharging transmission shaft and a feeding and discharging auxiliary transmission shaft; the feeding and discharging large belt wheel is connected with the extraction disc transmission part in a transmission way, the feeding and discharging small belt wheel is coaxially fixed on the feeding and discharging transmission shaft, the feeding and discharging auxiliary small belt wheel is coaxially fixed on the feeding and discharging auxiliary transmission shaft, and the feeding and discharging synchronous belt is respectively wound on the feeding and discharging large belt wheel, the feeding and discharging small belt wheel and the feeding and discharging auxiliary small belt wheel in a transmission way; one of the material inlet and outlet wheels is coaxially fixed on the material inlet and outlet transmission shaft, and the other material inlet and outlet wheel is coaxially fixed on the material inlet and outlet auxiliary transmission shaft.
Furthermore, the concentration actuator comprises a concentration fixed block, a membrane pulling plate, a membrane scraping plate and a concentration baffle plate; the concentration fixed block is positioned at the central position, the plurality of membrane scraping plates are arranged around the concentration fixed block in a vortex shape, and one end of each membrane scraping plate is fixed on the concentration fixed block; at least one film drawing plate is arranged between every two film scraping plates, and two ends of the film drawing plate are respectively connected with the two film scraping plates; concentrated baffle fixed connection is in the top of drawing the membrane board and scraping the membrane board, concentrated fixed block transmission connect in concentrated executor drive disk assembly.
Furthermore, the transmission part of the concentration actuator comprises a coupler, a concentration link rod, a concentration belt wheel retainer ring, a concentration transmission shaft, a concentration large belt wheel retainer ring and a concentration synchronous belt; the shaft coupling is coaxially fixed to an output shaft of the concentration motor and the concentration link rod respectively, and the concentration link rod is coaxially fixed to the concentration belt pulley; the concentration large belt wheel is coaxially fixed on the concentration transmission shaft, and the concentration synchronous belt is respectively wound on the concentration large belt wheel and the concentration small belt wheel in a transmission manner; the concentration belt pulley retaining ring and the concentration large belt pulley retaining ring are respectively sleeved on the outer edges of the concentration belt pulley and the concentration large belt pulley; the concentration transmission shaft is in transmission connection with the concentration actuator.
Further, the extraction cup conveyor comprises a bottom plate, a shell frame body, a motor support, a driving speed reduction motor, a driving small belt wheel, a driving large belt wheel, a driving synchronous belt, a driving roller, a driven roller, a carrier roller, a lining plate, a conveying belt guide wheel, a baffle plate and a tensioning device, wherein the driving speed reduction motor is electrically connected to the control system; the driving small belt pulley is coaxially connected with an output shaft of the driving speed reduction motor, the driving synchronous belt is in transmission connection with the driving small belt pulley and the driving large belt pulley, the driving large belt pulley is coaxially connected with the driving roller, the carrier roller is arranged below the conveying belt, the lining plate is arranged above the carrier roller, the driven roller is connected with the tensioning device, the conveying belt is in transmission connection with the driving roller and the driven roller, the conveying belt surface is provided with the conveying belt guide wheel through a hole, and the conveying belt guide wheel and the baffle are installed in a sliding manner; the shell frame body, the motor support and the baffle are fixedly connected to the bottom plate, and the driving speed reduction motor is fixed to the motor support.
Furthermore, the online detection system comprises a peristaltic pump, a refractometer and an electric three-way reversing valve, and the peristaltic pump, the refractometer and the electric three-way reversing valve are all electrically connected to the control system; an input port of the peristaltic pump is communicated with an extract outlet of the extraction concentration cavity, an output port of the peristaltic pump is communicated with an input port of the refractometer, and an output port of the refractometer is communicated with an extract inlet of the electric three-way reversing valve; and the unqualified extract outlet of the electric three-way reversing valve is communicated with the extract reflux port of the extraction concentration cavity, and the qualified extract outlet is communicated with the extract storage tank.
Further, the refrigeration heat recovery system comprises a refrigerant compressor, a plate heat exchanger, a condenser, a throttling device, an evaporator, a gas-liquid separator, a cold water tank, a hot water tank and a circulating water pump; the cold and hot water tank comprises a heating water tank, a heating mechanism, a heating water outlet, a heating water return port, a condensed water tank, a condensed water outlet, a condensed water return port, a hot water circulation outlet, a hot water circulation inlet, a condensed water circulation outlet, a condensed water circulation inlet, a temperature sensor, a liquid level sensor, a heat preservation layer and a cold and hot water tank cover; the refrigerant compressor, the circulating water pump, the temperature sensor, the liquid level sensor and the heating mechanism are all electrically connected to the control system;
the heating mechanism is connected to the heating water tank; the heating water tank and the condensed water tank are arranged in a cold and hot water tank housing, a heat-insulating layer is filled in the cold and hot water tank housing, the heating water outlet, the heating water return port, the hot water circulation inlet and the hot water circulation outlet are respectively communicated with the heating water tank, and the condensed water outlet, the condensed water return port, the condensed water circulation outlet and the condensed water circulation inlet are respectively communicated with the condensed water tank; the heating water tank and the condensed water tank are respectively connected with a temperature sensor and a liquid level sensor;
the refrigerant compressor, the plate heat exchanger, the condenser, the throttling device, the evaporator and the gas-liquid separator are sequentially communicated, and the gas-liquid separator is communicated with the refrigerant compressor; an inlet of the circulating water pump is respectively communicated with the hot water circulating outlet and the condensed water circulating outlet, and outlets of the circulating water pump are respectively communicated with a circulating inlet of the plate heat exchanger and a circulating inlet of the evaporator; and a circulating outlet of the plate heat exchanger is communicated with the hot water circulating inlet, and a circulating outlet of the evaporator is communicated with the condensed water circulating inlet.
The beneficial effects of the utility model reside in that:
1) the online detection system is adopted to perform real-time quality monitoring on the production process of the extract, the online detection system is combined with the control system to continuously compensate the operating parameters to obtain the ideal extract, continuous extraction and real-time monitoring can be realized, manual sampling detection is not needed, and extraction interruption is avoided.
2) The automatic control and monitoring of the extraction and concentration of the traditional Chinese medicine can be realized, and the control, the real-time monitoring of technical parameters such as production environment, pressure and the like in the traditional Chinese medicine production process can be accurately combined with the real-time adjustment of a database;
3) the production, extraction and concentration are carried out in a vacuum environment, so that the production efficiency of extraction and concentration can be effectively improved, and the damage of continuous high temperature to the medicine is reduced;
4) the materials are automatically transported and extracted, so that the manual operation is fully reduced, the manual operation influence in human, machine, material, method and ring is reduced, and the human only plays a role in supervision;
5) a closed-loop operation mode can be formed, and the influence of external adverse factors on the medicine is reduced;
6) the innovative vortex concentration scraper realizes the process flows of rapid film drawing, evaporation and film collection through the film drawing plate and the film scraping plate, so that the production is more stable and the efficiency is improved;
7) qualified extract is obtained from the raw materials of the traditional Chinese medicine, and the continuous extraction and concentration of the traditional Chinese medicine are realized by a complete streamlined operation mode, so that the efficiency is improved;
8) the unique refrigeration heat recovery system fully utilizes resources and realizes energy conservation and environmental protection;
9) ultrasonic wave generation system draws the production broken wall phenomenon to the medicinal material, raises the efficiency.
