CN210085632U - Bubble electrostatic spinning device for orderly controlling nano fiber molecule sequencing - Google Patents
Bubble electrostatic spinning device for orderly controlling nano fiber molecule sequencing Download PDFInfo
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- CN210085632U CN210085632U CN201920479759.0U CN201920479759U CN210085632U CN 210085632 U CN210085632 U CN 210085632U CN 201920479759 U CN201920479759 U CN 201920479759U CN 210085632 U CN210085632 U CN 210085632U
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- bubble
- pipe
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- nanofiber
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- 239000002121 nanofiber Substances 0.000 title claims abstract description 43
- 238000010041 electrostatic spinning Methods 0.000 title claims abstract description 26
- 238000012163 sequencing technique Methods 0.000 title claims abstract description 15
- 239000000243 solution Substances 0.000 claims abstract description 59
- 238000002347 injection Methods 0.000 claims abstract description 8
- 239000007924 injection Substances 0.000 claims abstract description 8
- 238000001523 electrospinning Methods 0.000 claims description 11
- 238000007664 blowing Methods 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 3
- 229920002521 macromolecule Polymers 0.000 abstract description 14
- 230000002045 lasting effect Effects 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 4
- 238000009987 spinning Methods 0.000 description 10
- 239000000835 fiber Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 4
- 229920001872 Spider silk Polymers 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003658 microfiber Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Images
Landscapes
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Nonwoven Fabrics (AREA)
Abstract
The utility model relates to a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing belongs to bubble electrostatic spinning field. This bubble electrostatic spinning device of orderly control nanofiber molecule sequencing includes the shower nozzle device, injection apparatus, air pump device, receiving arrangement and high-voltage electrostatic device, and the shower nozzle device includes the air duct and sets up the solution conveyer pipe in the air duct both sides, injection apparatus and solution duct connection, and the air pump device is connected with the air duct, and high-voltage electrostatic device is connected with shower nozzle device and receiving arrangement respectively, and the height that highly is less than the solution conveyer pipe of air duct, and 10cm is no less than to the height of solution conveyer pipe. The utility model relates to a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing passes through the transportation of the length and the fineness control macromolecule of shower nozzle device, and through lasting laminar flow in the long journey make the macromolecule orderly, the orientation of control nanofiber mesomolecule has improved fibrous crystallinity to optimize each item performance of material.
Description
Technical Field
The utility model relates to a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing belongs to bubble electrostatic spinning field.
Background
The nano-fiber is rapidly developed in the fields of textile engineering, tissue engineering, filtration, photoelectric devices, sensors and the like. The electrostatic spinning technology is the most common and simple method for producing the nano-fibers with low cost and high efficiency, is simple to operate and is widely applied to various fields. Bubble electrostatic spinning is a novel electrostatic spinning method proposed in recent years, and gas is introduced into spinning solution to form bubbles, the bubbles are equivalent to Taylor cones in electrostatic spinning, and the bubbles are gradually stretched and broken under the action of electric field force or airflow to form countless jet flows, and finally micro-nano fibers are formed. The bubble electrostatic spinning can effectively improve the spinning efficiency.
Compared with natural fibers such as spider silk, the artificially synthesized fibers have poorer performance. Many natural fibers such as spider silk or silk have good hierarchical structures, and micro/nano fiber molecular structures generated by electrostatic spinning or bubble spinning do not have folding symmetry and do not have the hierarchical structures of the natural fibers. Artificially synthesized fibers having a nano-scale hierarchical structure can exhibit many excellent characteristics of materials, which cannot be realized by a non-hierarchical structure. In order to improve mechanical properties, electronic properties, chemical properties, and the like of nanofibers, it is very important to improve the molecular orientation of nanofibers. Molecular motion during spinning or molecular orientation in nanofibers remains a problem to be studied. To date, it has been almost impossible to control the orientation of the molecules during spinning. If the spinning process can be controlled on a macro-molecular scale to improve the crystallinity, the method has important significance for controlling the fiber form and adjusting the mechanical, electronic and chemical properties of the fiber.
In view of the above problems, it is necessary to provide a device for controlling the order of macromolecules in nanofibers during spinning.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a can be to the bubble electrostatic spinning device of the orderly control's of macromolecule orderly control nanofiber molecule sequencing among the spinning process nanofiber.
In order to achieve the above purpose, the utility model provides a following technical scheme: the utility model provides a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing includes shower nozzle device, injection apparatus, air pump device, receiving arrangement and high-voltage electrostatic device, the shower nozzle device includes the air duct and sets up the solution conveyer pipe of air duct both sides, the injection apparatus with solution duct connections, the air pump device with the air duct is connected, high-voltage electrostatic device respectively with the shower nozzle device reaches receiving arrangement connects, the height of air duct is less than the height of solution conveyer pipe, 10cm are no less than to the height of solution conveyer pipe.
