CN209696953U - Gas experiment multi-purpose device with anti-suck, explosion prevention function - Google Patents
Gas experiment multi-purpose device with anti-suck, explosion prevention function Download PDFInfo
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- CN209696953U CN209696953U CN201920280169.5U CN201920280169U CN209696953U CN 209696953 U CN209696953 U CN 209696953U CN 201920280169 U CN201920280169 U CN 201920280169U CN 209696953 U CN209696953 U CN 209696953U
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Abstract
The utility model discloses a kind of gas experiment multi-purpose device with anti-suck, explosion prevention function, including conical flask and explosion-proof suck-back device;Conical flask is furnished with biforate rubber stopper, and explosion-proof suck-back device is made of air guide glass inner tube, outer glass tube, the first single hole rubber plug, the second single hole rubber plug and implosion guard inner tube;Outer glass tube one end is equipped with the first single hole rubber plug, and the other end is equipped with the second single hole rubber plug;Air guide glass inner tube one end inserts in conical flask through biforate rubber stopper, and the other end inserts in outer glass tube through the first single hole rubber plug, and the end port is special at pore, and blocks strip latex thin skin;Implosion guard inner tube is sharp nozzle canula, its sharp nozzle end connect with gas collector through plastic straw or connect through the second plastic flexible pipe with two-way glass point mouth, the other end inserts in outer glass tube through the second single hole rubber plug, tightly packed explosion-proof wire mesh column in implosion guard inner tube.Another hole is inserted with the two-way sharp mouth bend pipe in the right angle connecting with syringe or gas generating unit on biforate rubber stopper.
Description
Technical field
The utility model belongs to chemical experiment device field, is related to a kind of gas experiment with anti-suck, explosion prevention function
Multi-purpose device.
Background technique
Suck-back phenomenon is frequent a kind of bad phenomenon in chemical experiment.Because of experiment content difference, occur in experiment
Suck-back will lead to interrupt experiments or the failure of an experiment needs are reformed.In addition, being frequently necessary to produce some combustibility in chemical experiment
Gas, such as hydrogen, methane, ethylene and acetylene, but after being mixed into a certain amount of air in these gases of preparation, Ke Nengfa
Raw explosion, causes safety accident, causes the injury to experimenter, and influence experiment effect.Therefore, it is necessary to one kind with anti-down
It inhales, the gas experiment device of explosion prevention function, to solve the above problems.
Summary of the invention
In order to achieve the above object, it is multi-purpose to provide a kind of gas experiment with anti-suck, explosion prevention function for the utility model
Device solves the problems, such as that generation suck-back leads to experiment interruption in chemical experiment or the failure of an experiment needs to re-start and combustibility
The problem of being easy to happen explosion in gas preparation experiment.
In order to solve the above technical problems, the utility model is the technical scheme adopted is that with anti-suck, explosion prevention function
Gas experiment multi-purpose device, including conical flask and explosion-proof suck-back device;Conical flask is furnished with biforate rubber stopper, a hole on biforate rubber stopper
It is inserted with the two-way sharp mouth bend pipe in right angle, another hole is connect with explosion-proof suck-back device one end, and the two-way sharp mouth bend pipe other end in right angle is logical
The first plastic flexible pipe is crossed to connect with syringe or gas with various generating device;The explosion-proof suck-back device other end passes through plastic straw
It connect with gas with various collection device or is connect by the second plastic flexible pipe with two-way glass point mouth;
The explosion-proof suck-back device by air guide glass inner tube, outer glass tube, the first single hole rubber plug, the second single hole rubber plug and
Implosion guard inner tube composition;Caliber is 15mm in outer glass tube, is equipped with the first single hole rubber plug, the other end close to conical flask one end
Equipped with the second single hole rubber plug;Air guide glass inner tube one end inserts in conical flask through biforate rubber stopper, and the other end is through the first single hole rubber plug
It inserts in outer glass tube;Air guide glass inner tube outer tube diameter is 7~8mm, interior caliber is 5 ~ 6mm, and air guide glass inner tube inserts in glass
The port of one end is blocked in outer tube tightens and strip latex thin skin in the raw through copper wire, strip latex thin skin length
It is equal sized for 50mm, width and air guide glass inner tube outer tube diameter;Air guide glass inner tube inserts in the port of one end in outer glass tube
For the gas vent for being fused necking, polishing is formed, gas vent aperture is 3mm;Implosion guard inner tube is sharp nozzle canula, sharp nozzle end
It connect or is connect through the second plastic flexible pipe with two-way glass point mouth, the inner tube of plastic straw with gas collector through plastic straw
Diameter is 1.5 ~ 2mm, and the other end inserts in outer glass tube through the second single hole rubber plug, tightly packed in the straight tube of implosion guard inner tube to have
Explosion-proof wire mesh column.
