CN209952826U - A reation kettle for isophthalic acid-5-sodium sulfonate production - Google Patents
A reation kettle for isophthalic acid-5-sodium sulfonate production Download PDFInfo
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- CN209952826U CN209952826U CN201920052469.8U CN201920052469U CN209952826U CN 209952826 U CN209952826 U CN 209952826U CN 201920052469 U CN201920052469 U CN 201920052469U CN 209952826 U CN209952826 U CN 209952826U
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- barrel
- liquid outlet
- mixing
- shaft
- production
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses a reation kettle for isophthalic acid-5-sodium sulfonate production, including the barrel, the barrel is equipped with the cover, is equipped with rotating electrical machines and feed inlet on the cover, is equipped with the (mixing) shaft in the barrel, is equipped with dispersion impeller, stirring vane on the (mixing) shaft, is equipped with the baffling board in the barrel, and the barrel has the bin outlet, is equipped with the washing shower nozzle in the barrel, and the washing shower nozzle passes through the scavenging pump and connects the washing pond, and the barrel bottom is equipped with liquid outlet I, liquid outlet II, and liquid outlet I passes through the circulating pump and connects the washing pond, and liquid outlet II connects the waste liquor pond. The utility model discloses simple structure, reasonable in design has good corrosion resisting property, extension equipment life. The stirring and mixing effect is good, and the production efficiency is improved. The cleaning liquid can be recycled, so that the material is effectively saved, and the production cost is reduced.
Description
Technical Field
The utility model relates to a chemical production technical field especially relates to a reation kettle for m-phthalic acid-5-sodium sulfonate production.
Background
The reaction kettle is a container for physical or chemical reaction, realizes the heating, evaporation, cooling and low-speed and high-speed mixing functions required by the process through the structural design and parameter configuration of the container, is widely applied to petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, is a pressure container for completing the processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, and needs to be used as the reaction container in the production process of the p-dichlorobenzene.
The production of 5-sodium sulfoisophthalate has large corrosion to the reaction kettle, and the reaction kettle needs to be cleaned in time. The existing reaction kettle generally needs manual cleaning, has poor cleaning effect and low working efficiency, and the cleaning agent has great toxicity to human bodies.
SUMMERY OF THE UTILITY MODEL
In order to solve the defects, the utility model aims to provide a reaction kettle for producing sodium 5-sulfoisophthalate, which has reasonable design and high stirring efficiency of cleaning efficiency.
In order to achieve the above object, the utility model discloses a following technical scheme realizes: a reation kettle for m-phthalic acid-5-sodium sulfonate production, its characterized in that: the improved stirring barrel comprises a barrel body, the barrel top is equipped with the cover, the cover upside is equipped with rotating electrical machines and feed inlet, be equipped with the (mixing) shaft in the barrel, rotating electrical machines passes through the coupling joint with the (mixing) shaft, (mixing) shaft upper portion is equipped with the dispersion impeller, the (mixing) shaft lower part is equipped with a plurality of stirring vane, be equipped with the baffling board on the barrel inner wall, the barrel downside is equipped with the bin outlet, be equipped with the relief valve on the bin outlet, the inside top of barrel is equipped with the washing shower nozzle, the washing shower nozzle passes through the scavenging pump and connects the washing pond, the barrel bottom is equipped with liquid outlet I, liquid outlet II, be equipped with out the liquid valve on liquid outlet I, the liquid outlet II, liquid outlet II is connected the washing pond.
Preferably, a plurality of material guide holes are uniformly formed in the dispersion disc, and the diameter of each material guide hole is larger than that of the material.
Preferably, the inner side of the cylinder, the stirring shaft, the dispersion disc, the stirring blades and the baffle plate are all made of stainless steel materials, and the surface of the cylinder is provided with an anticorrosive coating.
Preferably, the surface of the cylinder body is provided with a viewing port.
The utility model has the advantages that: simple structure, reasonable in design has good corrosion resistance, has prolonged equipment life. The stirring and mixing of the reactants are faster and more uniform, and the production efficiency is improved. The cleaning liquid can be directly recycled, so that the material is effectively saved, and the production cost is reduced. The utility model discloses a reation kettle is a fine innovation scheme, has very much the marketing prospect.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Wherein: 1. barrel, 2, cover, 3, rotating electrical machines, 4, feed inlet, 5, (mixing) shaft, 6, shaft coupling, 7, dispersion impeller, 8, stirring vane, 9, baffling board, 10, bin outlet, 11, relief valve, 12, washing shower nozzle, 13, scavenging pump, 14, washing pond, 15, liquid outlet I, 16, liquid outlet II, 17, play liquid valve, 18, circulating pump, 19, viewing aperture, 20, zone of heating, 21, heat preservation.
Detailed Description
The following describes embodiments of the present invention with reference to the drawings.