Drawings
Fig. 1 is a schematic diagram of the overall structural distribution of an embodiment of the present invention;
FIG. 2 is a schematic view of the general structure of a solvent condensation storage chamber in an embodiment of the present invention;
FIG. 3 is a schematic diagram of the overall structure of the extraction concentration chamber in the embodiment of the present invention;
FIG. 4 is a schematic structural view of an extraction cup according to an embodiment of the present invention;
fig. 5 is a schematic structural view of a transmission part of the extracting tray in the embodiment of the present invention;
FIG. 6 is a schematic structural view of a feeding and discharging transmission part in an embodiment of the present invention;
fig. 7 is a schematic structural view of a feeding and discharging component in an embodiment of the present invention;
fig. 8 is a schematic structural diagram of a concentration actuator according to an embodiment of the present invention;
FIG. 9 is a schematic cross-sectional view of the ejection member of the extraction cup in the casing of the extraction concentration chamber according to the embodiment of the present invention;
fig. 10 is a schematic structural diagram of a transmission part of a concentration actuator according to an embodiment of the present invention;
fig. 11 is a schematic structural diagram of a speed measuring component in an embodiment of the present invention;
fig. 12 is a schematic cross-sectional view of an embodiment of the present invention showing an extraction pan and a concentration actuator within an extraction and concentration chamber housing;
fig. 13 is a schematic structural view of an extracting tray in an embodiment of the present invention;
fig. 14 is a schematic view of the general structure of an extraction cup conveyor according to an embodiment of the present invention;
FIG. 15 is a schematic diagram of an online detection system according to an embodiment of the present invention;
fig. 16 is a schematic view of the overall structure of the refrigeration heat recovery system according to the embodiment of the present invention;
FIG. 17 is a schematic view of a structure of one side of a hot and cold water tank according to an embodiment of the present invention;
fig. 18 is a schematic structural view of another side of the cold and hot water tank according to the embodiment of the present invention;
fig. 19 is a schematic diagram of a refrigeration heat recovery system according to an embodiment of the present invention;
fig. 20 is a schematic diagram of the vacuum system according to an embodiment of the present invention;
fig. 21 is a schematic structural diagram of the touch screen all-in-one machine according to the embodiment of the present invention;
fig. 22 is a schematic view of the overall state of the embodiment of the present invention.
Detailed Description
The present invention will be further described with reference to the accompanying drawings, and it should be noted that the present embodiment is based on the technical solution, and the detailed embodiments and the specific operation processes are provided, but the protection scope of the present invention is not limited to the present embodiment.
As shown in fig. 1-22, a novel continuous extraction and concentration device comprises a solvent condensation storage cavity 1, a vacuum solenoid valve 2, an extraction and concentration cavity 3, an extraction cup conveyor 4, an online detection system 5, a refrigeration and heat recovery system 6, a touch screen integrated machine 7, a vacuum system 8, an extraction cup 12, an extract storage tank 13 and a control system; an extraction solvent outlet 17 of the solvent condensation storage cavity 1 is communicated with a solvent inlet of the vacuum solenoid valve 2; the solvent outlet of the vacuum solenoid valve 2 is connected with the solvent inlet 312 of the extraction concentration cavity 3; an extract outlet 313 of the extraction concentration cavity is communicated with an extract inlet of the online detection system 5; an extract outlet of the online detection system 5 is respectively communicated with an extract inlet of the extract storage tank 13 and an extract reflux port 314 of the extraction concentration cavity 3; a condensed water outlet 676 and a condensed water return port 677 of the refrigeration heat recovery system 6 are respectively communicated with a condensed water inlet 14 and a condensed water outlet 15 of the solvent condensation storage cavity 1; the heating water outlet 673 and the heating water return port 674 of the refrigeration heat recovery system 6 are respectively communicated with the heating water inlet 315 and the heating water outlet 316 of the extraction concentration chamber 3; an extraction cup inlet and an extraction cup outlet of the extraction cup conveyor 4 respectively correspond to an extraction cup outlet and an extraction cup inlet of the extraction concentration cavity; the vacuum system 8 is connected to the solvent condensation storage cavity 1; the control system is respectively in control connection with the solvent condensation storage cavity, the vacuum solenoid valve, the extraction concentration cavity, the extraction cup conveyor, the online detection system, the refrigeration heat recovery system, the vacuum system and the touch screen all-in-one machine.
In this embodiment, novel continuous traditional chinese medicine draws enrichment facility still includes the frame, the frame includes whole skeleton 101 and locates skeleton backup pad 9 and skeleton bottom plate 10 of its top and bottom respectively, and novel continuous traditional chinese medicine draws all constitutions of enrichment facility and all installs in the frame. An integral enclosure 100 is also included, with the exception of the extraction cup conveyor and touch screen integration, all components being located within the integral enclosure, forming a substantially sealed operating environment, as shown in fig. 22.
Further, as shown in fig. 2, the solvent condensation storage cavity 1 comprises a solvent condensation storage cavity shell 11, a vortex condensation coil 111, a condensed water inlet 14, a condensed water outlet 15, a solvent filling port 110, a vacuum port 16, an extraction solvent outlet 17 and a vacuum pipeline 18; the condensed water inlet 14 and the condensed water outlet 15 are respectively communicated with the vortex condensing coil 111; the solvent filling port 110, the vacuum port 16, the extraction solvent outlet 17 and the vacuum pipeline 18 are respectively communicated with the solvent condensation storage cavity shell 11, and the vacuum port 16 is communicated with the vacuum system 8; the vacuum line 18 is also in communication with the extraction and concentration chamber 3.
Further, a layer of polyurethane heat-insulating material can be arranged inside the solvent condensation storage cavity shell 11, so that the heat-insulating performance is improved.
In the solvent condensation storage cavity 1, adding a certain amount of extraction solvent into the solvent condensation storage cavity 11 through the solvent filling port 110 for the first time; the extraction solvent outlet 17 delivers the extraction solvent to the solvent inlet of the vacuum solenoid valve 2, and the vacuum solenoid valve 2 delivers the extraction solvent to the solvent inlet 312 of the extraction concentration chamber 3 through the solvent outlet under the control of the control system. Under the control of the control system, the vacuum system realizes the vacuum pumping of the interior of the solvent condensation storage cavity 1 and the interior of the extraction concentration cavity 3 through the vacuum ports, so that the solvent condensation storage cavity and the extraction concentration cavity work under the set vacuum degree. The vacuum pipeline 18 is in through connection with the solvent condensation storage cavity 1 and the extraction concentration cavity 3, the extraction solvent gas evaporated in the extraction concentration cavity 3 returns to the solvent condensation storage cavity 11 through the vacuum pipeline 18, exchanges heat with the vortex condensation coil 111, is converted into a liquid extraction solvent again, and can flow back to the extraction concentration cavity 3 again through the vacuum solenoid valve for recycling. The condensed water is conveyed from a condensed water outlet 676 of the refrigeration heat recovery system 6 to a condensed water inlet 14 of the solvent condensation storage cavity 1, flows into the vortex condensing coil 111, and circulates in a counter-current manner from bottom to top to a condensed water outlet 15 of the solvent condensation storage cavity 1, so that heat exchange with the extracted solvent gas is realized in the solvent condensation storage cavity shell 11.
In this embodiment, the solvent condensation storage chamber 1 further includes a condensation support frame 19 respectively connected to the solvent storage chamber shell 11 and the extraction concentration chamber shell 31, and the vacuum pipeline 18 is located in the condensation support frame 19.
Specifically, the condensation support frame 19 is fixedly connected with the bottom surface of the solvent condensation storage cavity 1 and the top surface of the extraction concentration cavity 3, the position of the solvent condensation storage cavity 1 is higher than that of the extraction concentration cavity 3, and the extraction solvent is conveyed to a solvent inlet of the vacuum electromagnetic valve (normally closed) 2 in a self-flowing mode.