Further, the interior caliber of second plastic flexible pipe is greater than the interior caliber of plastic straw.
Further, the length of the explosion-proof wire mesh column is 3~4cm, and the diameter of wire is 0.1 ~ 0.15mm.
Further, the strip latex thin skin is with a thickness of 0.5 ~ 1mm.
Further, the biforate rubber stopper is 4# rubber plug;The first single hole rubber plug and the second single hole rubber plug are 0# glue
Plug.
Further, the outer glass tube length is 50mm;The air guide glass inner tube is outside right-angle elbow pipe, with glass
The pipe overall length of one end of pipe connection is 40mm, and the pipe overall length of the other end is 50mm.
Further, the bore of the two-way sharp mouth bend pipe in the right angle is 3 ~ 4mm;The implosion guard inner tube length is
50mm, outer diameter are 7~8mm, and the bore of sharp nozzle end is 4mm.
Further, the wire of the explosion-proof wire mesh column is derived from the copper wire in stainless steel window screening or conducting wire.
Further, the piston of the syringe is wrapped with the plastic film tightened through copper wire.
Further, the conical flask is reaction vessel, purifying vessel or drying receptacle.
The utility model has the beneficial effects that the gas experiment multi-purpose device with anti-suck, explosion prevention function, in air guide glass
One end that glass inner tube is placed in outer glass tube blocks strip latex thin skin, and as being positive pressure in conical flask, strip latex thin skin is rushed
It heaves, gas is smoothly discharged from gas vent through strip latex thin skin two sides, and as being negative pressure in conical flask, strip latex thin skin is tightly
The end for being attached to air guide glass inner tube is inhaled on ground, has blocked the reflux of gas, it is therefore prevented that the generation of liquid suck-back phenomenon both realized
The normal export of gas, and can effective anti-suck.In addition, being filled by the plastic straw and gas collection that interior caliber is 1.5 ~ 2mm
Connection is set, so that preparing, when ease of solubility gas, gas is discharged by micro- diameter of plastic straw, keeps the velocity of discharge of gas big
In its solution rate, thus will not because gas dissolve it is too fast due to generate liquid suck-back the phenomenon that, prevent secondary suck-back.Explosion-proof
Tightly packed a length of 3~4cm, the wire that diameter is 0.1 ~ 0.15mm are made with reducing temperature from two-way glass in glass inner tube
The tempering of sharp mouth conduction is extinguished or is blocked, and gas generating unit is effectively prevent to explode.And conical flask is connected through plastic flexible pipe and is injected
Device or gas with various generating device, implosion guard inner tube connects gas with various collection device through plastic straw or two-way glass is sharp
Different functions can be realized in mouth.Efficiently solving generation suck-back in chemical experiment leads to experiment interruption or the failure of an experiment needs
The problem of re-starting and imflammable gas prepare the problem of being easy to happen explosion in experiment, and provide one kind and have a variety of use
The gas experiment device on way.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor
Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is the gas experiment multi-purpose device structural schematic diagram that the utility model has anti-suck, explosion prevention function.
Fig. 2 is the strip latex thin skin schematic diagram of the utility model.
Fig. 3 is the two-way glass point mouth schematic diagram of the utility model.
