CN209771565U

CN209771565U - Organic reagent separator

Info

Publication number: CN209771565U
Application number: CN201920442018.5U
Authority: CN
Inventors: 于万枝; 姬茹一; 任飞
Original assignee: Bosen Zhongmei (tianjin) Chemical Technology Co Ltd
Current assignee: Bosen Zhongmei (tianjin) Chemical Technology Co Ltd
Priority date: 2019-04-03
Filing date: 2019-04-03
Publication date: 2019-12-13
Anticipated expiration: 2029-04-03

Abstract

the utility model discloses an organic reagent separator, including the processing box, processing box up end is opened there is the opening, the spiral-lock has sealed lid on the opening, sealed lid lower extreme is provided with the sealing plug, the relative both sides of sealed lid are provided with the connecting block respectively, the round pin hub connection has the swinging arms on the connecting block, be provided with the round pin pole on the swinging arms, the open-ended both sides be provided with the corresponding fixed block in connecting block position, the processing box internal bottom surface is provided with the receiving flask, the distillation tube pass the condenser pipe with the receiving flask communicates mutually, sealed epaxial central point of covering puts and opens threaded hole, the threaded hole interpolation is equipped with and twists the threaded rod soon, it is provided with the rolling disc to twist threaded rod upper end soon, it is provided with the laminating to twist the threaded rod lower. The utility model discloses can separate the reagent liquid of doping impurity, reject impurity, use once more, prevent that reagent from abandoning.

Description

Organic reagent separator

Technical Field

The utility model belongs to the technical field of a reagent processing technique and specifically relates to an organic reagent separator is related to.

Background

Chemical reagents are relatively standard substances for chemical research and component analysis, are important conditions for technological progress, are widely used for synthesis, separation, qualitative and quantitative analysis of substances, can be said to be eyes of chemical workers, and can not be separated from the chemical reagents in daily work of factories, schools, hospitals and research institutes, the chemical reagents are widely applied to various industries of industry, agriculture, medical health, life science, inspection and quarantine, environmental protection, energy development, national defense and military industry, scientific research and national economy, the utilization rate is very high, but dust is doped in liquid sometimes, and the reagents doped with dust are rejected due to unqualified cleaning, so that improvement is very inconvenient.

SUMMERY OF THE UTILITY MODEL

The to-be-solved technical problem of the utility model is to overcome current defect, provide a new organic reagent separator to solve above-mentioned problem.

In order to achieve the above object, the utility model provides a following technical scheme: an organic reagent separating device comprises a processing box body, wherein an opening is formed in the upper end face of the processing box body, a sealing cover is buckled on the opening, a sealing plug is arranged at the lower end of the sealing cover, connecting blocks are respectively arranged on two opposite sides of the sealing cover, a swinging rod is connected to the connecting blocks through a pin shaft, a pin rod is arranged on the swinging rod, fixed blocks corresponding to the connecting blocks are arranged on two sides of the opening, pin grooves meshed with the pin rods are formed in the fixed blocks, a filtering and separating barrel is arranged in the processing box body and communicated with the opening, a conical filtering screen plate is arranged inside the filtering and separating barrel, a heating electromagnetic oven is arranged on the inner bottom face of the processing box body, a distillation heating bottle is arranged on the heating electromagnetic oven, and a communicating pipe is connected between the distillation heating bottle and the filtering and separating barrel, the distillation heating bottle with be provided with the iron piece between the heating electromagnetism stove, distillation heating bottle upper end is provided with the distillation tube, the upper surface is provided with the gallows in the processing box, be provided with the suit ring on the gallows, the suit intra-annular is inlayed and is equipped with the condenser pipe, the bottom surface is provided with the receiving flask in the processing box, the distillation tube pass the condenser pipe with the receiving flask communicates mutually, the central point on the sealed lid puts and opens threaded hole, threaded hole interpolation is equipped with revolves the threaded rod, it is provided with the rolling disc to revolve the threaded rod upper end of revolving, it is provided with the laminating to revolve the threaded rod lower extreme.

preferably, a conical one-way diversion valve is arranged in the communicating pipe, and the tip of the one-way diversion valve is located at one end of the distillation heating bottle downwards.