As shown in figure 1, the reaction kettle for producing 5-sodium sulfoisophthalate comprises a barrel 1, a barrel cover 2 is arranged at the top end of the barrel 1, a rotating motor 3 and a feed inlet 4 are arranged on the upper side of the barrel cover 2, a stirring shaft 5 is arranged in the barrel 1, the rotating motor 3 is connected with the stirring shaft 5 through a coupling 6, a dispersion disc 7 is arranged on the upper portion of the stirring shaft 5, a plurality of stirring blades 8 are arranged on the lower portion of the stirring shaft 5, a baffle plate 9 is arranged on the inner wall of the barrel 1, a discharge hole 10 is arranged on the lower side of the barrel 1, a discharge valve 11 is arranged on the discharge hole 10, a cleaning nozzle 12 is arranged at the top end in the barrel 1, the cleaning nozzle 12 is connected with a cleaning pool 14 through a cleaning pump 13, a liquid outlet I15 and a liquid outlet II 16 are arranged at the bottom of the barrel 1, a liquid, a heating layer 20 is arranged outside the wall of the barrel body 1, and a heat preservation layer 21 is arranged outside the heating layer 20.
A plurality of material guide holes are uniformly arranged on the dispersion plate 7, and the diameter of each material guide hole is larger than that of the material. The inner side of the cylinder 1, the stirring shaft 5, the dispersion disc 7, the stirring blades 8 and the baffle plate 9 are all made of stainless steel materials, and the surfaces of the dispersion disc and the baffle plate are provided with anticorrosive layers. The surface of the cylinder 1 is provided with a viewing port 19.
The utility model discloses simple structure, reasonable in design has good corrosion resisting property, has prolonged equipment life. Dispersion impeller, stirring vane carry out dual stirring to the reactant, and the stirring mixes the effect better, improves production efficiency. The cleaning liquid can be directly recycled, so that the material is effectively saved, and the production cost is reduced.
Claims (4)
1. A reation kettle for m-phthalic acid-5-sodium sulfonate production, its characterized in that: the improved stirring barrel comprises a barrel body, the barrel top is equipped with the cover, the cover upside is equipped with rotating electrical machines and feed inlet, be equipped with the (mixing) shaft in the barrel, rotating electrical machines passes through the coupling joint with the (mixing) shaft, (mixing) shaft upper portion is equipped with the dispersion impeller, the (mixing) shaft lower part is equipped with a plurality of stirring vane, be equipped with the baffling board on the barrel inner wall, the barrel downside is equipped with the bin outlet, be equipped with the relief valve on the bin outlet, the inside top of barrel is equipped with the washing shower nozzle, the washing shower nozzle passes through the scavenging pump and connects the washing pond, the barrel bottom is equipped with liquid outlet I, liquid outlet II, be equipped with out the liquid valve on liquid outlet I, the liquid outlet II, liquid outlet II is connected the washing pond.
2. The reactor for the production of sodium 5-sulfoisophthalate according to claim 1, wherein: a plurality of material guide holes are uniformly formed in the dispersion disc, and the diameter of each material guide hole is larger than that of the material.
3. The reactor for the production of sodium 5-sulfoisophthalate according to claim 1, wherein: the inner side of the cylinder body, the stirring shaft, the dispersion disc, the stirring blades and the baffle plate are all made of stainless steel materials, and the surface of the cylinder body is provided with an anticorrosive coating.
4. The reactor for the production of sodium 5-sulfoisophthalate according to claim 1, wherein: the surface of the cylinder body is provided with an observation port.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920052469.8U CN209952826U (en) | 2019-01-14 | 2019-01-14 | A reation kettle for isophthalic acid-5-sodium sulfonate production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920052469.8U CN209952826U (en) | 2019-01-14 | 2019-01-14 | A reation kettle for isophthalic acid-5-sodium sulfonate production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209952826U true CN209952826U (en) | 2020-01-17 |
Family
ID=69236409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920052469.8U Expired - Fee Related CN209952826U (en) | 2019-01-14 | 2019-01-14 | A reation kettle for isophthalic acid-5-sodium sulfonate production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209952826U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111495310A (en) * | 2020-06-17 | 2020-08-07 | 烟台工程职业技术学院(烟台市技师学院) | Automatic easy abluent food stirring reation kettle of changing |
| CN115591512A (en) * | 2022-12-15 | 2023-01-13 | 联仕（昆山）化学材料有限公司（Cn） | Mixing arrangement in nitrogen methyl pyrrolidone preparation process |
| CN117101172A (en) * | 2023-10-24 | 2023-11-24 | 福建省龙德新能源有限公司 | Sodium hexafluorophosphate crystallization equipment and crystallization process thereof |
-
2019
- 2019-01-14 CN CN201920052469.8U patent/CN209952826U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111495310A (en) * | 2020-06-17 | 2020-08-07 | 烟台工程职业技术学院(烟台市技师学院) | Automatic easy abluent food stirring reation kettle of changing |
| CN115591512A (en) * | 2022-12-15 | 2023-01-13 | 联仕（昆山）化学材料有限公司（Cn） | Mixing arrangement in nitrogen methyl pyrrolidone preparation process |
| CN117101172A (en) * | 2023-10-24 | 2023-11-24 | 福建省龙德新能源有限公司 | Sodium hexafluorophosphate crystallization equipment and crystallization process thereof |
| CN117101172B (en) * | 2023-10-24 | 2023-12-22 | 福建省龙德新能源有限公司 | Sodium hexafluorophosphate crystallization equipment and crystallization process thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200117 |
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| CF01 | Termination of patent right due to non-payment of annual fee |