CN210180792U - Atmosphere quenching hot-pressing workstation - Google Patents

Atmosphere quenching hot-pressing workstation Download PDF

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Publication number
CN210180792U
CN210180792U CN201920766145.0U CN201920766145U CN210180792U CN 210180792 U CN210180792 U CN 210180792U CN 201920766145 U CN201920766145 U CN 201920766145U CN 210180792 U CN210180792 U CN 210180792U
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China
Prior art keywords
glove box
temperature sintering
sintering furnace
push rod
heating
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CN201920766145.0U
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Chinese (zh)
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Yongguo Cai
蔡永国
Liping Dai
代利平
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Henan Nobody Material Science And Technology Co Ltd
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Henan Nobody Material Science And Technology Co Ltd
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Abstract

The utility model discloses an atmosphere quenching hot-pressing workstation, which comprises a glove box and a high-temperature sintering furnace positioned at one side of the glove box, wherein the inner cavity of the glove box is communicated with a hearth of the high-temperature sintering furnace; a cooling base, a movable material receiving groove and a crucible positioned at the head of a rotating push rod are arranged at one end, close to the high-temperature sintering furnace, in the glove box from bottom to top, the rotating push rod is rotatably connected with a horizontal sliding seat, and a sealing plug for plugging a hearth of the high-temperature sintering furnace and a rotating torsion spring for axial resetting are arranged on the rotating push rod; and a heating and pressurizing testing mechanism is arranged at the other end of the glove box far away from the high-temperature sintering furnace. The utility model discloses simple structure, design benefit, each accredited testing organization is orderly, integrated in the glove box reliably, can make battery material be in the dustless high-purity environment of anhydrous anaerobic under the atmosphere protection all the time, has improved the accuracy of capability test result greatly, has shortened test work's cycle, has improved battery material's efficiency of software testing.

