CN209690139U - A kind of isothermal adsorption device changing gas density - Google Patents

A kind of isothermal adsorption device changing gas density Download PDF

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Publication number
CN209690139U
CN209690139U CN201920439211.3U CN201920439211U CN209690139U CN 209690139 U CN209690139 U CN 209690139U CN 201920439211 U CN201920439211 U CN 201920439211U CN 209690139 U CN209690139 U CN 209690139U
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gas
gas density
adsorption
switch valve
piping connection
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李波波
陈帅
张尧
王斌
高政
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Guizhou University
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Guizhou University
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Abstract

The utility model discloses a kind of isothermal adsorption devices for changing gas density, it includes: mixed gas feed system, and the mixed gas feed system and gas mixer (7) pass through piping connection;Gas mixer (7) and survey gas density mixing tank (11) pass through piping connection;It surveys gas density mixing tank (11) and gas adsorption system passes through piping connection;Gas adsorption system and pressure-loaded system pass through piping connection;It is equipped with Gas Density Sensor (12) in the survey gas density mixing tank (11), Gas Density Sensor is connect by conducting wire with display (13);Solving the prior art not can be used for changing the isothermal adsorption device of gas density, lead to do the technical problems such as the adsorption isotherm experiment under gas with various density conditions.

Description

A kind of isothermal adsorption device changing gas density
Technical field
The utility model belongs to experimental apparatus technical field more particularly to a kind of isothermal adsorption dress for changing gas density It sets.
Background technique
China is used as coal production big country, during coal mining activity, it is easy to natural environmental condition is destructively descended, such as It is mixed into the original density conditions of the biggish gas and changing of density.Contain coal bed gas resource abundant in coal seam, main component is Gas.Coal reservoir fracture system is one of important parameter of coal-bed gas exploitation, and permeability is always with the variation relation of various conditions The concern of numerous researchers, wherein crustal stress is sensitive prime factor of its variation, but with the increase of seam mining depth, The atmospheric density brought into therewith also increases, thus, influence of the mixed gas density to coal seam permeability can not be ignored, coal body infiltration The relationship of rate and crustal stress has many researchers and did corresponding research, but carries out the isothermal under gas with various density conditions Adsorption experiment is also fewer, and influence of the density of learning gas to coal gas adsorption amount is of great significance.So far, do not have also Have the isothermal adsorption device that can be used for changing gas density, it is therefore necessary to existing adsorbent equipment carry out certain improvement with Simulate the variation of coal mining scene mixed gas density.
Utility model content
Technical problem to be solved by the utility model is: a kind of isothermal adsorption device for changing gas density is provided, with solution Certainly the prior art not can be used for changing the isothermal adsorption device of gas density, cause to do under gas with various density conditions The technical problems such as adsorption isotherm experiment.
The technical solution of the utility model is:
A kind of isothermal adsorption device changing gas density, it includes: mixed gas feed system, and the mixed gas supplies Pass through piping connection to system and gas mixer;Gas mixer and survey gas density mixing tank pass through piping connection; It surveys gas density mixing tank and gas adsorption system passes through piping connection;Gas adsorption system and pressure-loaded system pass through pipeline Connection;Gas Density Sensor is installed, Gas Density Sensor passes through conducting wire and display in the survey gas density mixing tank Device connection.
The mixed gas feed system includes the first air accumulator and the second air accumulator;First air accumulator and gas mixing fill It sets and is sequentially installed with first switch valve and first pressure gauge on the pipeline of connection;What the second air accumulator was connect with gas mixer Second switch valve and second pressure gauge are sequentially installed on pipeline.
Gas mixer is sequentially installed with booster pump, vacuum pump and the with surveying on the pipeline that connect of gas density mixing tank Five switch valves.
Gas adsorption system includes reference chamber and adsorption chamber, and reference chamber and adsorption chamber pass through piping connection;On connecting line 7th switch valve is installed;6th switch valve and third pressure gauge are installed on reference chamber air inlet pipeline;Adsorption chamber is equipped with outside Constant temperature water bath system.
Pressure-loaded system includes axis press pump and confining pressure pump;Axis press pump and confining pressure pump respectively with the absorption of gas adsorption system Room connection.
A kind of test method for the isothermal adsorption device changing gas density, it includes:
Raw coal sample is put into adsorption chamber by step 1 first, is opened vacuum pump and is carried out de- vacuum processing to experimental provision;
Adsorption chamber and reference chamber are put into the constant temperature water bath system for setting temperature, and apply simultaneously to adsorption chamber by step 2 Add constant shaft pressure and confining pressure;
Step 3 first opens the first air accumulator that helium is housed, and closes the 7th switch valve, opens the 4th switch valve, third is opened Valve and the 5th switch valve are closed, after so that density is reached experiment setting value, the 6th switch valve is opened, gas is passed through reference chamber, surveyed The 7th switch valve is opened after constant-pressure, is passed through gas in adsorption chamber, measures volume change;