In figure, 1. syringes, 2. conical flasks, 3. biforate rubber stoppers, the two-way sharp mouth bend pipe in 4. right angles, 5. first plastic flexible pipes,
6. air guide glass inner tube, 7. outer glass tubes, 8. first single hole rubber plugs, 9. second single hole rubber plugs, 10. strip latex thin skins, 11. is anti-
Quick-fried glass inner tube, 12. explosion-proof wire mesh columns, 13. gas collectors, 14. plastic straws, 15. pistons, 16. gas vents,
17. two-way glass point mouth, 18. second plastic flexible pipes.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
As shown in Figure 1 and 2, with anti-suck, explosion prevention function gas experiment multi-purpose device include syringe 1, conical flask 2,
Explosion-proof suck-back device and gas collector 13;Syringe 1 is the plastic injector that a discarded specification is 20/50ml, is used
The liquid reagent to react is added, accurately controls the addition speed and additional amount of liquid, 15 outsourcing of piston of syringe 1
It is wrapped with the super-thin plastic film tightened through thin copper wire, reagent corrosion piston is prevented and makes piston aging, improve piston life, together
When prevent reagent contaminated.Conical flask 2 is that capacity is 150ml, is furnished with biforate rubber stopper 3, biforate rubber stopper 3 is 4# rubber plug, double
A hole, which is inserted with, on hole rubber plug 3 is about 200mm(30mm+170mm), the two-way sharp mouth bend pipe 4 in the right angle of 3 ~ 4mm of bore, another hole with
The connection of 6 one end of air guide glass inner tube, it is about 20mm that the two-way sharp mouth bend pipe 4 in right angle, which is located at distance of the one end away from bottom of bottle in conical flask 2,
Specifically can be according to needing to design, two-way sharp 4 other end of mouth bend pipe in right angle is connect by the first plastic flexible pipe 5 with syringe 1;Glass
7 inner hollow of outer tube is about 50mm, and interior caliber is 15mm, is equipped with the first single hole rubber plug 8, the other end close to 2 one end of conical flask
Equipped with the second single hole rubber plug 9, the first single hole rubber plug 8 and the second single hole rubber plug 9 are 0# rubber plug;Air guide glass inner tube 6 is right angle
Bend pipe is always about 90mm(50mm+40mm), the other end inserts in outer glass tube 7 through the first single hole rubber plug 8, and air guide glass
The pipe overall length that inner tube 6 inserts in one end in outer glass tube 7 is 40mm, and the end port blocks (elastic suitable) and has in nature
The strip latex thin skin 10 of state (deformation occurs), strip latex thin skin 10 is tightened through thin copper wire or filament, in air guide glass
The port that pipe 6 inserts in one end in outer glass tube 7 is the gas vent 16 for being fused necking, polishing formation, and 16 aperture of gas vent is about
3mm prevents from inhaling broken strip latex thin skin 10 when it is negative pressure that suck-back phenomenon or conical flask 2, which occurs, always.Strip latex thin skin 10 is long
50mm, wide 8mm, 0.5 ~ 1mm of thickness, are generally derived from balloon or disposable emulsion medical gloves.The pipe of 6 other end of air guide glass inner tube
Sub- overall length is 50mm, and 6 outer tube diameter of air guide glass inner tube is 7~8mm, internal diameter is 5 ~ 6mm, and air guide glass inner tube 6 can be used common
Glass tube production, osculum need to first fuse necking to about 3mm, after cooling with 600~800# silicon carbide paper polishing port to it is smooth,
It is smooth.Implosion guard inner tube 11 is the sharp nozzle canula for being about 50mm, and overall diameter is 7~8mm, and the bore of sharp nozzle end mouth is about
4mm, sharp nozzle end mouth caliber in the plastic straw 14(of scalp acupuncture is 1.5 ~ 2mm) it is connect with gas collector 13, it is another
End is placed in outer glass tube 7 through the second single hole rubber plug 9;It is tightly packed in the straight tube of implosion guard inner tube 11 to have a length of 3~4cm's
Explosion-proof wire mesh column 12, explosion-proof 12 diameter of wire mesh column are 0.1 ~ 0.15mm, the copper being derived from stainless steel window screening or conducting wire
Silk.
The utility model with anti-suck, explosion prevention function gas experiment multi-purpose device can be used for hydrogen, carbon monoxide,
The experiment for producing or preparing gas-saturated solutions of the gases such as sulfur dioxide, hydrogen sulfide.When doing such experiment, conical flask 2 is built-in
Solid or liquid reagent, syringe 1 is used as charger, interior to be packed into another acids or other that reacted with reagent in bottle
Reagent is collected by gas derived from plastics thin 14 with drainage, is passed through in gas collector 13.Pass through plastic straw 14
Micropore deflate, can be improved the degree of scatter of gas, increase the contact area of gas and water, to improve the utilization and suction of gas
It produces effects fruit.