Description

Atmosphere quenching hot-pressing workstation
Technical Field
The utility model relates to a battery material test equipment technical field especially relates to an atmosphere quenching hot pressing workstation.
Background
The performance of the battery material directly affects the cost and durability of the finished battery, and therefore, performance testing of the battery material is an important task. Due to the particularity of battery materials, performance tests are mostly required to be carried out in an anhydrous, oxygen-free and dust-free high-purity environment under the atmosphere protection, and generally, high-temperature sintering is firstly carried out, then rapid quenching is carried out, and then the performance tests are carried out under the high-temperature pressurizing condition. The existing testing equipment is complex to operate, cannot ensure that the battery material is always in an anhydrous, oxygen-free and dust-free high-purity environment, cannot ensure the accuracy of a performance testing result, and has certain potential safety hazards.
Disclosure of Invention
In order to solve the problems, the utility model provides an atmosphere quenching hot-pressing workstation, which can adopt the following technical proposal:
the atmosphere quenching hot-pressing work station comprises a glove box and a high-temperature sintering furnace positioned on one side of the glove box, wherein the inner cavity of the glove box is communicated with a hearth of the high-temperature sintering furnace; a cooling base, a movable material receiving groove and a crucible positioned at the head of a rotating push rod are arranged at one end, close to the high-temperature sintering furnace, in the glove box from bottom to top, the rotating push rod is rotatably connected with a horizontal sliding seat, and a sealing plug for plugging a hearth of the high-temperature sintering furnace and a rotating torsion spring for axial resetting are arranged on the rotating push rod; and a heating and pressurizing testing mechanism is arranged at the other end of the glove box far away from the high-temperature sintering furnace.
The heating and pressurizing testing mechanism comprises a supporting frame, a horizontal sliding plate driven by a hydraulic oil cylinder is arranged in the supporting frame, a heating and pressurizing furnace is arranged between the horizontal sliding plate and a supporting frame top plate, and an upper pressing column fixedly connected to the supporting frame top plate and a lower pressing column fixedly connected to the horizontal sliding plate penetrate through a furnace wall of the heating and pressurizing furnace and extend into a hearth.
The glove box is an atmosphere protection type glove box.
And a water-cooling sealing flange is arranged between the glove box and the high-temperature sintering furnace.
An electric cabinet is arranged above the high-temperature sintering furnace.
The hydraulic oil cylinder is a pedal oil cylinder.
The heating and pressurizing testing mechanism further comprises a touch control screen and a digital display pressure gauge.
The atmosphere quenching hot-pressing workstation provided by the utility model has the advantages of simple structure and ingenious design, and all the testing mechanisms are orderly and reliably integrated in the glove box, so that the battery material is always in the water-free, oxygen-free and dust-free high-purity environment under atmosphere protection, the probability of oxidation is reduced, and the accuracy of performance test results is greatly improved; meanwhile, the material to be tested can be conveniently operated among all the working procedures, so that the manual operation errors are reduced, the period of the test work is shortened, and the test efficiency of the battery material is improved.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a cross-sectional view of fig. 1.
Detailed Description
As shown in figures 1 and 2, the atmosphere quenching hot pressing work station comprises an atmosphere protection type glove box 1 and a high-temperature sintering furnace 2 positioned on the left side of the atmosphere protection type glove box, wherein the inner cavity of the glove box 1 is communicated with a hearth of the high-temperature sintering furnace 2. A quartz furnace tube 2.2 which controls the heating time and the heating temperature through an electric cabinet 2.1 is arranged in the hearth of the high-temperature sintering furnace 2. In order to avoid the overhigh temperature of the glove box 1, a water-cooling sealing flange 3 is arranged at the connecting section of the glove box 1 and the high-temperature sintering furnace 2. The one end that is close to high temperature sintering stove 2 in the glove box 1 is installed horizontal sliding seat 4.1, and the rotation mounting groove in-connection on this horizontal sliding seat 4.1 has rotation push rod 4.2, and rotation push rod 4.2 can remove about along with horizontal sliding seat 4.1, can also carry out axial rotation under external force promotes to carry out axial through rotatory torsional spring 4.3 and reset. The head of the rotating push rod 4.2 is provided with a tungsten crucible 4.4 for containing samples, and the middle part is provided with a sealing plug 4.5 for plugging the hearth of the high-temperature sintering furnace 2. A movable material receiving copper groove 5 connected with the trolley is arranged below the horizontal sliding seat 4.1, and a cooling base 6 made of a water-cooling copper sleeve is contacted with the lower side of the material receiving copper groove 5. The other end of the glove box 1 far away from the high-temperature sintering furnace is provided with a heating and pressurizing testing mechanism 7. The heating and pressurizing testing mechanism 7 comprises a supporting frame 7.1, a horizontal sliding plate 7.3 is connected to left and right upright posts of the supporting frame 7.1 through a guide sliding sleeve 7.2, the horizontal sliding plate 7.3 is controlled to lift by a pedal hydraulic oil cylinder 7.4, a heating and pressurizing furnace 7.5 is installed between the horizontal sliding plate 7.3 and a top plate of the supporting frame 7.1, and a corundum upper pressing post 7.6 fixedly connected to the top plate of the supporting frame 7.1 and a corundum lower pressing post 7.7 fixedly connected to the horizontal sliding plate 7.3 penetrate through a furnace wall of the heating and pressurizing furnace 7.5 and extend into a hearth. A graphite mould 7.8 is arranged in the hearth. In addition, the heating and pressurizing test mechanism 7 is also provided with a touch control screen 7.9 and a digital display pressure gauge 7.10.
The utility model comprises two procedures of quenching and cooling and hot-pressing measurement when in use.
Firstly, the rotating push rod 4.2 is pulled to the rightmost end, a sample is placed in the tungsten crucible 4.4, then the rotating push rod 4.2 is pushed to the leftmost end, at the moment, the tungsten crucible 4.4 is positioned in the hearth of the high-temperature sintering furnace 2, and the sealing plug 4.5 just blocks the hearth of the high-temperature sintering furnace 2, so that heat is prevented from being dissipated outwards. Then, the quartz furnace tube 2.2 starts to be heated to a certain temperature, the sample in the tungsten crucible 4.4 is in a molten liquid state, at this time, the rotating push rod 4.2 is rapidly pulled out, meanwhile, the rotating push rod 4.2 is rotated to enable the tungsten crucible 4.4 to turn over by 100 degrees and pour the molten sample into the copper receiving groove 5, and then the rotating push rod 4.2 automatically returns to the original position under the action of the rotating torsion spring 4.3 to enable the tungsten crucible 4.4 to be kept horizontal. The cooling base 6 is in contact with the material receiving copper groove 5, so that the heat of the sample can be taken away quickly, and the purpose of quick cooling is achieved. After the sample is cooled, the trolley is pulled rightwards, so that the material receiving copper groove 5 leaves the horizontal sliding seat 4.1, and the cooled sample in the material receiving copper groove 5 is taken out.
Then, a cooling sample is loaded into a graphite mold 7.8, a furnace door of a heating and pressurizing furnace 7.5 is opened, the graphite mold 7.8 is placed on a corundum lower pressure column 7.7, a pressurizing pedal of a hydraulic oil cylinder 7.4 is stepped, a hydraulic station starts to work, the hydraulic oil cylinder 7.4 pushes a horizontal sliding plate 7.3 and a guide sliding sleeve 7.2 to lift upwards along a left upright post and a right upright post of a supporting frame 7.1, after the graphite mold 7.8 is contacted with the corundum upper pressure column 7.6, the reading of a digital display pressure gauge 7.10 is observed, and after the pressure applied on the graphite mold 7.8 reaches 1Mpa, the pressurizing pedal of the hydraulic oil cylinder 7.4 is stopped being stepped, so that pre-pressurizing is completed; and then, closing the furnace door, starting heating, and continuously pressurizing to the specified pressure according to the pressurizing step after the temperature of the hearth of the heating and pressurizing furnace 7.5 reaches a set value, so as to test the performance of the sample.