It is after step 4, records of values, helium processing is clean, coal sample test specimen is changed, second switch valve, third are opened Switch valve and the 4th switch valve, are passed through methane, make helium and methane blended, reach experiment by densimeter measurement density later and set The 6th switch valve is opened after definite value makes methane and helium mix gas enter reference chamber, measures pressure, opens after stable reading 7th switch valve makes gas enter adsorption chamber, and methane and helium mix gas start to be adsorbed on raw coal pore surface, measures it certainly By spatial volume;
Step 5 finally establishes a Dynamic Adsorption equilibrium state, measures the pressure and body of mixed gas under the state Product, the gas volume being adsorbed at a given pressure is calculated according to the difference of the initial volume of mixed gas and final volume.
Beneficial effect
The utility model connects two air accumulators with gas mixer by gas mixer to mix gas Close, and vacuum pump be set in connecting tube, reduce experimental error, gas mixing system Connection Density detecting element can be real-time The variation of monitored density, and variable density can be controlled by switch valve, pass through the axis press pump connected in adsorption chamber end port It is loaded with confining pressure pump to sample, and constant temperature water bath system is set outside adsorption chamber, temperature, stress and mixed gas can be carried out The experiment that variable density influences permeability.The utility model can make raw coal carry out the isothermal under gas with various density conditions Adsorption experiment, and be able to carry out not coaxially pressure and confining pressure various factors coupling under the conditions of adsorption isotherm experiment, being capable of real simulation The adsorption isotherm experiment of mixed gas in process of coal mining, the experimental provision is simple to operation, and using effect is good, is easy to push away Extensively;Solving the prior art not can be used for changing the isothermal adsorption device of gas density, lead to that gas with various density cannot be done Under the conditions of the technical problems such as adsorption isotherm experiment.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model entirety;
Fig. 2 is the structural schematic diagram of the utility model gas mixer;
In figure: the first air accumulator of 1-, 2- first switch valve, 3- first pressure gauge, the second air accumulator of 4-, 5- second switch Valve, 6- second pressure gauge, 7- gas mixer, 8- booster pump, 9- vacuum pump, the 5th switch valve of 10-, 12- survey gas density Mixing tank, 12- inductor, 13- display, the 6th switch valve of 14-, 15- reference chamber, 16- third pressure gauge, 18- adsorption chamber, 19- constant temperature water bath system, 20- axis press pump, 21- confining pressure pump, 22- third switch valve, 23- gas mixing box, 24- the 4th switch Valve.
Specific embodiment
Please refer to Fig. 1-2
A kind of isothermal adsorption device changing gas density, it includes: mixed gas feed system, and the mixed gas supplies Pass through piping connection to system and gas mixer 7;Gas mixer 7 and survey gas density mixing tank 11 pass through pipeline and connect It connects;It surveys gas density mixing tank 11 and gas adsorption system passes through piping connection;Gas adsorption system and pressure-loaded system are logical Cross piping connection;Gas Density Sensor 12 is installed in the survey gas density mixing tank 11, Gas Density Sensor passes through Conducting wire is connect with display 13.
The mixed gas feed system includes the first air accumulator 1 and the second air accumulator 4;First air accumulator 1 and gas are mixed It attaches together and is sequentially installed with first switch valve 2 and first pressure gauge 3 on the pipeline for setting 7 connections;Second air accumulator 4 is filled with gas mixing It sets and is sequentially installed with second switch valve 5 and second pressure gauge 6 on the pipeline of 7 connections.
Booster pump 8, vacuum pump are sequentially installed on the pipeline that gas mixer 7 is connect with survey gas density mixing tank 11 9 and the 5th switch valve 10.
Gas adsorption system includes reference chamber 15 and adsorption chamber 18, and reference chamber 15 and adsorption chamber 18 pass through piping connection;Even Adapter tube road is equipped with the 7th switch valve 17;The 6th switch valve 14 and third pressure gauge are installed on 15 air inlet pipeline of reference chamber 16;Constant temperature water bath system 19 is equipped with outside adsorption chamber (18).
Pressure-loaded system includes axis press pump 20 and confining pressure pump 21;Axis press pump 20 and confining pressure pump 21 respectively with gas absorption system The adsorption chamber 18 of system connects.
In use, raw coal sample is put into adsorption chamber first, vacuum pump is opened, closes rest switch valve, experiment is filled It sets and carries out de- vacuum processing, be then put into adsorption chamber and reference chamber in the constant temperature water bath system for setting temperature, and right simultaneously Adsorption chamber applies constant shaft pressure and confining pressure.The first air accumulator that helium is housed first is opened later, closes the 7th switch valve, opens the Four switch valves, third switch valve and the 5th switch valve, will after so that density is reached experiment setting value through mixing after a period of time 6th switch valve is opened, and gas is passed through reference chamber, is opened the 7th switch valve after measuring pressure, is passed through gas in adsorption chamber, Measure volume change;It is after to records of values, helium processing is clean, coal sample test specimen is changed later, opens second switch valve With third switch valve and the 4th switch valve, it is passed through methane, makes helium and methane blended, density is measured by densimeter later and is reached Opening the 6th switch valve after experiment setting value makes methane and helium mix gas enter reference chamber, pressure is measured, to stable reading Opening the 7th switch valve afterwards makes gas enter adsorption chamber, and methane and helium mix gas start to be adsorbed on raw coal pore surface, survey Its fixed free space volumes, finally establish a Dynamic Adsorption equilibrium state, measure under the state pressure of mixed gas and Volume can calculate the gas being adsorbed at a given pressure according to the initial volume of mixed gas and the difference of final volume Volume.