Furthermore, the bubble electrostatic spinning device for orderly controlling the sequencing of the nanofiber molecules comprises an extension part arranged on the outer side of the solution conveying pipe, air guide channels are arranged in the extension part and are axially symmetrically arranged by taking the axis of the air guide pipe as an axis, the intersection points of the extension lines of the air guide channels on the two sides are positioned on the axis of the air guide pipe, an air inlet and an air outlet are defined in the air guide channels, and the air outlet faces the solution conveying pipe.
Further, the bubble electrostatic spinning device for orderly controlling the order of the nanofiber molecules further comprises a blowing device, and the blowing device is communicated with the air inlet.
Further, the inner parts of the air guide pipe and the solution conveying pipe are circular.
Furthermore, the air duct and the inside of solution transport pipe are the rectangle, the air duct with the rectangle minor face of solution transport pipe all is less than 3 mm.
Further, the rectangular short side of the air duct is 2mm and the rectangular short side of the solution conveying pipe is 1 mm.
Further, the positive pole of the high-voltage electrostatic device is connected with the solution conveying pipe, and the negative pole of the high-voltage electrostatic device is connected with the receiving device.
Further, the solution conveying pipes are metal pipes, the number of the solution conveying pipes is 2, and the height of each solution conveying pipe is 15 cm.
Further, the receiving device is a roller type receiving device or a flat plate type receiving device.
Further, the outer walls of the air guide pipe and the solution conveying pipe are rectangular.
The beneficial effects of the utility model reside in that: the utility model relates to a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing passes through the transportation of the length and the fineness control macromolecule of shower nozzle device, and through lasting laminar flow in the long journey make the macromolecule orderly, the orientation of control nanofiber mesomolecule has improved fibrous crystallinity to optimize each item performance of material.
The above description is only an overview of the technical solution of the present invention, and in order to make the technical means of the present invention clearer and can be implemented according to the content of the description, the following detailed description is made with reference to the preferred embodiments of the present invention and accompanying drawings.
Drawings
Fig. 1 is a schematic structural diagram of the bubble electrostatic spinning device for orderly controlling the order of nanofiber molecules.
Detailed Description
The following detailed description of the embodiments of the present invention is provided with reference to the accompanying drawings and examples. The following examples are intended to illustrate the invention, but are not intended to limit the scope of the invention.
Referring to fig. 1, in the utility model relates to an in order bubble electrostatic spinning device of control nanofiber molecule sequencing in preferred embodiment includes shower nozzle device 1, injection apparatus 2, air pump device 3, receiving arrangement 4 and high-voltage electrostatic device 5, shower nozzle device 1 includes air duct 11 and the solution conveyer pipe 12 of setting in air duct 11 both sides, injection apparatus 2 is connected with solution conveyer pipe 12, air pump device 3 is connected with air duct 11, high-voltage electrostatic device is connected with shower nozzle device 1 and receiving arrangement 4 respectively, air duct 11 highly is less than the height of solution conveyer pipe 12, 10cm are not less than to the height of solution conveyer pipe 12, at the in-process of actual implementation, the height of solution conveyer pipe 12 is 15 cm.
In the above embodiment, the bubble electrospinning device for orderly controlling the order of the nanofiber molecules comprises an extension portion 6 arranged outside the solution conveying pipe 12, the extension portion 6 is internally provided with air guide channels 61 which are arranged in an axisymmetric manner by taking the axis of the air guide pipe 11 as an axis, the intersection point of the extension lines of the air guide channels 61 at the two sides is on the axis of the air guide pipe 11, the air guide channels 61 are defined with an air inlet 611 and an air outlet 612, the air outlet 612 faces the solution conveying pipe, and the bubble electrospinning device for orderly controlling the order of the nanofiber molecules further comprises a blowing device (not shown), and the blowing device is communicated with the air inlet 611.
In the above embodiment, the inside of the air duct 11 and the solution conveying pipe 12 is rectangular. Indeed, in other embodiments, the inside of the air duct 11 and the solution transportation pipe 12 may be circular, the short rectangular sides of the air duct 11 and the solution transportation pipe 12 are smaller than 3mm, in practical implementation, the short rectangular side of the air duct 11 is 2mm, the short rectangular side of the solution transportation pipe 12 is 1mm, and the outer walls of the air duct 11 and the solution transportation pipe 12 are rectangular
In the above embodiment, the positive electrode of the high-voltage electrostatic device 5 is connected to the solution delivery pipe 12, the positive electrode of the high-voltage electrostatic device 5 is connected to the receiving device 4, the solution delivery pipe 12 is a metal pipe, and the number of the solution delivery pipes 12 is 2.
In the above embodiment, the receiving device 4 is a drum receiving device or a flat receiving device.
In specific use, the utility model discloses a control shower nozzle device 1's length and internal diameter come the transportation of control macromolecule, the solution transport pipe 12 in the shower nozzle device's length is very long and extremely thin narrow, the transportation of solution in the shower nozzle device is elongated, the molecule moving speed that is close to the pipe wall in solution transport pipe 12 is less than the molecule motion of pipe center department, macromolecule 8's moving speed is crescent (the velocity distribution 9 of molecule in the pipe) from pipe wall to pipe center, macromolecule 8 inside has formed the lasting laminar flow of long range in solution transport pipe 12, the difference in speed in the pipe makes the molecule straighten gradually, thereby become orderly, macromolecule 8 is in bubble 7 along the vertical orderly range of bubble in bubble 7, make the nanofiber that forms in order, the orientation of molecule in the effectual control nanofiber.