Claims (7)

1. An atmosphere quenching hot pressing workstation, characterized by: the device comprises a glove box and a high-temperature sintering furnace positioned on one side of the glove box, wherein the inner cavity of the glove box is communicated with a hearth of the high-temperature sintering furnace; a cooling base, a movable material receiving groove and a crucible positioned at the head of a rotating push rod are arranged at one end, close to the high-temperature sintering furnace, in the glove box from bottom to top, the rotating push rod is rotatably connected with a horizontal sliding seat, and a sealing plug for plugging a hearth of the high-temperature sintering furnace and a rotating torsion spring for axial resetting are arranged on the rotating push rod; and a heating and pressurizing testing mechanism is arranged at the other end of the glove box far away from the high-temperature sintering furnace.
2. The atmospheric quenching hot pressing station of claim 1, characterized in that: the heating and pressurizing testing mechanism comprises a supporting frame, a horizontal sliding plate driven by a hydraulic oil cylinder is arranged in the supporting frame, a heating and pressurizing furnace is arranged between the horizontal sliding plate and a supporting frame top plate, and an upper pressing column fixedly connected to the supporting frame top plate and a lower pressing column fixedly connected to the horizontal sliding plate penetrate through a furnace wall of the heating and pressurizing furnace and extend into a hearth.
3. An atmosphere quenching hot pressing station according to claim 1 or 2, characterized in that: the glove box is an atmosphere protection type glove box.
4. An atmosphere quenching hot pressing station according to claim 1 or 2, characterized in that: and a water-cooling sealing flange is arranged between the glove box and the high-temperature sintering furnace.
5. An atmosphere quenching hot pressing station according to claim 1 or 2, characterized in that: an electric cabinet is arranged above the high-temperature sintering furnace.
6. The atmospheric quenching hot pressing station of claim 2, characterized in that: the hydraulic oil cylinder is a pedal oil cylinder.
7. The atmospheric quenching hot pressing station of claim 2, characterized in that: the heating and pressurizing testing mechanism further comprises a touch control screen and a digital display pressure gauge.
CN201920766145.0U 2019-05-27 2019-05-27 Atmosphere quenching hot-pressing workstation Active CN210180792U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201920766145.0U CN210180792U (en) 2019-05-27 2019-05-27 Atmosphere quenching hot-pressing workstation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201920766145.0U CN210180792U (en) 2019-05-27 2019-05-27 Atmosphere quenching hot-pressing workstation

Publications (1)

Publication Number Publication Date
CN210180792U true CN210180792U (en) 2020-03-24

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Application Number Title Priority Date Filing Date
CN201920766145.0U Active CN210180792U (en) 2019-05-27 2019-05-27 Atmosphere quenching hot-pressing workstation

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112556426A (en) * 2020-12-15 2021-03-26 江西科技学院 Sintering furnace with gas-phase quenching function and quenching process thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112556426A (en) * 2020-12-15 2021-03-26 江西科技学院 Sintering furnace with gas-phase quenching function and quenching process thereof
CN112556426B (en) * 2020-12-15 2022-08-23 江西科技学院 Sintering furnace with gas-phase quenching function and quenching process thereof

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