Preferably, a taking-out port is formed in the side surface of the processing box body, and the height of the taking-out port is matched with that of the collecting bottle.

Preferably, the outer contour of the sealing plug is attached to the side surface of the filtering separation barrel to realize sealing.

Preferably, the condensation pipe adopts a refrigeration pipe for water circulation refrigeration.

Compared with the prior art, the beneficial effects of the utility model are that: can separate the reagent liquid of doping impurity, reject impurity, use once more, prevent that reagent from abandoning.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:

FIG. 1 is a schematic view of a structure of an organic reagent separating apparatus;

FIG. 2 is an enlarged view of a portion of an organic reagent separating apparatus;

shown in the figure: 1. processing the box body; 2. an opening; 3. a sealing cover; 4. a sealing plug; 5. connecting blocks; 6. a swing lever; 7. a pin rod; 8. a fixed block; 9. a pin slot; 10. a filtering separation barrel; 11. a conical filter screen plate; 12. heating the induction cooker; 13. distilling and heating the bottle; 14. a communicating pipe; 15. an iron sheet; 16. a distillation tube; 17. a hanger; 18. sleeving a ring; 19. a condenser tube; 20. a collection bottle; 21. a threaded hole; 22. screwing the threaded rod; 23. rotating the disc; 24. a sealing plate; 25. a one-way diverter valve; 26. a removal port.

Detailed Description

The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by a person of ordinary skill in the art without creative work belong to the protection scope of the present invention based on the embodiments of the present invention.

Referring to fig. 1-2, the present invention provides a technical solution: an organic reagent separating device comprises a processing box body 1, wherein an opening 2 is formed in the upper end face of the processing box body 1, a sealing cover 3 is buckled on the opening 2, a sealing plug 4 is arranged at the lower end of the sealing cover 3, connecting blocks 5 are respectively arranged on two opposite sides of the sealing cover 3, a swinging rod 6 is connected to the connecting blocks 5 through a pin shaft, a pin 7 is arranged on the swinging rod 6, fixing blocks 8 corresponding to the connecting blocks 5 are arranged on two sides of the opening 2, pin grooves 9 meshed with the pin 7 are formed in the fixing blocks 8, a filtering and separating barrel 10 is arranged in the processing box body 1 and communicated with the opening 2, a conical filtering screen plate 11 is arranged in the filtering and separating barrel 10 in a semicircular mode, a heating electromagnetic oven 12 is arranged on the inner bottom face of the processing box body 1, and a distillation heating bottle 13 is arranged on the heating electromagnetic oven 12, distillation heating bottle 13 with be connected with communicating pipe 14 between filtering separation bucket 10, distillation heating bottle 13 with be provided with iron piece 15 between the heating electromagnetism stove 12, distillation heating bottle 13 upper end is provided with distillation tube 16, the upper surface is provided with gallows 17 in the processing box 1, be provided with suit ring 18 on the gallows 17, the embedded condenser pipe 19 that is equipped with of suit ring 18, the bottom is provided with receiving flask 20 in the processing box 1, distillation tube 16 pass the condenser pipe 19 with receiving flask 20 is linked together, central point on the sealed lid 3 puts and opens threaded hole 21, threaded hole 21 interpolation is equipped with revolves wrong threaded rod 22, it is provided with rolling disc 23 to revolve wrong threaded rod 22 upper end, it is provided with the laminating to revolve wrong threaded rod 22 lower extreme filtering separation bucket 10 inner wall's closing plate 24.

In this embodiment, a tapered one-way diversion valve 25 is disposed in the communication pipe 14, a tip of the one-way diversion valve 25 is located at one end of the distillation heating bottle 13 downward, a take-out port 26 is formed in a side surface of the processing box 1, a height of the take-out port 26 matches a height of the collecting bottle 20, an outer contour of the sealing plug 4 is attached to a side surface of the filtration separation barrel 10 to realize sealing, and the condensation pipe 19 is a refrigeration pipe for water circulation refrigeration.