After the spinning solution is pumped into the solution delivery pipe 12, the spinning solution flows along the slit to the nozzle of the nozzle device 1. During the flowing process, the speed of the slit is maximum in the middle, and the speed of the slit is zero on the inner wall of the solution conveying pipe 12 and the outer wall of the air duct 11. The macromolecules flow through the slots and become more and more ordered. When a bubble is formed at the nozzle port, the macromolecules 8 at the bottom of the bubble 7 are ordered.
The beneficial effects of the utility model reside in that: the utility model relates to a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing passes through the length and the fineness control macromolecule 8's of shower nozzle device 1 transportation, and through lasting laminar flow in the long journey make the macromolecule orderly, the orientation of molecule in the control nanofiber has improved fibrous crystallinity to optimize each item performance of material.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only represent some embodiments of the present invention, and the description thereof is specific and detailed, but not to be construed as limiting the scope of the present invention. It should be noted that, for those skilled in the art, without departing from the spirit of the present invention, several variations and modifications can be made, which are within the scope of the present invention. Therefore, the protection scope of the present invention should be subject to the appended claims.
Claims (10)
1. The utility model provides a bubble electrostatic spinning device of orderly control nanofiber molecule sequencing which characterized in that: the bubble electrostatic spinning device for orderly controlling the sequencing of nanofiber molecules comprises a sprayer device, an injection device, an air pump device, a receiving device and a high-voltage electrostatic device, wherein the sprayer device comprises an air guide pipe and solution conveying pipes arranged on two sides of the air guide pipe, the injection device is connected with the solution conveying pipes, the air pump device is connected with the air guide pipe, the high-voltage electrostatic device is respectively connected with the sprayer device and the receiving device, the height of the air guide pipe is lower than that of the solution conveying pipes, and the height of the solution conveying pipes is not less than 10 cm.
2. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the bubble electrostatic spinning device for orderly controlling the sequencing of the nanofiber molecules comprises an extension part arranged on the outer side of a solution conveying pipe, air guide channels are arranged in the extension part and are arranged by taking the axis of the air guide pipe as axial symmetry, the intersection points of the extension lines of the air guide channels on the two sides are positioned on the axis of the air guide pipe, the air guide channels are defined with an air inlet and an air outlet, and the air outlet faces towards the solution conveying pipe.
3. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 2, wherein: the bubble electrostatic spinning device for orderly controlling the order of the nanofiber molecules further comprises a blowing device, and the blowing device is communicated with the air inlet.
4. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the air duct and the solution delivery pipe are circular.
5. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the air duct with the inside of solution conveyer pipe is the rectangle, the air duct with the rectangle minor face of solution conveyer pipe all is less than 3 mm.
6. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 5, wherein: the rectangular short side of the air duct is 2mm, and the rectangular short side of the solution conveying pipe is 1 mm.
7. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the positive pole of the high-voltage electrostatic device is connected with the solution conveying pipe, and the negative pole of the high-voltage electrostatic device is connected with the receiving device.
8. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the solution conveying pipe is a metal pipe, the number of the solution conveying pipes is 2, and the height of each solution conveying pipe is 15 cm.
9. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the receiving device is a roller type receiving device or a flat plate type receiving device.
10. The bubble electrospinning apparatus of order controlled nanofiber molecular ordering of claim 1, wherein: the outer walls of the air duct and the solution conveying pipe are rectangular.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920479759.0U CN210085632U (en) | 2019-04-10 | 2019-04-10 | Bubble electrostatic spinning device for orderly controlling nano fiber molecule sequencing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920479759.0U CN210085632U (en) | 2019-04-10 | 2019-04-10 | Bubble electrostatic spinning device for orderly controlling nano fiber molecule sequencing |
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| Publication Number | Publication Date |
|---|---|
| CN210085632U true CN210085632U (en) | 2020-02-18 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201920479759.0U Expired - Fee Related CN210085632U (en) | 2019-04-10 | 2019-04-10 | Bubble electrostatic spinning device for orderly controlling nano fiber molecule sequencing |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055599A (en) * | 2019-04-10 | 2019-07-26 | 苏州大学 | A kind of device for spinning and method of orderly control nanofiber molecular order |
-
2019
- 2019-04-10 CN CN201920479759.0U patent/CN210085632U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055599A (en) * | 2019-04-10 | 2019-07-26 | 苏州大学 | A kind of device for spinning and method of orderly control nanofiber molecular order |
| CN110055599B (en) * | 2019-04-10 | 2024-04-19 | 苏州大学 | Spinning device and method for orderly controlling molecular ordering of nanofibers |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200218 |