In the present embodiment, as shown in fig. 3, the extraction concentration chamber 3 includes an extraction concentration chamber housing 31, an extraction motor 32, an extraction disc transmission part 34, an extraction disc 33, a feeding and discharging part 35, a feeding and discharging transmission part 36, a concentration motor 37, a concentration actuator transmission part 38, a concentration actuator 39, a speed measurement part 310, an extraction concentration chamber vacuum port 311, a solvent inlet 312, an extract outlet 313, an extract return port 314, a heated water inlet 315, a heated water outlet 316, a position sensor 317, a liquid level sensor 318, a vacuum pressure gauge 319, and an ultrasonic wave generation system 320; the extraction motor 32, the concentration motor 37, the speed measurement part 310, the position sensor 317, the liquid level sensor 318, the vacuum pressure gauge 319 and the ultrasonic wave generation system 320 are all electrically connected to the control system; the extracting and concentrating cavity shell 31 is provided with an extracting cup inlet and an extracting cup outlet which respectively correspond to the extracting cup outlet and the extracting cup inlet of the extracting cup conveyor 4; as shown in fig. 12, the concentration actuator 39 is located in the concentration area of the extraction and concentration chamber housing 31, and the extraction disc 33 is located in the extraction and concentration chamber housing 31 and corresponds to the position of the concentration area;
the extracting motor 32 is in transmission connection with the extracting disc 33 through an extracting disc transmission part 34, the feeding and discharging transmission part 36 is in transmission connection with the extracting disc transmission part 34, and the feeding and discharging transmission part 36 is in transmission connection with the feeding and discharging part 35; the concentration motor 37 is in transmission connection with the concentration actuator 39 through a concentration actuator transmission part 38, and the speed measurement part 310 is connected with the concentration actuator transmission part 38; the extraction concentration cavity vacuum port 311, the solvent inlet 312, the extract outlet 313, the extract reflux port 314, the heated water inlet 315, the heated water outlet 316 and the vacuum pressure gauge 319 are all communicated with the extraction concentration cavity shell 31, and the extraction concentration cavity vacuum port 311 is also communicated with the solvent condensation storage cavity 1 (specifically communicated with the vacuum pipeline 18 in this embodiment); the positions of the solvent inlet 312, the position sensor 317 and the liquid level sensor 318 correspond to the positions of the extraction stations of the extraction tray 33 respectively; the ultrasonic wave generation system 320 is connected to the extraction and concentration cavity shell 31;
the feeding and discharging part comprises at least two feeding and discharging wheels 351, as shown in fig. 7, each feeding and discharging wheel 351 is provided with a receiving cavity 354, and an extracting cup feeding part is arranged in each receiving cavity 354; the extraction cup sending part comprises a boosting rod 352 and a compression spring 353, and the boosting rod 352 is slidably connected with a receiving cavity 354 of the material inlet and outlet wheel 351 through the compression spring 353; one of the receiving cavities 354 of the in-out wheel 351 can correspond to the inlet of the extracting cup of the rotating and extracting concentrating chamber shell 31 and the extracting station of the extracting tray 33, and the other receiving cavity 354 of the in-out wheel 351 can correspond to the outlet of the extracting cup of the rotating and extracting concentrating chamber shell 31 and the extracting station of the extracting tray 33; each material inlet and outlet wheel 351 is in transmission connection with the material inlet and outlet transmission part 36;
as shown in fig. 9, an extracting station of the extracting tray is correspondingly provided with an extracting cup pushing-out member 321, the extracting cup pushing-out member 321 includes a pushing-out rod fixing block 3211 and an extracting cup pushing-out rod 3212, the extracting cup pushing-out rod 3212 is connected to the pushing-out rod fixing block 3211 through an elastic member (a compression spring may also be used), the pushing-out rod fixing block 3211 is disposed on the extracting tray, and the pushing-out rod fixing block 3211 is disposed above the extracting tray 33 and is fixedly connected to the inner wall of the extracting and concentrating chamber housing 31; the extraction cup push rod 3212 corresponds to the receiving cavity 354 of the in-out wheel 351.
Before the extraction and concentration work, crushing and pressing the traditional Chinese medicine materials into blocks, putting the blocks into an extraction cup, and putting the extraction cup on an extraction cup conveyor for preparing the materials. Carry out and draw concentrated during operation, position sensor does not detect and draws the station and has to draw the cup and wait to draw, control system triggers and draws the motor start, drive simultaneously through drawing a set drive disk 34 and draw set 33 and business turn over material drive component 36 and rotate, business turn over material drive component 36 drives two business turn over material wheels 351 simultaneously when rotating and rotates, one of them business turn over material wheel 351 rotates and drives its helping hand pole 352 along drawing concentrated chamber 31 inside track route cooperation and rotate 90 degrees, draw concentrated chamber 31 inner wall under the extrusion of helping hand pole, compress spring 353 with helping hand pole 352 elastic connection. When the receiving cavity of the material inlet and outlet wheel 351 rotates to correspond to the inlet of the extracting cup of the extracting and concentrating cavity shell 31, the extracting cup 12 conveyed by the extracting cup conveyor 4 enters the receiving cavity, the material inlet and outlet wheel continues rotating for 270 degrees, the inner wall of the extracting and concentrating cavity shell generates extrusion force on the extracting cup, the extracting cup continues to extrude the boosting rod, at the moment, until the receiving cavity corresponds to the extracting station of the extracting disc 33, the compression spring is released, the boosting rod 352 pushes the extracting cup 12 in the receiving cavity to enter the extracting station corresponding to the extracting disc 33, and therefore feeding of the corresponding extracting station is completed.
The position sensor 317 detects the extraction cup 12 on the extraction station, if the extraction cup 12 is detected, the control system triggers the vacuum electromagnetic valve 2 corresponding to the extraction station to open, the vacuum electromagnetic valve 2 conveys the extraction solvent to the extraction cup 12 corresponding to the extraction station, and the traditional Chinese medicine and the extraction solvent in the extraction cup are subjected to vacuum ultrasonic immersion through the ultrasonic wave generation system 320, so that the traditional Chinese medicine extraction process is completed. When the vacuum solenoid valve delivers the extraction solvent to the extraction cup 12, the liquid level sensor 318 is used for detecting the liquid level in the extraction cup, and when the liquid level reaches the set height, the vacuum solenoid valve 2 is triggered to close, and the delivery of the extraction solvent to the extraction cup 12 is stopped. The extracting cup 12 conveys extracting solution to the concentration area of the extracting concentration cavity shell 31, after the conveying is finished, the control system triggers the extracting motor to rotate for a set angle, and the extracting disc is driven to rotate the extracting cup of the next extracting station to the position corresponding to the concentration area. And (5) performing reciprocating circulation and continuously extracting until the set extraction times are finished. For the extraction cup which finishes extraction, when the extraction station where the extraction cup is located rotates under the rotation of the extraction disc, when the position of the extraction cup does not reach the position corresponding to the receiving cavity of the other material inlet and outlet wheel, the inner wall of the extraction concentration cavity shell generates extrusion force on the extraction cup, the elastic piece of the extraction cup push-out component is compressed under the extrusion of the extraction cup, the push rod of the extraction cup shrinks until the extraction station corresponds to the receiving cavity of the other material inlet and outlet wheel, the elastic piece is released, and the extraction cup push-out rod pushes the extraction cup into the receiving cavity of the other material inlet and outlet wheel. After the extracting motor rotates for a set angle, the other material inlet and outlet wheel rotates for 90 degrees until the receiving cavity of the other material inlet and outlet wheel corresponds to the extracting cup outlet of the extracting and concentrating cavity shell, and the boosting rod pushes the extracting cup which is extracted into the extracting cup inlet of the extracting cup conveyor under the action of the compression spring so as to participate in the next extraction. The concentration actuator 39 performs concentration on the extracting solution delivered by the extracting cup in the concentration area to obtain an extract, and outputs the extract to the leaching outlet 313.