Claims (5)

1. a kind of isothermal adsorption device for changing gas density, it includes: mixed gas feed system, it is characterised in that: described Mixed gas feed system and gas mixer (7) pass through piping connection;Gas mixer (7) is mixed with gas density is surveyed Case (11) passes through piping connection;It surveys gas density mixing tank (11) and gas adsorption system passes through piping connection;Gas absorption system System passes through piping connection with pressure-loaded system;Gas Density Sensor is installed in the survey gas density mixing tank (11) (12), Gas Density Sensor is connect by conducting wire with display (13).
2. a kind of isothermal adsorption device for changing gas density according to claim 1, it is characterised in that: the gaseous mixture Body feed system includes the first air accumulator (1) and the second air accumulator (4);First air accumulator (1) is connect with gas mixer (7) Pipeline on be sequentially installed with first switch valve (2) and first pressure gauge (3);Second air accumulator (4) and gas mixer (7) Second switch valve (5) and second pressure gauge (6) are sequentially installed on the pipeline of connection.
3. a kind of isothermal adsorption device for changing gas density according to claim 1, it is characterised in that: gas mixing dress It sets and is sequentially installed with booster pump (8) on the pipeline that (7) are connect with survey gas density mixing tank (11), vacuum pump (9) and the 5th is opened It closes valve (10).
4. a kind of isothermal adsorption device for changing gas density according to claim 1, it is characterised in that: gas absorption system System includes reference chamber (15) and adsorption chamber (18), and reference chamber (15) and adsorption chamber (18) pass through piping connection;Pacify on connecting line Equipped with the 7th switch valve (17);The 6th switch valve (14) and third pressure gauge are installed on reference chamber (15) air inlet pipeline (16);Constant temperature water bath system (19) are equipped with outside adsorption chamber (18).
5. a kind of isothermal adsorption device for changing gas density according to claim 1, it is characterised in that: pressure-loaded system System includes axis press pump (20) and confining pressure pump (21);Axis press pump (20) and confining pressure pump (21) respectively with the adsorption chamber of gas adsorption system (18) it connects.
CN201920439211.3U 2019-04-02 2019-04-02 A kind of isothermal adsorption device changing gas density Active CN209690139U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109870400A (en) * 2019-04-02 2019-06-11 贵州大学 A kind of isothermal adsorption device and test method changing gas density
CN110018107A (en) * 2019-05-08 2019-07-16 贵州大学 A kind of the isothermal adsorption device and operating method of changeable mixed gas viscosity
CN110987719A (en) * 2019-12-26 2020-04-10 辽宁工程技术大学 Coal adsorbs flue gas process simulation experiment system of power plant

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109870400A (en) * 2019-04-02 2019-06-11 贵州大学 A kind of isothermal adsorption device and test method changing gas density
CN110018107A (en) * 2019-05-08 2019-07-16 贵州大学 A kind of the isothermal adsorption device and operating method of changeable mixed gas viscosity
CN110987719A (en) * 2019-12-26 2020-04-10 辽宁工程技术大学 Coal adsorbs flue gas process simulation experiment system of power plant

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