When in specific use: the swing rod 6 is broken off, the pin rod 7 is separated from the constraint of the pin groove 9, the sealing cover 3 is removed, the liquid reagent doped with impurities is injected into the filtering and separating barrel 10, at the moment, the liquid reagent is filtered by the conical filtering screen plate 11 and flows into the communicating pipe 14, blocked by the one-way diversion valve 25, the sealing cover 3 is buckled at the moment, the rotating disc 23 is screwed after the sealing plug 4 is used for sealing, by gradually moving downward by screwing the threaded rod 22, the sealing plate 24 is pushed to squeeze the liquid in the filtering and separating tub 10, so that the liquid enters the distillation heating bottle 13 through the one-way diversion valve 25, the heating electromagnetic oven 12 is opened, the temperature of the distillation heating bottle 13 is increased after the iron sheet 15 heats, the generated steam can only enter the distillation pipe 16 through the obstruction of the one-way diversion valve 25, the refrigeration through the condenser tube 19 causes the vapor to condense and fall into the collection bottle 20, and the collection bottle 20 is finally removed from the outlet 26.

Finally, it should be further noted that the above examples and descriptions are not limited to the above embodiments, and technical features of the present invention that are not described may be implemented by or using the prior art, and are not described herein again; the above embodiments and drawings are only for illustrating the technical solutions of the present invention and not for limiting the present invention, and the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that changes, modifications, additions or substitutions within the spirit and scope of the present invention may be made by those skilled in the art without departing from the spirit of the present invention, and the present invention should also fall within the scope of the claims of the present invention, and the above embodiments are only given as an arbitrary example of one currently used embodiment.

Claims

1. An organic reagent separating device comprises a processing box body (1) and is characterized in that an opening (2) is formed in the upper end face of the processing box body (1), a sealing cover (3) is buckled on the opening (2), a sealing plug (4) is arranged at the lower end of the sealing cover (3), connecting blocks (5) are arranged on two opposite sides of the sealing cover (3) respectively, a swing rod (6) is connected to the connecting blocks (5) through a pin shaft, a pin rod (7) is arranged on the swing rod (6), fixing blocks (8) corresponding to the connecting blocks (5) in position are arranged on two sides of the opening (2), pin grooves (9) meshed with the pin rod (7) are formed in the fixing blocks (8), a filtering and separating barrel (10) is communicated with the opening (2) in the processing box body (1), the inner bottom face of the filtering and a conical filtering screen plate (11) is arranged in the filtering and separating barrel (10), the processing box body (1) is internally provided with a heating electromagnetic oven (12) on the bottom surface, a distillation heating bottle (13) is arranged on the heating electromagnetic oven (12), a communicating pipe (14) is connected between the distillation heating bottle (13) and the filtering separation barrel (10), an iron sheet (15) is arranged between the distillation heating bottle (13) and the heating electromagnetic oven (12), a distillation pipe (16) is arranged at the upper end of the distillation heating bottle (13), a hanging bracket (17) is arranged on the inner upper surface of the processing box body (1), a sleeving ring (18) is arranged on the hanging bracket (17), a condensation pipe (19) is embedded in the sleeving ring (18), a collecting bottle (20) is arranged on the inner bottom surface of the processing box body (1), the distillation pipe (16) penetrates through the condensation pipe (19) to be communicated with the collecting bottle (20), and a threaded hole (21) is formed in the center position of the sealing cover (3), a screwing threaded rod (22) is inserted into the threaded hole (21), a rotating disc (23) is arranged at the upper end of the screwing threaded rod (22), and a sealing plate (24) attached to the inner wall of the filtering and separating barrel (10) is arranged at the lower end of the screwing threaded rod (22).

2. The organic reagent separating device as claimed in claim 1, wherein a tapered one-way diverter valve (25) is disposed in the communicating tube (14), and a tip of the one-way diverter valve (25) is located at one end of the retort heating bottle (13) downward.

3. An organic reagent separating device as claimed in claim 1, wherein a take-out port (26) is formed in a side surface of the processing box (1), and a height of the take-out port (26) is matched with a height of the collecting bottle (20).

4. An organic reagent separating device according to claim 1, characterized in that the outer contour of the sealing plug (4) fits against the side surface of the filter separating barrel (10) to achieve sealing.

5. The organic reagent separating device as claimed in claim 1, wherein the condensing pipe (19) is a refrigerating pipe for refrigerating by water circulation.