In this embodiment, as shown in fig. 4, the extracting cup 12 includes an extracting cup housing 121, a traditional Chinese medicine filter cup 122, and a siphon pipe 123, wherein the traditional Chinese medicine filter cup 122 is disposed in the extracting cup housing 121, and the siphon pipe is communicated with the extracting cup housing 121. The traditional Chinese medicine filter cup 122 is used for containing traditional Chinese medicines, and after the siphon pipeline is filled with the extracting solution, the extracting solution in the shell of the extracting cup can be continuously conveyed to a concentration area of the extracting concentration cavity through the siphon pipeline by utilizing the action force phenomenon of the height difference of the liquid level.
Specifically, after the set time of soaking the traditional Chinese medicine is reached, the control system triggers the vacuum electromagnetic valve to be opened again to convey the set amount of extraction solvent to the extraction cup, so that the extraction solvent reaches the highest point of the siphon pipeline of the extraction cup, the control system triggers the vacuum electromagnetic valve to be closed, and the siphon pipeline conveys the extraction liquid to the concentration area of the extraction concentration cavity to concentrate the traditional Chinese medicine extraction liquid.
In this embodiment, the extracting motor 32 is a stepping speed reducing motor for providing power for accurate positioning of the extracting disc, the concentrating motor 37 is a dc speed reducing motor for providing power with adjustable rotation speed for the concentrating actuator 39, and both the extracting motor 32 and the concentrating motor 37 are fixedly connected to the extracting and concentrating cavity housing 31. In this embodiment, the extraction tray 33, the feeding and discharging member 35 and the concentration actuator 39 are all installed in the extraction and concentration chamber 3.
Further, as shown in fig. 5, the picking tray transmission part 34 includes a picking tray large pulley 341, a picking tray small pulley 342, a picking tray synchronous belt 343, a picking tray transmission shaft 344, a picking tray large pulley retainer ring 345, and a picking tray small pulley retainer ring 346; the large extraction disc pulley retainer 345 and the small extraction disc pulley retainer 346 are respectively arranged at the bottoms of the large extraction disc pulley 341 and the small extraction disc pulley 342, the outer diameters of the large extraction disc pulley 345 and the small extraction disc pulley 342 are respectively larger than the inner diameter and the outer diameter of the large extraction disc pulley 341 and the small extraction disc pulley 342, the large extraction disc pulley 341 is coaxially fixed on the transmission shaft 344 of the extraction disc, the small extraction disc pulley 342 is coaxially fixed on the output shaft of the extraction motor 32, and the synchronous extraction disc 343 is respectively arranged at the small extraction disc pulley 342 and the large extraction disc pulley 341 in a transmission winding manner; the extraction disc drive shaft 344 and the extraction disc 33 are coaxially fixed.
During operation, the small extracting disc belt wheel 342 is driven by the extracting motor to rotate, the small extracting disc belt wheel 342 drives the large extracting disc belt wheel 341 to rotate through the extracting disc synchronous belt 343, and the large extracting disc belt wheel 341 drives the extracting disc transmission shaft 344 to rotate, so that the extracting disc transmission shaft 344 drives the extracting disc 33 to rotate.
Further, as shown in fig. 6, the feeding and discharging transmission part 36 includes a feeding and discharging large pulley 361, a feeding and discharging synchronous belt 362, a feeding and discharging small pulley 363, a feeding and discharging auxiliary small pulley 364, a feeding and discharging large pulley retainer ring 365, a feeding and discharging small pulley retainer ring 366, a feeding and discharging auxiliary small pulley retainer ring 367, a feeding and discharging transmission shaft 368, and a feeding and discharging auxiliary transmission shaft 369; the feeding and discharging large belt wheel retainer ring 365, the feeding and discharging small belt wheel retainer ring 366 and the feeding and discharging auxiliary small belt wheel retainer ring 367 are respectively arranged at the bottoms of the feeding and discharging large belt wheel 361, the feeding and discharging small belt wheel 363 and the feeding and discharging auxiliary small belt wheel 364, and the outer diameters of the feeding and discharging large belt wheel 361, the feeding and discharging small belt wheel 363 and the feeding and discharging auxiliary small belt wheel 364 are respectively larger than the outer diameters of the feeding and discharging large belt wheel 361, the feeding and discharging small belt wheel 363 and the feeding and; the feeding and discharging large belt wheel 361 is in transmission connection with the extraction tray transmission part 34 (in this embodiment, is specifically coaxially fixed to the extraction tray transmission shaft 344), the feeding and discharging small belt wheel 363 is coaxially fixed to the feeding and discharging transmission shaft 368, the feeding and discharging auxiliary small belt wheel 364 is coaxially fixed to the feeding and discharging auxiliary transmission shaft 369, and the feeding and discharging synchronous belt 362 is respectively in transmission winding with the feeding and discharging large belt wheel 361, the feeding and discharging small belt wheel 363, and the feeding and discharging auxiliary small belt wheel 364; one of the wheels is coaxially fixed to the feeding and discharging transmission shaft 368, and the other wheel is coaxially fixed to the feeding and discharging auxiliary transmission shaft 369.
When the automatic feeding and discharging device works, the extracting disc can simultaneously drive the feeding and discharging large belt wheel 361 to rotate when rotating, and the feeding and discharging large belt wheel 361 drives the feeding and discharging small belt wheel 363 and the feeding and discharging auxiliary small belt wheel 364 to rotate together through the feeding and discharging synchronous belt 362. The small feeding and discharging belt wheel 363 drives the feeding and discharging transmission shaft 368 to rotate, the small feeding and discharging belt wheel 364 drives the feeding and discharging auxiliary transmission shaft 369 to rotate, the feeding and discharging transmission shaft 368 and the feeding and discharging auxiliary transmission shaft 369 respectively drive the two feeding and discharging wheels 351 to rotate together, and feeding of the extraction station of the extraction disc and taking of materials from the extraction station of the extraction disc after extraction are simultaneously realized.
Further, as shown in fig. 8, the concentration actuator 39 includes a concentration fixing block 391, a film pulling plate 393, a film scraping plate 394 and a concentration baffle 392; the concentration fixed block 391 is positioned at the center, a plurality of membrane scraping plates 394 are arranged around the concentration fixed block 391 in a vortex shape, and one end of each membrane scraping plate is fixed on the concentration fixed block 391; at least one film drawing plate 393 is arranged between every two film scraping plates 394, and the two ends of the film drawing plate 393 are respectively connected to the two film scraping plates 394; the concentration baffle 392 is fixedly connected above the film drawing plate 393 and the film scraping plate 394, and the concentration fixed block 391 is in transmission connection with the concentration actuator transmission part 38.
The concentration area is substantially divided into a heating area 200, an evaporation area 300 and an extract collecting area 400, wherein the heating area 200 is outside the concentration actuator 39, the evaporation area 300 is the area enclosed between the film pulling plate 393 and the two film scraping plates 394, and the extract collecting area 400 is below the fixed block. The concentration actuator divides the extracting solution into 3 states, and the extracting solution is concentrated and heated, concentrated and membrane-stretched, concentrated and membrane-collected. The extraction cup conveys the extracting solution to a concentration area of the extraction concentration cavity for concentrating the traditional Chinese medicine extracting solution, and specifically, the extracting solution is firstly conveyed into a heating area of the concentration area, and the heating area is heated by heating water from a refrigeration and heating recovery system. After the concentration motor is started, the transmission part of the concentration actuator is driven to rotate, the transmission part of the concentration actuator drives the concentration fixing block 391 to rotate, and the film pulling plate 393 and the film scraping plate 394 rotate together. A gap is formed between the film-drawing plate and the bottom of the extraction and concentration cavity shell, so that the extracting solution can be pushed to form a layer of film in the evaporation area, the extracting solution is rapidly concentrated in the evaporation area to obtain a concentrated extract, and an extraction solvent in the extracting solution is evaporated to the solvent condensation storage cavity. And the scraping plate collects the concentrated extract in the evaporation area to an extract collection area along the angle of the scraping plate, and the concentrated extract is sent to an online detection system through an extract outlet. The concentrating baffle is used for preventing the extracting solution from entering the evaporation zone.