What the device can be used for the gases such as methane, ethylene, acetylene produces experiment.When doing such experiment, remove spare note
Emitter 1, purifying vessel of the conical flask 2 as gas are directly connected with the generator for generating gas, built-in removing gaseous impurity
Reaction solution (such as sodium hydroxide solution, copper/saturated copper sulphate solution);By gas derived from plastic straw 14, or use drainage
It collects, or is passed directly into the relevant nature test for verifying gas in invisible spectro reaction solution.If completing the flammable examination of gas
When testing, the sharp nozzle end of implosion guard inner tube 11 connects two-way glass point mouth 17 as shown in Figure 3 i.e. by the second plastic flexible pipe 18
Can, the interior caliber of the second plastic flexible pipe 18 is greater than the interior caliber of plastic straw 14.
The device can be used for ethylbenzene, test to the preparation of the organic matters such as di-tert-butyl, acetophenone.When doing such experiment,
Remove spare syringe 1, drying receptacle of the conical flask 2 as gas is directly connected with the flask of preparation, built-in suitable chlorine
Change calcium desiccant, is recycled in the water or lye that the hydrogen halide of export plastic straw 14 can be passed directly into beaker.It overcomes
The shortcomings that traditional gas recyclable device needs fixed and exhaust gas easily to reveal and cause laboratory pollution.
Anti-suck, explosion-proof principle: when experiment, if being positive pressure in conical flask 2, gas, which can rush, heaves strip latex thin skin
10, so that gas is smoothly discharged from gas vent 16;If being negative pressure in conical flask 2, strip latex thin skin 10 will tightly
The end for being attached to air guide glass inner tube 6 is inhaled, that is, has blocked gas vent 16, has blocked the reflux of gas, it is therefore prevented that liquid suck-back is existing
The generation of elephant.When preparing the gases such as readily soluble ammonia, hydrogen chloride, because gas is discharged by micro- diameter of plastic straw 14, it can make
The velocity of discharge of gas be greater than its solution rate, therefore will not because gas dissolve it is too fast due to generate liquid suck-back the phenomenon that, prevent from sending out
Raw secondary suck-back.Even if a small amount of reflux occurs because of gas dissolution, also air guide glass can be tightly attached to because of strip latex thin skin 10
The end of inner tube 6 blocks and terminates.Therefore use the device that there is dual fail-safe anti-suck effect.
It is proved by flammability test, implosion guard inner tube 11 has apparent explosion-proof, is carrying out gas flammability
When test, even if containing a certain amount of air in the imflammable gas of preparation, gas generating unit will not explode.Because from double
The tempering of the burning to come to 17 port of glass point mouth can cause after encountering explosion-proof wire mesh column 12 because heat scatters and disappears rapidly
The temperature of gas reduces and extinguishes or block, therefore the tempering burnt is difficult to burn into outer glass tube 7 and conical flask 2.
The above is only the preferred embodiment of the utility model only, is not intended to limit the protection model of the utility model
It encloses.Any modification, equivalent substitution, improvement and etc. made within the spirit and principle of the present invention, are all contained in this reality
With in novel protection scope.