Further, as shown in fig. 10, the transmission component of the concentration actuator includes a shaft coupler 381, a concentration link 382, a concentration small pulley 383, a concentration small pulley retaining ring 384, a concentration transmission shaft 385, a concentration large pulley 386, a concentration large pulley retaining ring 387, a concentration synchronous belt 388; the shaft coupler 381 is coaxially fixed to an output shaft of the concentration motor 37 and the concentration link 382, respectively, and the concentration link 382 is coaxially fixed to the concentration pulley 383; the concentrated large belt wheel 386 is coaxially fixed on the concentrated transmission shaft 385, and the concentrated synchronous belt 388 is respectively wound on the concentrated large belt wheel 386 and the concentrated small belt wheel 383 in a transmission manner; the rich-small pulley stopper 384 and the rich-large pulley stopper 387 are provided at the bottoms of the rich-small pulley 383 and the rich-large pulley 386, respectively, and have outer diameters larger than those of the rich-small pulley 383 and the rich-large pulley 386, respectively; the concentration transmission shaft 385 is in transmission connection with the concentration actuator 39 (in this embodiment, a concentration fixing block coaxially fixed to the concentration actuator). The setting of band pulley retaining ring prevents that the hold-in range from droing from the band pulley in rotating.
During operation, the output shaft of the concentration motor 37 drives the shaft coupler 381 to rotate, the shaft coupler 381 drives the concentration link rod 382 to rotate, the concentration link rod 382 drives the concentration belt pulley 383 to rotate, and thus the concentration belt pulley 383 drives the concentration large belt pulley 386 to rotate through the concentration synchronous belt 388; the concentration large belt wheel 386 drives the concentration transmission shaft 385 to rotate, and finally the concentration actuator 39 is driven to rotate by the concentration transmission shaft 385.
Further, as shown in fig. 11, the tachometer means 310 includes a tachometer sensor 3102 and a tachometer disk 3103; the speed measuring disk 3103 is fixedly connected with the concentrated transmission shaft 385, the speed measuring disk 3103 corresponds to the speed measuring sensor 3102, and the speed measuring sensor is electrically connected to the control system. In this embodiment, the speed measurement component further includes a speed measurement sensor support 3101, the speed measurement sensor 3102 is fixedly connected to the speed measurement sensor support 3101, and the speed measurement sensor support 3101 is fixedly connected to the support plate 9.
When extracting the concentration, concentrated transmission shaft 385 rotates and can drive speed measuring disc 3103 to rotate simultaneously, speed measuring disc 3013 is last to have a plurality of points of testing the speed (be equipped with 6 points of testing the speed in this embodiment, also can set up the quantity of the point of testing the speed according to actual need, it is more to test the speed, it is more accurate to record rotational speed data), each point of testing the speed is corresponding with speed sensor 3102 and transmits signal input to speed sensor in proper order, realize measuring concentrated executor real-time work rotational speed.
Further, the ultrasonic generation system 320 includes an ultrasonic generator and an ultrasonic transducer, the ultrasonic generator drives the ultrasonic transducer, and the ultrasonic transducer is fixedly connected to the extraction concentration chamber housing 31. In the process of extracting and concentrating, the wall breaking phenomenon of the medicinal materials can be caused by the ultrasonic generation system, and the soaking time is reduced.
In the present embodiment, as shown in fig. 13, the extraction tray 3 has a plurality of extraction stations, and the number of the solvent inlet 312, the liquid level sensor 318, the position sensor 317, and the vacuum solenoid valve 2 of the extraction concentration chamber is equal to the number of the extraction stations of the extraction tray, and corresponds to each extraction station of the extraction tray 33.
Furthermore, a layer of polyurethane thermal insulation material may be disposed inside the extraction concentration chamber housing 31 to enhance the thermal insulation effect.
In this embodiment, as shown in fig. 14, the extraction cup conveyor 4 includes a bottom plate 40, a housing frame 41, a motor support 42, a driving deceleration motor 43, a driving small pulley 44, a driving large pulley 45, a driving timing belt 46, a driving roller 47, a driven roller 48, a supporting roller 49, a lining plate 410, a conveying belt 411, a conveying belt guide wheel 412, a baffle 413, and a tensioning device 414, where the driving deceleration motor 43 is electrically connected to the control system; the driving small belt pulley 44 is coaxially connected with an output shaft of the driving speed reduction motor 43, the driving synchronous belt 46 is in transmission connection with the driving small belt pulley 44 and the driving large belt pulley 45, the driving large belt pulley 45 is coaxially connected with the driving roller 47, the supporting roller 49 is arranged below the conveying belt 411, a lining plate 410 is arranged above the supporting roller 41, the driven roller 48 is connected with the tensioning device 414, the conveying belt 411 is in transmission connection with the driving roller 47 and the driven roller 48, the surface of the conveying belt 411 is provided with a through hole, a conveying belt guide wheel 412 is arranged, and the conveying belt guide wheel 412 is slidably arranged with the baffle 413; the housing frame body 41, the motor support 42 and the baffle 413 are fixedly connected to the bottom plate 40, and the driving speed reduction motor 43 is fixed on the motor support 42.
In this embodiment, the bottom plate 40, the housing frame body 41 and the motor frame 42 play a role of integral fixing and supporting when the extraction cup conveyor works, the bottom plate 40 is fixedly connected with the support plate 9, the tension device 414 is fixed to the bottom plate 40, and the carrier roller 49 is fixed to the housing frame body 41. The driving gear motor 43, the small driving belt wheel 44, the large driving belt wheel 45, the driving synchronous belt 46 and the driving roller 47 are driving devices, the driving gear motor 43 is fixed on the motor support 42 and drives the small driving belt wheel 44 to rotate, so that the driving synchronous belt 46 drives the large driving belt wheel 45 to rotate together with the driving roller 47, the driving roller 47 drives the driven roller 48 to rotate through the conveying belt, and the extracting cup is conveyed into the extracting concentration cavity through the conveying belt. In this embodiment, the tensioning device 414 is a screw-jack type, and is used to keep the conveyor belt 411 at a predetermined initial tension so as not to slip on the driving roller or the driven roller. The conveying belt 411 is provided with the conveying belt guide wheel 412 in a perforated manner, and the conveying belt guide wheel 412 is connected with the baffle 413 in a sliding manner, so that the deviation of the conveying belt 411 during the operation in a curve can be prevented. The carrier roller 49 is rotatably connected with the frame 41, so that the impact of materials on the conveying belt 411 can be reduced, and the deviation of the conveying belt 411 can be prevented.
In this embodiment, as shown in fig. 15, the online detection system 5 includes a peristaltic pump 50, a refractometer 51, and an electric three-way reversing valve (L-shaped) 52, and the peristaltic pump 50, the refractometer 51, and the electric three-way reversing valve 52 are all electrically connected to the control system; an input port 501 of the peristaltic pump is communicated with an extract outlet 313 of the extraction concentration cavity, an output port 502 of the peristaltic pump is communicated with an input port 511 of the refractometer 51, and an output port 512 of the refractometer 51 is communicated with an extract inlet 521 of the electric three-way reversing valve 52; the unqualified extract outlet 522 of the electric three-way reversing valve 52 is communicated with the extract reflux port 314 of the extraction concentration cavity, and the qualified extract outlet 523 is communicated with the extract storage tank 13. In this embodiment, the extraction concentration chamber 3, the peristaltic pump 50, the refractometer 51, the electric three-way reversing valve (L-shaped) 52 and the extract storage tank are all connected by pipes. In this embodiment, the refractometer 51, the electric three-way reversing valve 52 and the peristaltic pump 50 are all fixedly connected to the support plate 9.
During the extraction and concentration process, undetected extract obtained by extraction and concentration flows out from an extract outlet 313 of an extraction and concentration cavity 3, is reversely conveyed to a refractometer 51 of an online detection system through a peristaltic pump 50 for concentration detection, the refractometer compares the detection result with the standard concentration data of traditional Chinese medicines in a database, when the extract concentration does not reach the standard concentration, the control system modifies the set parameters (the rotating speed of a concentration motor, the heating temperature of heating water provided by a refrigeration and heating recovery system and the like) of the extraction and concentration cavity, and opens an unqualified extract outlet 522 triggering an electric three-way reversing valve 52 to convey the unqualified extract into the extraction and concentration cavity again for concentration; if the concentration of the extract is qualified, the control system opens a qualified extract outlet 523 which touches the electric three-way reversing valve (L-shaped) 52, and the qualified extract is conveyed to an extract storage tank for storage through reversing by the electric three-way reversing valve (L-shaped) 52. Through the arrangement of the on-line detection system, sampling detection is not needed in the process of extracting and concentrating the traditional Chinese medicine, and real-time monitoring and continuous concentration can be realized.
In the present embodiment, as shown in fig. 16, the cooling and heat recovery system 6 includes a refrigerant compressor 61, a plate heat exchanger 62, a condenser 63, a throttling device 64, an evaporator 65, a gas-liquid separator 66, a cold-hot water tank 67, and a circulating water pump 68; as shown in fig. 17 to 18, the cold and hot water tank includes a heated water tank 671, a heating mechanism 672, a heated water outlet 673, a heated water return 674, a condensed water tank 675, a condensed water outlet 676, a condensed water return 677, a hot water circulation outlet 678, a hot water circulation inlet 679, a condensed water circulation outlet 6710, a condensed water circulation inlet 6711, a temperature sensor 6712, a liquid level sensor 6713, an insulating layer 6714, and a cold and hot water tank housing 6715; the refrigerant compressor 61, the circulating water pump 68, the temperature sensor 6712, the liquid level sensor 6713 and the heating mechanism 672 are electrically connected to the control system;
the heating mechanism 672 is connected to the heating water tank 671; the heating water tank 671 and the condensed water tank 675 are installed in a cooling water tank housing 6715, a heat insulation layer 6714 is filled in the cooling water tank housing 6715, the heating water outlet 673, the heating water return port 674, the hot water circulating inlet 679 and the hot water circulating outlet 678 are respectively communicated with the heating water tank 671, and the condensed water outlet 676, the condensed water return port 677, the condensed water circulating outlet 6710 and the condensed water circulating inlet 6711 are respectively communicated with the condensed water tank 675; the heating water tank 671 and the condensed water tank 675 are respectively connected with a temperature sensor 6712 and a liquid level sensor 6713;
the refrigerant compressor 61, the plate heat exchanger 62, the condenser 63, the throttling device 64, the evaporator 65 and the gas-liquid separator 66 are sequentially communicated, and the gas-liquid separator 66 is communicated with the refrigerant compressor 61; the inlet of the circulating water pump 68 is respectively communicated with the hot water circulating outlet 678 and the condensed water circulating outlet 6710, and the outlet is respectively communicated with the circulating inlet of the plate heat exchanger 62 and the circulating inlet of the evaporator 65; the circulation outlet of the plate heat exchanger 62 is communicated with the hot water circulation inlet 679, and the circulation outlet of the evaporator 65 is communicated with the condensed water circulation inlet 6711.
In this embodiment, the refrigerant compressor, the plate heat exchanger, the condenser, the throttling device, the evaporator, the gas-liquid separator, the cold-hot water tank, and the circulating water pump are all fixedly connected by pipelines. As shown in fig. 19, during the extraction and concentration process, the refrigerant compressor 61, the plate heat exchanger 62, the condenser 63, the throttling device 64, the evaporator 65, and the gas-liquid separator 66 function to provide a refrigerant carrying medium to the condensed water tank 675 and a heat carrying medium to the heated water tank 671. On the basis of consuming certain electric energy, the refrigerant compressor 61 obtains the low-temperature and low-pressure gaseous refrigerant which absorbs heat from the evaporator 65 from the gas-liquid separator 66, and the low-temperature and low-pressure gaseous refrigerant is compressed into a high-temperature and high-pressure gaseous refrigerant and is conveyed to the plate heat exchanger 62; the heat carrier in the heating water tank enters an inlet of the circulating water pump 68 through the hot water circulating outlet 678, then enters the plate heat exchanger through an outlet of the circulating water pump 68, exchanges heat with the plate heat exchanger, and finally returns to the heating water tank 671 through the hot water circulating inlet 679, so that the heat carrier in the heating water tank 671 is heated, and at the moment, the high-temperature and high-pressure gaseous refrigerant is condensed into a high-pressure medium-temperature gas-liquid mixed refrigerant. The condenser 63 fully condenses the high-pressure medium-temperature gas-liquid mixed refrigerant into a high-pressure normal-temperature liquid refrigerant; the high-pressure normal-temperature liquid refrigerant enters the throttling device 64, and the capillary component in the throttling device 64 throttles and reduces the pressure of the high-pressure normal-temperature liquid refrigerant, so that the liquid refrigerant is changed into a low-pressure low-temperature state and enters the evaporator. Since the inside diameter of the evaporator 65 is much larger than the diameter of the capillary member of the throttle device 64, the pressure of the liquid refrigerant suddenly decreases, and the liquid refrigerant is rapidly evaporated. The refrigerant carried by the condensed water tank 675 enters the inlet of the circulating water pump 68 through the condensed water circulating outlet 6710 and enters the evaporator 65 through the outlet of the circulating water pump 68, and the liquid refrigerant rapidly evaporated in the evaporator 65 absorbs heat from the refrigerant carried by the condensed water tank 675 until the liquid refrigerant is completely gasified and converted into low-pressure and low-temperature gaseous refrigerant, so that the process of cooling the refrigerant carried by the condensed water tank 675 is completed. The low pressure, low temperature gaseous refrigerant is filtered back into the refrigerant compressor by the gas-liquid separator 66. The cooling of the refrigerant carried by the condensed water tank and the heating of the heat carrying medium of the heating water tank are realized by the repeated circulation. The heating mechanism 672 has the effect that when the heat carrier in the heating water tank does not reach the set temperature, the heat carrier is heated to reach the required use temperature through auxiliary heating.
In this embodiment, as shown in fig. 20, the vacuum system 8 includes a muffler 81, a vacuum pump 82, a vacuum pressure reducing valve 83, a vacuum tank 84, a filter triplet 85, a vacuum pressure switch 86, a normally open vacuum switching valve 87, a normally open vacuum switching valve 88, and a normally closed vacuum switching valve 89, wherein the muffler 81, the vacuum pump 82, the vacuum pressure reducing valve 83, the vacuum tank 84, the filter triplet 85, the vacuum pressure switch 86, and the normally open vacuum switching valve 87 are sequentially communicated, and the normally open vacuum switching valve 87 is communicated with the solvent condensation storage chamber 1; and the second normally-open vacuum switching valve 88 is communicated between the extraction concentration cavity 3 and the extract storage tank 13, and the normally-closed vacuum switching valve 89 is communicated between the second normally-open vacuum switching valve 88 and the extract storage tank 13.