Claims (10)
1. with anti-suck, explosion prevention function gas experiment multi-purpose device, which is characterized in that including conical flask (2) and it is explosion-proof prevent
Suck-back device;The conical flask (2) is furnished with biforate rubber stopper (3), and a hole is inserted with the two-way sharp mouth bend pipe in right angle on biforate rubber stopper (3)
(4), another hole is connect with described explosion-proof suck-back device one end, and two-way sharp mouth bend pipe (4) other end in right angle passes through the first plastics
Hose (5) is connect with syringe (1) or gas with various generating device;The explosion-proof suck-back device other end passes through plastic straw (14)
It is connect with gas with various collection device (13) or the explosion-proof suck-back device other end passes through the second plastic flexible pipe (18) and two-way glass
Glass point mouth (17) connection;
The explosion-proof suck-back device is by air guide glass inner tube (6), outer glass tube (7), the first single hole rubber plug (8), the second single hole
Rubber plug (9) and implosion guard inner tube (11) composition;Outer glass tube (7) interior caliber is 15mm, is equipped with close to conical flask (2) one end
First single hole rubber plug (8), the other end are equipped with the second single hole rubber plug (9);It is inserted through biforate rubber stopper (3) air guide glass inner tube (6) one end
In conical flask (2), the other end inserts in outer glass tube (7) through the first single hole rubber plug (8);Air guide glass inner tube (6) outer tube diameter
It is 5 ~ 6mm for 7~8mm, interior caliber, the port that air guide glass inner tube (6) inserts in outer glass tube (7) interior one end has been blocked through copper wire
It tightens and strip latex thin skin (10) in the raw, strip latex thin skin (10) length is 50mm, width and air guide
Glass inner tube (6) outer tube diameter is equal sized;The port that air guide glass inner tube (6) inserts in outer glass tube (7) interior one end is through fusing
The gas vent (16) that necking, polishing are formed, gas vent (16) aperture are 3mm;Implosion guard inner tube (11) is sharp nozzle canula, point
Mouth end is connect through plastic straw (14) with gas collector (13) or sharp nozzle end is through the second plastic flexible pipe (18) and two-way glass
Sharp mouth (17) connection, the interior caliber of plastic straw (14) is 1.5 ~ 2mm, and the other end inserts in outside glass through the second single hole rubber plug (9)
It manages in (7), it is tightly packed in the straight tube of implosion guard inner tube (11) to have explosion-proof wire mesh column (12).
2. the gas experiment multi-purpose device according to claim 1 with anti-suck, explosion prevention function, which is characterized in that institute
The interior caliber for stating the second plastic flexible pipe (18) is greater than the interior caliber of plastic straw (14).
3. the gas experiment multi-purpose device according to claim 1 with anti-suck, explosion prevention function, which is characterized in that institute
The length for stating explosion-proof wire mesh column (12) is 3~4cm, and the diameter of wire is 0.1 ~ 0.15mm.
4. the gas experiment multi-purpose device according to claim 1 with anti-suck, explosion prevention function, which is characterized in that institute
Strip latex thin skin (10) is stated with a thickness of 0.5 ~ 1mm.
5. described in any item gas experiment multi-purpose devices with anti-suck, explosion prevention function according to claim 1 ~ 4, feature
It is, the biforate rubber stopper (3) is 4# rubber plug;
The first single hole rubber plug (8) and the second single hole rubber plug (9) are 0# rubber plug.
6. described in any item gas experiment multi-purpose devices with anti-suck, explosion prevention function according to claim 1 ~ 4, feature
It is, outer glass tube (7) length is 50mm;
The air guide glass inner tube (6) is right-angle elbow pipe, and the pipe overall length of the one end connecting with outer glass tube (7) is 40mm,
The pipe overall length of the other end is 50mm.
7. described in any item gas experiment multi-purpose devices with anti-suck, explosion prevention function according to claim 1 ~ 4, feature
It is, the bore of the two-way sharp mouth bend pipe (4) in the right angle is 3 ~ 4mm;
Implosion guard inner tube (11) length is 50mm, outer diameter is 7~8mm, and the bore of sharp nozzle end is 4mm.
8. the gas experiment multi-purpose device according to claim 1 or 3 with anti-suck, explosion prevention function, which is characterized in that
The wire of the explosion-proof wire mesh column (12) is derived from the copper wire in stainless steel window screening or conducting wire.
9. the gas experiment multi-purpose device according to claim 7 with anti-suck, explosion prevention function, which is characterized in that institute
The piston (15) for stating syringe (1) is wrapped with the plastic film tightened through copper wire.
10. according to claim 1 or the gas experiment multi-purpose device described in 9 with anti-suck, explosion prevention function, feature exist
In the conical flask (2) is reaction vessel, purifying vessel or drying receptacle.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115104534A (en) * | 2022-07-19 | 2022-09-27 | 赣南师范大学 | Non-damage physical disinfection and separation method after plant callus contamination |
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2019
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115104534A (en) * | 2022-07-19 | 2022-09-27 | 赣南师范大学 | Non-damage physical disinfection and separation method after plant callus contamination |
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