During the extraction and concentration process, the vacuum pressure switch 86 is started, and the vacuum switching valve I87, the filter triplet 85, the vacuum tank 84, the vacuum pressure reducing valve 83, the vacuum pump 82 and the muffler 81 are opened frequently to evacuate the volumes of the solvent condensation storage cavity 1 and the extraction and concentration cavity 3 to reach the set vacuum degree. The vacuum pressure switch 86 is a pressure protection automatic controller of the vacuum system to prevent the pressure in the system from being too high or too low; the vacuum gauge 319 plays a role of monitoring the vacuum degree value in the device in real time. The normally closed vacuum switching valve 89 is used for switching the normally open vacuum switching valve II 88 into a closed mode and switching the normally closed vacuum switching valve 89 into an open mode to fill atmospheric air into the extract storage tank so as to take down the extract storage tank if the extract storage tank is separated.
In this embodiment, as shown in fig. 21, the man-machine interface of the touch screen all-in-one machine 7 includes 6 units, which are an auxiliary device unit 71, a vacuum adjusting unit 72, a conveyor unit 73, an extracting unit 74, a concentrating unit 75, and a process detecting unit 76; the auxiliary equipment unit comprises a heating water tank liquid level alarm display, a condensed water tank liquid level alarm display, a heat supply temperature display, a cold and heat source on/off switch, an auxiliary heat temperature regulation and a refrigeration temperature display; the vacuum adjusting unit comprises a vacuum switch, a vacuum degree adjusting unit and a vacuum degree display unit; the conveyor unit comprises an extraction cup conveyor switch, a rotating speed display and a rotating speed regulation; the extraction unit comprises extraction starting on/off, monomer immersion time display, monomer immersion time adjustment, extraction station display, monomer immersion frequency display and monomer immersion frequency adjustment; the concentration unit comprises concentration starting on/off, rotating speed display and rotating speed adjustment; the process detection unit comprises a standard substance concentration curve and a product concentration curve. Before the extraction and concentration work is started, operation parameters (in the embodiment, the operation parameters comprise cold and heat source opening, radiant heat opening, heating temperature of 60 ℃, refrigerating temperature of 3 ℃, vacuum opening, vacuum degree adjustment of 0.75Mpa, monomer extraction times, monomer immersion time and concentration rotating speed) can be set through each unit of the touch screen integrated machine.
Various corresponding changes and modifications can be made by those skilled in the art according to the above technical solutions and concepts, and all such changes and modifications should be included in the protection scope of the present invention.

Claims (10)

1. A novel continuous extraction and concentration device is characterized by comprising a solvent condensation storage cavity, a vacuum solenoid valve, an extraction and concentration cavity, an extraction cup conveyor, an online detection system, a refrigeration and heat recovery system, a touch screen integrated machine, a vacuum system, an extraction cup, an extract storage tank and a control system; an extraction solvent outlet of the solvent condensation storage cavity is communicated with a solvent inlet of the vacuum electromagnetic valve; a solvent outlet of the vacuum electromagnetic valve is connected with a solvent inlet of the extraction concentration cavity; an extract outlet of the extraction concentration cavity is communicated with an extract inlet of the online detection system; an extract outlet of the online detection system is respectively communicated with an extract inlet of the extract storage tank and an extract reflux port of the extraction concentration cavity; a condensed water outlet and a condensed water return port of the refrigeration heat recovery system are respectively communicated with a condensed water inlet and a condensed water outlet of the solvent condensation storage cavity; the heating water outlet and the heating water return port of the refrigeration heat recovery system are respectively communicated with the heating water inlet and the heating water outlet of the extraction concentration cavity; an extraction cup inlet and an extraction cup outlet of the extraction cup conveyor respectively correspond to an extraction cup outlet and an extraction cup inlet of the extraction concentration cavity; the vacuum system is connected with the solvent condensation storage cavity; the control system is respectively in control connection with the solvent condensation storage cavity, the vacuum solenoid valve, the extraction concentration cavity, the extraction cup conveyor, the online detection system, the refrigeration heat recovery system, the vacuum system and the touch screen all-in-one machine.
2. The novel continuous extraction and concentration device as claimed in claim 1, wherein the solvent condensation storage cavity comprises a solvent condensation storage cavity shell, a vortex condensation coil, a condensed water inlet, a condensed water outlet, a solvent filling port, a vacuum port, an extraction solvent outlet and a vacuum pipeline; the condensed water inlet and the condensed water outlet are respectively communicated with the vortex condensing coil; the solvent filling port, the vacuum port, the extraction solvent outlet and the vacuum pipeline are respectively communicated with the solvent condensation storage cavity shell, and the vacuum port is communicated with the vacuum system; the vacuum pipeline is also communicated with the extraction concentration cavity.
3. The novel continuous extraction and concentration device according to claim 1, wherein the extraction and concentration cavity comprises an extraction and concentration cavity shell, an extraction motor, an extraction disc transmission part, an extraction disc, a feeding and discharging part, a feeding and discharging transmission part, a concentration motor, a concentration actuator transmission part, a concentration actuator, a speed measurement part, an extraction and concentration cavity vacuum port, a solvent inlet, an extract outlet, an extract reflux port, a heating water inlet, a heating water outlet, a position sensor, a liquid level sensor, a vacuum pressure gauge and an ultrasonic generation system; the extraction motor, the concentration motor, the speed measurement part, the position sensor, the liquid level sensor, the vacuum pressure gauge and the ultrasonic generation system are all electrically connected to the control system; the extracting and concentrating cavity shell is provided with an extracting cup inlet and an extracting cup outlet which respectively correspond to the extracting cup outlet and the extracting cup inlet of the extracting cup conveyor; the concentration actuator is positioned in a concentration area of the extraction and concentration cavity shell, and the extraction disc is arranged in the extraction and concentration cavity shell and corresponds to the position of the concentration area;
the extracting motor is in transmission connection with the extracting disc through an extracting disc transmission part, the feeding and discharging transmission part is in transmission connection with the extracting disc transmission part, and the feeding and discharging transmission part is in transmission connection with the feeding and discharging part; the concentration motor is in transmission connection with the concentration actuator through a concentration actuator transmission part, and the speed measurement part is connected with the concentration actuator transmission part; the extraction concentration cavity vacuum port, the solvent inlet, the extract outlet, the extract reflux port, the heating water inlet, the heating water outlet and the vacuum pressure gauge are all communicated with the extraction concentration cavity shell, and the extraction concentration cavity vacuum port is also communicated with the solvent condensation storage cavity; the positions of the solvent inlet, the position sensor and the liquid level sensor respectively correspond to the positions of the extraction stations of the extraction disc; the ultrasonic generating system is connected with the extraction and concentration cavity shell;
the feeding and discharging part comprises at least two feeding and discharging wheels, each feeding and discharging wheel is provided with a receiving cavity, and an extraction cup feeding part is arranged in each receiving cavity; the receiving cavity of one of the material inlet and outlet wheels can correspond to an extraction cup inlet of the extraction concentration cavity shell and an extraction station of the extraction disc through rotation, and the receiving cavity of the other material inlet and outlet wheel can correspond to an extraction cup outlet of the extraction concentration cavity shell and an extraction station of the extraction disc through rotation; each feeding and discharging wheel is in transmission connection with the feeding and discharging transmission part; and the extraction station of the extraction disc is correspondingly provided with an extraction cup push-out component.
4. The novel continuous extraction and concentration device according to claim 3, wherein the extraction disc transmission part comprises an extraction disc large belt pulley, an extraction disc small belt pulley, an extraction disc synchronous belt and an extraction disc transmission shaft; the large extracting disc belt wheel is coaxially fixed on the extracting disc transmission shaft, the small extracting disc belt wheel is coaxially fixed on an output shaft of the extracting motor, and the extracting disc synchronous belt is respectively wound on the small extracting disc belt wheel and the large extracting disc belt wheel in a transmission manner; the extracting disc transmission shaft and the extracting disc are coaxially fixed.
5. The novel continuous extraction and concentration device as claimed in claim 3, wherein the feeding and discharging transmission part comprises a large feeding and discharging belt wheel, a synchronous feeding and discharging belt, a small feeding and discharging belt wheel, a small feeding and discharging auxiliary belt wheel, a feeding and discharging transmission shaft and a feeding and discharging auxiliary transmission shaft; the feeding and discharging large belt wheel is connected with the extraction disc transmission part in a transmission way, the feeding and discharging small belt wheel is coaxially fixed on the feeding and discharging transmission shaft, the feeding and discharging auxiliary small belt wheel is coaxially fixed on the feeding and discharging auxiliary transmission shaft, and the feeding and discharging synchronous belt is respectively wound on the feeding and discharging large belt wheel, the feeding and discharging small belt wheel and the feeding and discharging auxiliary small belt wheel in a transmission way; one of the material inlet and outlet wheels is coaxially fixed on the material inlet and outlet transmission shaft, and the other material inlet and outlet wheel is coaxially fixed on the material inlet and outlet auxiliary transmission shaft.
6. The novel continuous extraction and concentration device as claimed in claim 3, wherein the concentration actuator comprises a concentration fixed block, a membrane drawing plate, a membrane scraping plate and a concentration baffle plate; the concentration fixed block is positioned at the central position, the plurality of membrane scraping plates are arranged around the concentration fixed block in a vortex shape, and one end of each membrane scraping plate is fixed on the concentration fixed block; at least one film drawing plate is arranged between every two film scraping plates, and two ends of the film drawing plate are respectively connected with the two film scraping plates; concentrated baffle fixed connection is in the top of drawing the membrane board and scraping the membrane board, concentrated fixed block transmission connect in concentrated executor drive disk assembly.
7. The novel continuous extraction and concentration device as claimed in claim 3 or 6, wherein the concentration actuator transmission component comprises a coupling, a concentration link rod, a concentration small belt wheel retainer ring, a concentration transmission shaft, a concentration large belt wheel retainer ring and a concentration synchronous belt; the shaft coupling is coaxially fixed to an output shaft of the concentration motor and the concentration link rod respectively, and the concentration link rod is coaxially fixed to the concentration belt pulley; the concentration large belt wheel is coaxially fixed on the concentration transmission shaft, and the concentration synchronous belt is respectively wound on the concentration large belt wheel and the concentration small belt wheel in a transmission manner; the concentration belt pulley retaining ring and the concentration large belt pulley retaining ring are respectively sleeved on the outer edges of the concentration belt pulley and the concentration large belt pulley; the concentration transmission shaft is in transmission connection with the concentration actuator.
8. The novel continuous extraction and concentration device as claimed in claim 1, wherein the extraction cup conveyor comprises a bottom plate, a housing frame body, a motor support, a driving gear motor, a driving small belt wheel, a driving large belt wheel, a driving synchronous belt, a driving roller, a driven roller, a carrier roller, a lining plate, a conveying belt guide wheel, a baffle plate and a tensioning device, wherein the driving gear motor is electrically connected to the control system; the driving small belt pulley is coaxially connected with an output shaft of the driving speed reduction motor, the driving synchronous belt is in transmission connection with the driving small belt pulley and the driving large belt pulley, the driving large belt pulley is coaxially connected with the driving roller, the carrier roller is arranged below the conveying belt, the lining plate is arranged above the carrier roller, the driven roller is connected with the tensioning device, the conveying belt is in transmission connection with the driving roller and the driven roller, the surface of the conveying belt is provided with a through hole, the conveying belt guide wheel is arranged on the through hole, and the conveying belt guide wheel is slidably arranged on the baffle; the shell frame body, the motor support and the baffle are fixedly connected to the bottom plate, and the driving speed reduction motor is fixed to the motor support.
9. The novel continuous extraction and concentration device as claimed in claim 1, wherein the online detection system comprises a peristaltic pump, a refractometer and an electric three-way reversing valve, and the peristaltic pump, the refractometer and the electric three-way reversing valve are all electrically connected to the control system; an input port of the peristaltic pump is communicated with an extract outlet of the extraction concentration cavity, an output port of the peristaltic pump is communicated with an input port of the refractometer, and an output port of the refractometer is communicated with an extract inlet of the electric three-way reversing valve; and the unqualified extract outlet of the electric three-way reversing valve is communicated with the extract reflux port of the extraction concentration cavity, and the qualified extract outlet is communicated with the extract storage tank.
10. The novel continuous extraction and concentration device as claimed in claim 1, wherein the refrigeration heat recovery system comprises a refrigerant compressor, a plate heat exchanger, a condenser, a throttling device, an evaporator, a gas-liquid separator, a cold-hot water tank and a circulating water pump; the cold and hot water tank comprises a heating water tank, a heating mechanism, a heating water outlet, a heating water return port, a condensed water tank, a condensed water outlet, a condensed water return port, a hot water circulation outlet, a hot water circulation inlet, a condensed water circulation outlet, a condensed water circulation inlet, a temperature sensor, a liquid level sensor, a heat preservation layer and a cold and hot water tank cover; the refrigerant compressor, the circulating water pump, the temperature sensor, the liquid level sensor and the heating mechanism are all electrically connected to the control system;
the heating mechanism is connected to the heating water tank; the heating water tank and the condensed water tank are arranged in a cold and hot water tank housing, a heat-insulating layer is filled in the cold and hot water tank housing, the heating water outlet, the heating water return port, the hot water circulation inlet and the hot water circulation outlet are respectively communicated with the heating water tank, and the condensed water outlet, the condensed water return port, the condensed water circulation outlet and the condensed water circulation inlet are respectively communicated with the condensed water tank; the heating water tank and the condensed water tank are respectively connected with a temperature sensor and a liquid level sensor;
the refrigerant compressor, the plate heat exchanger, the condenser, the throttling device, the evaporator and the gas-liquid separator are sequentially communicated, and the gas-liquid separator is communicated with the refrigerant compressor; an inlet of the circulating water pump is respectively communicated with the hot water circulating outlet and the condensed water circulating outlet, and outlets of the circulating water pump are respectively communicated with a circulating inlet of the plate heat exchanger and a circulating inlet of the evaporator; and a circulating outlet of the plate heat exchanger is communicated with the hot water circulating inlet, and a circulating outlet of the evaporator is communicated with the condensed water circulating inlet.
CN201920358433.2U 2019-03-20 2019-03-20 Novel continuous extraction and concentration device Active CN210205954U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109758784A (en) * 2019-03-20 2019-05-17 河北鑫民和医药科技开发有限责任公司 A kind of new type of continuous traditional Chinese medicine extraction enrichment facility
CN111855344A (en) * 2020-06-29 2020-10-30 河南广电计量检测有限公司 A preceding processing apparatus for pesticide residue detects
CN113018895A (en) * 2021-03-03 2021-06-25 江门职业技术学院 Natural purple rice dye and ultrasonic extraction equipment

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109758784A (en) * 2019-03-20 2019-05-17 河北鑫民和医药科技开发有限责任公司 A kind of new type of continuous traditional Chinese medicine extraction enrichment facility
CN109758784B (en) * 2019-03-20 2024-04-26 河北鑫民和医药科技开发有限责任公司 Continuous traditional chinese medicine draws enrichment facility
CN111855344A (en) * 2020-06-29 2020-10-30 河南广电计量检测有限公司 A preceding processing apparatus for pesticide residue detects
CN111855344B (en) * 2020-06-29 2023-09-15 河南广电计量检测有限公司 Pretreatment device for pesticide residue detection
CN113018895A (en) * 2021-03-03 2021-06-25 江门职业技术学院 Natural purple rice dye and ultrasonic extraction equipment

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